光谱学与光谱分析 |
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Determination of Phloroglucinol by a New Flow Injection Chemiluminescence Method |
XIE Cheng-gen,LI Huai-fen |
Department of Chemistry, West Anhui University, Liu An 237012, China |
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Abstract Abstract Chemiluminescence reaction of phloroglucinol with potassium permanganate in the presence of formaldehyde as an enhancer was investigated. A new chemiluminescence method for the determination of phloroglucinol with flow injection technique was developed. The linear range for phloroglucinol is 5.0×10-9-5.0×10-5 mol·L-1 with a detection limit of 3.0×10-9 mol·L-1. The relative standard deviation is 2.5% for 1.0×10-6 mol·L-1 phloroglucinol in 11 repeated measurements. The method has been used to determine the content of phloroglucinol in simulated water with satisfactory results.
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Received: 2003-05-07
Accepted: 2003-09-22
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Corresponding Authors:
XIE Cheng-gen
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Cite this article: |
XIE Cheng-gen,LI Huai-fen. Determination of Phloroglucinol by a New Flow Injection Chemiluminescence Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(12): 1521-1523.
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URL: |
https://www.gpxygpfx.com/EN/Y2004/V24/I12/1521 |
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