| 光谱学与光谱分析 |
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| Study on Crystalline and Properties of N’,N-Bis(n-butyl)-3,4,9,10-Perylene Tetracarboxylic Diimide |
| ZHANG Wen-guan, ZHAO Sheng-min |
| Beijing Area Major Laboratory of Printing Packaging Material and Technology, Beijing Institute of Graphic Communication, Beijing 102600, China |
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Abstract N’,N-Bis(n-butyl)-3,4,9,10-perylene tetracarboxylic diimide was synthesized , purified and crystallized, then IR, element analysis and X-ray diffraction were tested. The spectrum of UV-Vis absorption (maximum absorption peak at 524.80 nm), fluorescence emission (maximum emission intensity at 539.0 nm) and stokes displacement (15 nm) of the compound in DMF were analyzed. The UV-Vis absorption spectrum between 400 and 700 nm in a film can indicate that α-crystal has much stronger absorption peaks than β-crystal and that red shift of maximum absorption occurs (545 to 580 nm) when β-crystal is changed into α-crystal. It is obvious that CPS of α，β-crystal are respectively 2 508 at 26.0° and 1 891 at 25.2° in the X-ray diffraction pattern. The functional separate photoreceptors of α，β-crystal as charge generation material were made, and photoconductivity properties were tested after charging the sample and then using spectral light of 532 nm formed by a band path filter.
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Received: 2004-12-16
Accepted: 2005-03-18
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Corresponding Authors:
ZHANG Wen-guan
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| Cite this article: |
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ZHANG Wen-guan,ZHAO Sheng-min. Study on Crystalline and Properties of N’,N-Bis(n-butyl)-3,4,9,10-Perylene Tetracarboxylic Diimide [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(02): 302-305.
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https://www.gpxygpfx.com/EN/Y2006/V26/I02/302 |
[1] HUANG De-yin, DUAN Xue-hui, LAN Min-bo(黄德音，段学辉，蓝闽波). Photographic Materials(感光材料), 1996, (5): 3.
[2] ZHANG Wen-guan, ZHAO Sheng-min(张文官，赵生敏). Photographic Science and Photochemistry(感光科学与光化学)，2005，23(2)：88.
[3] Katsumi Nukada, Motoko Komatsu. United States Patent, 5, 395, 722., 1995-3-7.
[4] REN Sheng-wu，SHENG Min-bo(任绳武，盛闽波). Shanghai Dye(上海染料), 1991, (4): 12.
[5] YANG Lian-min, WANG Lei, LI Hui-ling, et al(杨联明，王 雷，李会玲，等). Information Recording Materials(信息纪录材料), 2003, 4(2): 3.
[6] LI Du-xin(李笃信). Photographic Materials(感光材料), 1998, (5): 6.
[7] 松岛朝夫，大柴 武雄，江藤 嘉彦. 特开平. 6 222597, 1994-8-12.
[8] LIU Dong-zi(刘东志). Dye Industry(染料工业), 1994, 31(1): 17-19 |
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