光谱学与光谱分析 |
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Analysis of Different Parts of Scorpio by Fourier Transform Infrared Spectroscopy |
ZHANG Sheng-jun1, XU Chang-hua2, CHEN Jian-bo2, ZHOU Qun2, SUN Su-qin2* |
1. Department of Chemical and Biological Agriculture, Anshun College, Anshun 561000, China 2. Key Laboratory of Bioorganic Phosphorus Chemistry Biology (Ministry of Education), Department of Chemistry, Tsinghua University, Beijing 100084, China |
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Abstract Fourier transform infrared (FTIR) spectroscopy and second derivative IR spectroscopy were applied to analyze and evaluate different parts of Scorpio. The second derivative IR spectra show clear differences while the origin spectra are quite similar. It was found that proteins are the dominant components in each part and the tail has distinct proteins compared to the others; fats are mainly stored in the trunk; sulfates are ubiquitous in all parts. Interestingly, the back part of the trunk of degenerative Scorpio contains some purine. It was demonstrated that FTIR spectroscopy integrated with second derivative IR spectroscopy not only can offer a fast, comprehensive and objective methodology for analyzing and evaluating the micro-differences among the various parts of same medicinal materials, but also can provide a rational guidance for medicinal and pharmacological studies.
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Received: 2011-04-01
Accepted: 2011-07-20
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Corresponding Authors:
SUN Su-qin
E-mail: sunsq@tsinghua.edu.cn
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[1] YU Chun-sheng(余椿生). Food and Medicine(食品与药品), 2005, 7(3): 40. [2] LIU Chun-an, ZHANG Ming(刘春安, 彰 明). The Pharmacopoeia of Chinese Herbs for Anti-cancer(抗癌中草药大辞典), 1994. 462. [3] LUO Zhu-lan(罗珠兰). Journal of Practical Traditional Chinese Medicine(实用中医药杂志), 2002, 18(3): 28. [4] SHEN Lan(沈 岚). Journal of External Therapy of Traditional Chinese Medicine(中医外治杂志), 2002, 11(4): 45. [5] WANG Qi-jun(王启君). Lishizhen Medicine and Materia Medica Research(时珍国医国药), 2003, 14(5): 283. [6] XIANG Xing-hua(向兴华). China’s Naturopathy(中国民间疗法), 2004, 12(12): 13. [7] ZHOU Tang-heng(周堂恒). Hunan Journal of Traditional Chinese Medicine(湖南中医杂志), 2003, 19(5): 25. [8] ZHAN Xu-qing(詹绪清). Zhejiang Journal of Traditional Chinese Medicine(浙江中医杂志), 2005, 40(7): 316. [9] TANG Yi, YANG Wen-hua, SHI Zhe-xin, et al(汤 毅, 杨文华, 史哲新, 等). Chinese Traditional and Herbal Drugs(中草药), 2003, 34(12): 1125. [10] WANG Ji-hong(王继红). Modern Journal of Integrated Traditional Chinese and Western Medicine(现代中西医结合杂志), 2003, 12(15): 1662. [11] CHENG Ren-quan, CHENG Jian-ping, JIA Zheng-hong, et al(程仁权, 程建萍, 贾正红). Chinese Journal of Surgery of Integrated Traditional and Western Medicine (中国中西医结合外科杂志), 2002, 8(5): 360. [12] LIU Yu-qing, HONG Lan, WU Hong-mei, et al(刘玉清, 洪 澜, 吴宏美, 等). Journal of Tropical Medicine(热带医学杂志), 2003, 3(4): 484. [13] ZHANG Min, ZHANG Yong-qing(张 敏, 张永清). Shandong Medical Industry(山东医药工业), 2003, 22(1): 36. [14] ZHANG Pu-tong, XU Zai-sheng(张甫同, 许在生). Acta Academiae Medicinae Wannan(皖南医学院学报), 1990, 9(1): 1. [15] XIAO Wei, ZHAO Wei-cheng, YU De-quan(肖 伟, 赵维诚, 于德泉). Journal of Practical Oncology(实用肿瘤学杂志), 2000, 14(1): 18. [16] Xu C H, Sun S Q, Guo C Q, et al. Vibrational Spectroscopy, 2006, 41(1): 118. [17] Zhou Q, Sun S Q, Lin Z. Vibrational Spectroscopy, 2004, 36(2 SPEC. ISS.): 207. [18] Zhou Q, Sun S Q, Yu L, et al. Journal of Molecular Structure, 2006, 799(1-3): 77. [19] SUN Su-qin, ZHOU Qun, QIN Zhu(孙素琴, 周 群, 秦 竹). Atlas of Two-Dimensional Correlation Infrared Spectroscopy for Traditional Chinese Medicine Identification(中药二维相关红外光谱鉴定图集). Beijing: Chemical Industry Press(北京:化学工业出版社), 2003. 49. [20] SUN Su-qin, ZHOU Qun, CHEN Jian-bo(孙素琴, 周 群, 陈建波). Analysis of Traditional Chinese Medicine by Infrared Spectroscopy(中药红外光谱分析与鉴定). Beijing: Chemical Industry Press(北京: 化学工业出版社), 2010.
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