光谱学与光谱分析 |
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Raman Spectroscopic Study of Ming Dynasty Bar-Tile from Heijing of Lufeng |
WANG Yi-lin1,YANG Qun1,LI Chao-zhen2 |
1. Department of Physics,Yunnan Chuxiong Teachers College,Chuxiong 675000,China 2. Yunnan Chuxiong Museum,Chuxiong 675000,China |
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Abstract Ming dynasty bar-tile from the archaeological site of Heijing (Lufeng of Yunnan Province, China ) was analyzed by Raman microscopy, X-ray diffraction and electron probe microscopy (EPMA). It was found that the major components of the tile are SiO2, besides moonstone(KAlSi3O8var.of K-orthoclase), Na-orthoclase(NaAlSi3O8)and an unknown mineral(Al, Fe)3(PO4,VO4)2(OH)3·8H2O etc. The studies revealed that the agglomerant temperature of the bar-tile reached up to 1 500 ℃, indicating that the agglomerant technology of ceramics of Yunnan in the Ming dynasty (before 17 century) already attained a high level. Raman microscopy proves especially excellent in studing antiques. The results show that the facility and reliability of Raman spectroscopy,as a non-destructive unique technique, are suitable for the discrimination between moonstone and K-orthoclase within tile. No other technique tried was successful in its identification. This research demonstrates that only by combining several complementary techniques is possible to conduct comprehensive research on antiques.
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Received: 2002-08-05
Accepted: 2002-12-25
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Corresponding Authors:
WANG Yi-lin
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Cite this article: |
WANG Yi-lin,YANG Qun,LI Chao-zhen. Raman Spectroscopic Study of Ming Dynasty Bar-Tile from Heijing of Lufeng [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(07): 823-825.
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http://www.gpxygpfx.com/EN/Y2004/V24/I07/823 |
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