光谱学与光谱分析 |
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Determination of Trace Elements in Sika Bone Powder by Inductively Coupled Plasma Mass Spectrometry with Microwave Digestion |
LIU Yan-ming1, CHEN Zhi-yong1,HAN Jin-tu1, WANG Hui1 , WANG Zhi-wen2 |
1. College of Chemistry and Chemical Engineering, Xinyang Normal University, Xinyang 464000,China 2. School of Pharmacy, Peking University, Beijing 100083, China |
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Abstract Contents of trace elements in sika bone powder were determined with microwave digestion and inductively coupled plasma mass spectrometry. Under the optimum conditions, the detection limits (3σ, n=11) are in the range of 0.000 6-1.498 ng·mL-1 with relative standard deviations of 1.7%-6.8%. The recoveries are between 91% and 109%. The analytical results of national certified reference demonstrated the applicability of the proposed method.
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Received: 2005-02-28
Accepted: 2005-07-08
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Corresponding Authors:
LIU Yan-ming
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Cite this article: |
LIU Yan-ming,CHEN Zhi-yong,HAN Jin-tu, et al. Determination of Trace Elements in Sika Bone Powder by Inductively Coupled Plasma Mass Spectrometry with Microwave Digestion[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(05): 947-949.
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URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I05/947 |
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