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| Research on Steaming Procedure of Aconite Root with FTIR and Two-Dimensional IR Correlation Spectroscopy |
| WU Zhi-sheng1, LIU Xiao-na2, TAN Peng1, PEI Yan-ling3, DAI Xing-xing1, QIAO Yan-jiang1* |
1. Beijing University of Chinese Medicine, Beijing 100102, China
2. School of Integrated Traditional Chinese and Western Medicine, Bizhou Medical University, Yantai 256603, China
3. Ximihe Testing (Hebei) Co. Ltd., Baoding 071200, China |
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Abstract Fourier transform infrared spectroscopy (FTIR), second derivative infrared spectroscopy, and two-dimensional correlation infrared spectroscopy (2D-IR) were used to study the steaming procedure of aconite tuber. The results showed that samples with steaming procedures were similar to each other in one-dimensional IR spectra but different in 2D-IR spectra. The FTIR spectra combined with second derivative infrared spectroscopy of different samples during boiling procedure present characteristic peaks at 1 634.87 cm-1 (CO), 1 603.18, 1 571.58 cm-1, 1 485.09, 1 413.08 cm-1 (vibration of phenyl framework) and 1 153.73, 1 081.84, 1 021.35 cm-1 (C—O) respectively. There were two conspicuous time sequences in two dimensional infrared correlation spectroscopy of autopeaks intensity. Since, the intensity of autopeaks was relatively high during 2～3 and 8～9 h. The function of FTIR and 2D-IR for analysis of the alkaloid from aconite root attributed high speed and high efficiency. The results were reliable and valuable.
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Received: 2015-04-16
Accepted: 2015-11-09
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Corresponding Authors:
QIAO Yan-jiang
E-mail: yjqiao@263.net
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[1] Pharmacopoeia Committee of Ministry of Health, the People’s Republic of China(中华人民共和国卫生部药典委员会). Pharmacopoeia of People’s Republic of China·Ⅰ(中华人民共和国药典·一部). Beijing: Chemical Industry Press(北京: 化学工业出版社) , 2010. 177.
[2] ZHOU Lin, REN Yu-zhen, LI Fei, et al(周 林, 任玉珍, 李 飞, 等). Journal of Anhui TCM(安徽中医学院学报), 2012, 31 (5): 7.
[3] YANG Hui, YAN Fang(杨 慧, 严 芳). Guangming Journal of Chinese Medicine(光明中医), 2013, 28(2): 397.
[4] RAN Mao-xiong, GUO Jian-min(冉懋雄, 郭建民). Handbook of Modern Frying Chinese Medicinal Herbs(现代中药炮制手册). China Press of Traditional Ciinese Medicine(北京: 中国中医药出版社) , 2002. 464.
[5] PENG Yun, SHEN Yi, WU Pei-yi, et al(彭 云, 沈 怡, 武培怡, 等). Analytical Chemistry(分析化学), 2005, 33(10): 1499.
[6] YANG Chang-lin, HUANG Zhi-fang, ZHANG Yi-han, et al (杨昌林, 黄志芳, 张意涵, 等). China Journal of Chinese Material Medica(中国中药杂志), 2014, 39(24): 4798.
[7] WANG Chang-li, LEI Jian-lin, ZHANG Jun-wu, et al(王昌利, 雷建林, 张军武, 等). Journal of Shaanxi College of Traditional Chinese Medicine(陕西中医学院学报), 2009, 32(2): 61.
[8] CHEN Rong-chang, SUN Gui-bo, ZHANG Qiang, et al(陈荣昌, 孙桂波, 张 强, 等). Chinese Journal of Experimental Traditional Medical Formulae(中国实验方剂学杂志), 2014, 20(15): 237. |
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