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| A Static Sample Cell System for Gas Absorbance Spectrum Measurement Under High Temperature |
| HUANG Wen-jian, ZHANG Ming-ke, GAO Guang-zhen*, WANG Xuan, YANG Yu-bing, CAI Ting-dong* |
School of Physics and Electronic Engineering, Jiangsu Normal University, Xuzhou 221116, China
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Abstract In the practical high-temperature gas detection case, the measured results of the gas spectral line parameters are often affected by temperature changes. Sometimes, it is even difficult to achieve real-time online measurement.Therefore, this paper aims to design and process a new high-temperature sample cell to simulate a high-temperature environment and build a tunable diode laser absorption spectrum measurement system to detect the spectrums of the target gas in a high-temperature environment. In this way, the accurate detection of spectral line parameters can be achieved.In the design of a high-temperature sample cell, Comsol was used to simulate and analyze the solid thermal conductivity of various materials to determine the optimal processing materials and size. The results show that good properties of the high-temperature sample cell are obtained. It can work in the temperature range of 300~1 000 K and the pressure range of -0.1～10 atm. The maximum temperature deviation of the sample cell at 1 000 K is 20 K. The measured leakage rates at 300 and 1 000 K are 5 and 60 Pa·min-1, respectively.This paper uses a distributed feedback (DFB) semiconductor laser with a center wavelength of 1 573 nm as the light source to measure the partial high-temperature spectrums of CO molecules with relatively accurate parameters in the HITRAN2016 database. The comparison between the spectral line parameters obtained from the inversion and those in the HITRAN database indicates that the error is within 5%. The good performance of the designed high-temperature sample cell was proved, which can help in the measurement of gas spectral line parameters in high-temperature environments.
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Received: 2023-02-18
Accepted: 2023-10-16
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Corresponding Authors:
GAO Guang-zhen, CAI Ting-dong
E-mail: ggz@jsnu.edu.cn; caitingdong@126.com
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[1] Hansen N, Cool T A, Westmoreland P R, et al. Progress in Energy and Combustion Science, 2009, 35(2): 168.
[2] Witezl O, Klein A, Meffert C, et al. Optics Express, 2013, 21(17): 19951.
[3] PENG Wei, YANG Sheng-wei, HE Tian-bo, et al(彭 伟, 杨生威, 何天博, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2023, 43(3): 698.
[4] Liu K, Wang L, Tan T, et al. Sensors and Actuators B: Chemical, 2015, 220: 1000.
[5] Deng B T, Sima C, Xiao Y F, et al. Optics and Lasers in Engineering, 2022, 151: 106906.
[6] Nasim H, Jamil Y. Optics and Laser Technology, 2014, 56: 211.
[7] Goldenstein C S, Spearrin R M, Jeffries J B, et al. Progress in Energy and Combustion Science, 2016, 60: 132.
[8] Klingbeil A E, Jeffries J B, Hanson R K. Measurement Science and Technology, 2006, 17(7): 1950.
[9] He D, Peng Z M, Ding Y J. Fuel, 2021, 288: 118980.
[10] Bürkle S, Biondo L, Ding C P, et al. Flow, Turbulence and Combustion, 2018, 101(1): 139.
[11] Popa C, Banita S, Patachia M, et al. Romanian Reports in Physis, 2015, 67(3): 946.
[12] ZHANG Rui, WANG Biao, XUE Jin-bo, et al(张 瑞, 王 彪, 薛金波，等). Laser Journal(激光杂志), 2022, 43(10): 30.
[13] Liu N W, Xu L G, Zhou S, et al. Journal of Quantitative Spectroscopy and Radiative Transfer, 2019, 236: 106587.
[14] Qiao S D, Ma Y F, Patimisco P, et al. Optics Letters, 2021, 46(5): 977.
[15] SONG Zhen-ming, LI Ji-dong, PENG Zhi-min, et al(宋振明，李济东，彭志敏，等). Laser & Infrared(激光与红外)，2022, 52(4): 586.
[16] KAN Rui-feng, XIA Hui-hui, XU Zhen-yu, et al(阚瑞峰，夏晖晖，许振宇，等). Chinese Journal of Lasers(中国激光)，2018，45(9)：0911005.
[17] Xin F X, Li J, Guo J J, et al. Sensors, 2021, 21(5): 1722.
[18] Docquier N, Candel S. Progress in Energy and Combustion Science, 2002, 28(2): 107.
[19] CHEN Jiu-ying, LIU Jian-guo, HE Ya-bai, et al(陈玖英, 刘建国, 何亚柏, 等). Acta Physica Sinica(物理学报), 2013, 62(22): 224206.
[20] FU Na, ZHANG Xi(伏 娜, 张 晞). Journal of Beijing University of Aeronautics and Astronautics(北京航空航天大学学报), 2019, 45(4): 735. |
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