光谱学与光谱分析 |
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Study on the Vibrational Spectra and XRD Characters of Huanglong Jade from Longling County, Yunnan Province |
PEI Jing-cheng1, FAN Lu-wei2, XIE Hao3* |
1. Gemological Institute, China University of Geosciences, Wuhan 430074, China 2. Yifu Museum, China University of Geosciences, Wuhan 430074, China 3. Wuhan University of Engineering Science, Wuhan 430200, China |
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Abstract Based on the conventional test methods, the infrared absorption spectrum, Raman spectrum and X-ray diffraction (XRD) were employed to study the characters of the vibration spectrum and mineral composition of Huanglong jade. The testing results show that Huanglong jade shows typical vibrational spectrum characteristics of quartziferous jade. The main infrared absorption bands at 1 162, 1 076, 800, 779, 691, 530 and 466 cm-1 were induced by the asymmetric stretching vibration, symmetrical stretching vibration and bending vibration of Si-O-Si separately. Especially the absorption band near 800 cm-1 is split, which indicates that Huanglong jade has good crystallinity. In Raman spectrum, the main strong vibration bands at 463 and 355 cm-1 were attributed to bending vibration of Si—O—Si. XRD test confirmed that Quartz is main mineral composition of Huanglong jade and there is a small amount of hematite in red color samples which induced the red color of Huanglong jade. This is the first report on the infrared, Raman and XRD spectra feature of Huanglong jade. It will provide a scientific basis for the identification, naming and other research for huanglong jade.
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Received: 2014-07-16
Accepted: 2014-10-12
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Corresponding Authors:
XIE Hao
E-mail: siobhanxie@163.com
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[1] ZHANG Jin-fu, WANG Shi-xun(张金富, 王世勋). Yunnan Geology(云南地质), 2007, 26(1): 25. [2] YAO Xue(姚 雪). Journal of Gems and Gemmology(宝石和宝石学杂志), 2007, 9(2): 13. [3] LIU Xue, QIAN Jian-ping, CHEN Shan-shan(刘 学,钱建平,陈珊珊). Mineral Resources and Geology(矿产与地质), 2013, 27(2): 162. [4] WEN Lu, LIANG Wan-xue, ZHANG Zheng-gang, et al(闻 辂, 梁婉雪, 章正刚,等). The Infrared Spectroscopy of Minerals(矿物红外光谱学). Chongqing: Chongqing University Press(重庆: 重庆大学出版社), 1989 . 116. [5] Etchepare J, Merian M, Smetankine L. Journal of Chemical Physics, 1974, 60: 1873. [6] Masaki Enami, Tadao Nishiyama, TakashiI Mouri. American Mineralogist, 2007, 92: 1303. [7] ZHANG Yong, LU Tai-jin, YANG Tian-chang, et al(张 勇,陆太进,杨天畅,等). Acta Petrologica et Mineralogica (岩石矿物学杂志), 2014, 33(s1): 83. |
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