|
|
|
|
|
|
Study on Detection of Nafcillin Residues in Duck Meat Using Surface Enhanced Raman Spectroscopy |
PENG Yi-jie, LIU Mu-hua, ZHAO Jin-hui*, YUAN Hai-chao, LI Yao, TAO Jin-jiang, GUO Hong-qing |
Optics-Electrics Application of Biomaterials Lab, College of Engineering, Jiangxi Agricultural University, Nanchang 330045, China |
|
|
Abstract A new method using Surface enhanced Raman spectroscopy (SERS) was established for the rapid detection of Nafcillin residues in duck meat, and Au nanoparticles were used as enhancement substrate while NaCl solutions were used as active agent. In this research, the SERS characteristic peaks of Nafcillin solutions as well as their vibrational assignment were analyzed. Then, the SERS characteristic peaks of Nafcillin in duck extract were analyzed and determined for the identification of Nafcillin residues in duck meat,and the Raman intensities of nafcillin residues in duck meat extracted at 521 and 1 449 cm-1 were applied to optimize the detection conditions. Lastly, the internal standard method was used to quantitatively analyze the nafcillin residues in duck meat. It was revealed that 4 calibration curves built by Raman peaks intensities ratio had a good linearity when the residues concentrations of nafcillin in duck were 0.2~10 mg·L-1, and the determination coefficients were larger than 0.95. Three of the calibration curves using Raman peaks intensities ratio had superior accuracy with the recoveries of 88%~144%. The results showed the detection of nafcillin residues in duck meat using SERS was feasible, and the method was simple, rapid and accurate providing the technical support for detect the nafcillin residues in poultry meat food.
|
Received: 2016-11-10
Accepted: 2017-03-19
|
|
Corresponding Authors:
ZHAO Jin-hui
E-mail: zjhxiaocao@sina.com
|
|
[1] ZHU Zi-ying, GU Ren-ao, LU Tian-hong(朱自莹, 顾仁敖, 陆天虹). Application of Raman Spectroscopy in Chemistry(拉曼光谱在化学中的应用). Shengyang:Northeastern University Press(沈阳:东北大学出版社), 1998. 71.
[2] JI Wei(吉 薇). Studies on the Detection of Chloramphenicol and Its Sodium Succinate by Surface-Enhanced Raman Scattering(表面增强拉曼光谱测定氯霉素及其琥珀酸钠的研究). Jiangsu: Jiangnan University(江苏:江南大学), 2013. 1.
[3] SUN Mei-juan, TAO Zhan-hua(孙美娟, 陶站华). Journal of Guangxi Teachers Education University·Natural Science Edition(广西师范学院学报·自然科学版), 2014, 31(4): 27.
[4] WU Ya-dong, XU Wei-ping, JIN Qin-yu, et al(吴亚东, 徐维平, 金勤玉, 等). Guangzhou Chemical Industry(广州化工), 2015, 43(4): 17.
[5] LIU Yu-xing, JIAN Gui-qin, HE Xi-wen, et al(刘雨星, 菅桂芹, 何锡文, 等). Chinese Journal of Analytical Chemistry(分析化学), 2013, 41(2): 161.
[6] WU Qiang, HE Sheng-hu, CHEN Juan, et al(吴 强, 何生虎, 陈 娟, 等). Progress in Veterinary Medicine(动物医学进展), 2015, 36(6): 64.
[7] Bailón-Pérez M I, García-Campaa A M, del Olmo-Iruela M, et al. Journal of Chromatography, A, 2009, 1216(47): 8355.
[8] Ren Z Q, Zhang W D, Li J, et al. Journal of Chemical & Engineering Data, 2010, 55(8), 2687.
[9] TAO Xin-chen, HUANG He, LIAO Jian-meng, et al(陶昕晨, 黄 和, 廖建萌, 等). Journal of Chinese Institute of Food Science and Technology(中国食品学报), 2014, 14(1): 232.
[10] LIU Ping, HE Bao-xiang, HUANG Yun-fei(刘 平, 何宝祥, 黄云飞). The Rapid Diagnostic Stripe of the Candida Albicans in Cow Mastitis: (Chinese Patent)(奶牛乳房炎白色念珠菌快速诊断试纸条, 中国专利),201310674116.9. 2013-12-11.
[11] CHENG Jing-quan, YAO Su-wei(程敬泉, 姚素薇). Rare Metal Materials and Engineering(稀有金属材料与工程), 2012, 41(2): 348.
[12] WANG Lan, HUANG Shao-hua, HUANG Zu-fang et al(王 兰,黄少华,黄祖芳,等). The Journal of Light Scattering(光散射学报),2014, 26(1):13.
[13] WANG Shi, CHENG Jie, SU Xiao-ou(王 石,程 劼,苏晓鸥). Scientia Agricultura Sinica(中国农业科学),2014,47(11): 2224.
[14] ZHANG Quan, WENG Yu-xiang(张 权,翁羽翔). The Journal of Light Scattering(光散射学报),2015, 27(1):1.
[15] ZHAO Jin-hui, YUAN Hai-chao, HONG Qian, et al(赵进辉, 袁海超, 洪 茜, 等). Journal of Food Safety and Quality(食品安全质量检测学报), 2014, 5(3): 703.
[16] KANG Qian-qian, ZHOU Guang-ming(康倩倩, 周光明). The Journal of Light Scattering(光散射学报), 2011, 23(4): 368.
[17] Foteli W G, Lindsay F P, Bentley F F. Characteristic Raman Frequency of Organic Compounds(有机化合物的特征拉曼频率). Beijing: China Chemical Publishing House(北京:中国化学出版社), 1980. 93, 143.
[18] XU Yang, LUO Hai-xia, FAN Qiang, et al(徐 洋, 罗海霞, 范 强, 等). Contemporary Chemical Industry(当代化工), 2015, 44(4): 699.
[19] GAO Xiao-ling, Butler J S(高小玲, 巴特勒 J S). Chinese Journal of Analysis Laboratory(分析试验室), 1995, 14(4): 52. |
[1] |
XING Hai-bo1, ZHENG Bo-wen1, LI Xin-yue1, HUANG Bo-tao2, XIANG Xiao2, HU Xiao-jun1*. Colorimetric and SERS Dual-Channel Sensing Detection of Pyrene in
Water[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 95-102. |
[2] |
LU Wen-jing, FANG Ya-ping, LIN Tai-feng, WANG Hui-qin, ZHENG Da-wei, ZHANG Ping*. Rapid Identification of the Raman Phenotypes of Breast Cancer Cell
Derived Exosomes and the Relationship With Maternal Cells[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3840-3846. |
[3] |
GUO He-yuanxi1, LI Li-jun1*, FENG Jun1, 2*, LIN Xin1, LI Rui1. A SERS-Aptsensor for Detection of Chloramphenicol Based on DNA Hybridization Indicator and Silver Nanorod Array Chip[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3445-3451. |
[4] |
LI Wen-wen1, 2, LONG Chang-jiang1, 2, 4*, LI Shan-jun1, 2, 3, 4, CHEN Hong1, 2, 4. Detection of Mixed Pesticide Residues of Prochloraz and Imazalil in
Citrus Epidermis by Surface Enhanced Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3052-3058. |
[5] |
ZHAO Ling-yi1, 2, YANG Xi3, WEI Yi4, YANG Rui-qin1, 2*, ZHAO Qian4, ZHANG Hong-wen4, CAI Wei-ping4. SERS Detection and Efficient Identification of Heroin and Its Metabolites Based on Au/SiO2 Composite Nanosphere Array[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3150-3157. |
[6] |
SU Xin-yue1, MA Yan-li2, ZHAI Chen3, LI Yan-lei4, MA Qian-yun1, SUN Jian-feng1, WANG Wen-xiu1*. Research Progress of Surface Enhanced Raman Spectroscopy in Quality and Safety Detection of Liquid Food[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2657-2666. |
[7] |
ZHAO Yu-wen1, ZHANG Ze-shuai1, ZHU Xiao-ying1, WANG Hai-xia1, 2*, LI Zheng1, 2, LU Hong-wei3, XI Meng3. Application Strategies of Surface-Enhanced Raman Spectroscopy in Simultaneous Detection of Multiple Pathogens[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2012-2018. |
[8] |
CHENG Chang-hong1, XUE Chang-guo1*, XIA De-bin2, TENG Yan-hua1, XIE A-tian1. Preparation of Organic Semiconductor-Silver Nanoparticles Composite Substrate and Its Application in Surface Enhanced Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2158-2165. |
[9] |
LI Chun-ying1, WANG Hong-yi1, LI Yong-chun1, LI Jing1, CHEN Gao-le2, FAN Yu-xia2*. Application Progress of Surface-Enhanced Raman Spectroscopy for
Detection Veterinary Drug Residues in Animal-Derived Food[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(06): 1667-1675. |
[10] |
HUANG Xiao-wei1, ZHANG Ning1, LI Zhi-hua1, SHI Ji-yong1, SUN Yue1, ZHANG Xin-ai1, ZOU Xiao-bo1, 2*. Detection of Carbendazim Residue in Apple Using Surface-Enhanced Raman Scattering Labeling Immunoassay[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(05): 1478-1484. |
[11] |
LU Yan-hua, XU Min-min, YAO Jian-lin*. Preparation and Photoelectrocatalytic Properties Study of TiO2-Ag
Nanocomposites[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1112-1116. |
[12] |
WANG Yi-tao1, WU Cheng-zhao1, HU Dong1, SUN Tong1, 2*. Research Progress of Plasticizer Detection Based on Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1298-1305. |
[13] |
LI Wei1, 2, HE Yao1, 2, LIN Dong-yue2, DONG Rong-lu2*, YANG Liang-bao2*. Remove Background Peak of Substrate From SERS Signals of Hair Based on Gaussian Mixture Model[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 854-860. |
[14] |
HAN Xiao-long1, LIN Jia-sheng2, LI Jian-feng2*. SERS Analysis of Urine for Rapid Estimation of Human Energy Intake[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(02): 489-494. |
[15] |
HE Yao1, 2, LI Wei1, 2, DONG Rong-lu2, QI Qiu-jing3, LI Ping5, LIN Dong-yue2*, MENG Fan-li4, YANG Liang-bao2*. Surface Enhanced Raman Spectroscopy Analysis of Fentanyl in Urine Based on Voigt Line[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(01): 85-92. |
|
|
|
|