|
|
|
|
|
|
| Study on the Fracture Mechanism by Multi-Spectrum Methods |
| HU Rui-feng1, HAN Jing-hua1, FENG Guo-ying1*, HAN Wei2, ZHU Qi-hua2, WANG Zhu-ping1, GU Qiong-qiong1 |
1. College of Electronics ＆ Information Engineering, Sichuan University, Chengdu 610064, China
2. Laser Fusion Research Center, China Academy of Engineering Physics, Mianyang 621900, China |
|
|
|
|
Abstract Fused silica glass is a kind of indispensable material in high-energy laser system, and the damage of it has been one of the bottlenecks restricting the energy of system. In this paper, laser pulse shock wave was used to break down the fused glass samples, then the cause of the morphology of fractures on fused silica glass surface as well as internal phase transition were investigated experimentally and theoretically by multi-spectrum detecting of the samples before and after fracture, and the relationship between fracture morphologies and phase transition structure was explained from macro to micro. The fracture of the fused silica was induced by laser plasma shock wave, and during the shock wave, the tip of hoop stress produced from the inside glass would promote the crack propagation outward. We found that the whole fracture region could be divided into hackle zone, mist zone and mirror zone by morphology differences produced by the tip of hoop stress. The transmittance spectra and energy dispersive spectrometer were used to detect the samples before and after fracture. The results showed that the decrease of the transmittance and band gap of the glass were induced by the cracks, and the oxygen free or absent appeared in the fracture zone. Using the Raman spectrum to detect the different morphological areas of samples before and after broken, we found that the Si—O—Si band of fused glass breakage and recombination could reduce the relative content of three- and four-number rings structures corresponding to the stishovite and coesite of hackle zone, mist zone and mirror zone at the macro level. This kind of changes destroyed the mesh topology severely and induced the material fracture zone transforming to a higher density phase. From the micro level, the non-bridging oxygen hole center and E’center led to the decrease of the optical band gaps as well as transmittance which seriously affected the performance of glass.
|
|
Received: 2016-12-05
Accepted: 2017-05-06
|
|
|
|
Corresponding Authors:
FENG Guo-ying
E-mail: guoing_feng@scu.edu.cn
|
|
[1] YU Zhen-kun, HE Hong-bo , QI Hong-ji, et al(余振坤，贺洪波，齐红基，等). Chinese Physics Letters(中国物理快报), 2013, 30(6): 067801.
[2] HE Xiang, WANG Gang, ZHAO Heng, et al(何 祥，王 刚，赵 恒，等). Chinese Physics B(中国物理B), 2016, 25(4): 048104.
[3] Liang Lv, Ma Ping, Huang Jinyong, et al. Applied Optics, 2016, 55(9): 2252.
[4] ZUO Yan-lei, WEI Xiao-feng, ZHOU Kai-nan, et al(左言磊，魏晓峰，周凯南，等). Chinese Physics B(中国物理B), 2016, 25(3): 256.
[5] Ocana J L, Morales M, Molpeceres C, et al. Applied Surface Science, 2004, 238(1-4): 242.
[6] ZHOU Qiang, QIU Rong, JIANG Yong, et al(周 强，邱 荣，蒋 勇，等). Chinese Optics Letters, 2016, 14(5): 051402.
[7] Raman R N, Demos S G, Shen N, et al. Optics Express, 2016, 24(3): 2634.
[8] Zhen J S, Yang Q, Yan Y H, et al. Radiation Effects and Defects in Solids, 2016, 171(3-4): 340.
[9] Lawn B. Fracture of brittle solids. Cambridge University Press, 1993. 25.
[10] Kajihara K, Hirano M, Skuja L, et al. Physical Review B Condensed Matter, 2008, 78(9): 1884.
[11] Cheng S, Schiefelbein S, Moore L, et al. Journal of Non-Crystalline Solids, 2006, 352(28): 3140.
[12] LU Peng-fei, WU Li-yuan, YANG Yang, et al(芦鹏飞，伍利源, 杨 阳，等). Chinese Physics B(中国物理B), 2016, 25(8): 086801.
[13] Shimada Y, Okuno M, Syono Y, et al. Physics & Chemistry of Minerals, 2002, 29(4): 233.
[14] Arndt J, Stffler D. The Science of Nature, 1968, 55(5): 226.
[15] Alfredo Pasquarello R C. Physical Review Letters, 1998, 80(23): 5145. |
| [1] |
WANG Gan-lin1, LIU Qian1, LI Ding-ming1, YANG Su-liang1*, TIAN Guo-xin1, 2*. Quantitative Analysis of NO-3，SO2-4，ClO-4 With Water as Internal Standard by Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1855-1861. |
| [2] |
HUANG Bin, DU Gong-zhi, HOU Hua-yi*, HUANG Wen-juan, CHEN Xiang-bai*. Raman Spectroscopy Study of Reduced Nicotinamide Adenine Dinucleotide[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1679-1683. |
| [3] |
ZHU Xiang1, 2*, YUAN Chao-sheng1, CHENG Xue-rui1, LI Tao1, ZHOU Song1, ZHANG Xin1, DONG Xing-bang1, LIANG Yong-fu2, WANG Zheng2. Study on Performances of Transmitting Pressure and Measuring Pressure of [C4mim][BF4] by Using Spectroscopic Techniques[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1674-1678. |
| [4] |
WANG Ming-xuan, WANG Qiao-yun*, PIAN Fei-fei, SHAN Peng, LI Zhi-gang, MA Zhen-he. Quantitative Analysis of Diabetic Blood Raman Spectroscopy Based on XGBoost[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1721-1727. |
| [5] |
YOU Gui-mei1, ZHANG Wen-jie1, CAO Zhen-wei2, HAN Xiang-na1*, GUO Hong1. Analysis of Pigments of Colored Paintings From Early Qing-Dynasty Fengxian Dian in the Forbidden City[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1874-1880. |
| [6] |
LI Qing1, 2, XU Li1, 2, PENG Shan-gui1, 2, LUO Xiao1, 2, ZHANG Rong-qin1, 2, YAN Zhu-yun3, WEN Yong-sheng1, 2*. Research on Identification of Danshen Origin Based on Micro-Focused
Raman Spectroscopy Technology[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1774-1780. |
| [7] |
WANG Zhong, WAN Dong-dong, SHAN Chuang, LI Yue-e, ZHOU Qing-guo*. A Denoising Method Based on Back Propagation Neural Network for
Raman Spectrum[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1553-1560. |
| [8] |
FU Qiu-yue1, FANG Xiang-lin1, ZHAO Yi2, QIU Xun1, WANG Peng1, LI Shao-xin1*. Research Progress of Pathogenic Bacteria and Their Drug Resistance
Detection Based on Surface Enhanced Raman Technology[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1339-1345. |
| [9] |
YAN Ling-tong, LI Li, SUN He-yang, XU Qing, FENG Song-lin*. Spectrometric Investigation of Structure Hydroxyl in Traditional Ceramics[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1361-1365. |
| [10] |
ZHAO Yong1, HE Men-yuan1, WANG Bo-lin2, ZHAO Rong2, MENG Zong1*. Classification of Mycoplasma Pneumoniae Strains Based on
One-Dimensional Convolutional Neural Network and
Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1439-1444. |
| [11] |
LI Meng-meng1, TENG Ya-jun2, TAN Hong-lin1, ZU En-dong1*. Study on Freshwater Cultured White Pearls From Anhui Province Based on Chromaticity and Raman Spectra[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1504-1507. |
| [12] |
JIAO Ruo-nan, LIU Kun*, KONG Fan-yi, WANG Ting, HAN Xue, LI Yong-jiang, SUN Chang-sen. Research on Coherent Anti-Stokes Raman Spectroscopy Detection of
Microplastics in Seawater and Sand[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1022-1027. |
| [13] |
ZHANG Li-sheng. Photocatalytic Properties Based on Graphene Substrate[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1058-1063. |
| [14] |
LÜ Yang, PEI Jing-cheng*, GAO Ya-ting, CHEN Bo-yu. Chemical Constituents and Spectra Characterization of Gem-Grade
Triplite[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1204-1208. |
| [15] |
FU Ying-ying, ZHANG Ping, ZHENG Da-wei , LIN Tai-feng*, WANG Hui-qin, WU Xi-hao, SONG Jia-chen. Preparation and SERS Performance of Au-Nylon Flexible Membrane Substrate[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 692-698. |
|
|
|
|
