|
|
|
|
|
|
| Advances in Equipment for Deep Ultra-Violet Excimer Laser Ablation Coupled Plasma Mass and Optical Emission Spectrometry |
| GONG Ge-lian1, 2, YOU Li-bing3, LI Cong-ying4, FANG Xiao-dong3, SUN Wei-dong4, 5, 6 |
1. State Key Laboratory of Isotope Geochemistry, Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, China
2. CAS Center for Excellence in Deep Earth Science, Guangzhou 510640, China
3. Anhui Provincial Key Laboratory of Photonic Devices and Materials, Anhui Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Hefei 230031, China
4. Center of Deep Sea Research, Ocean Mega-Science Center, Institute of Oceanography, Chinese Academy of Sciences, Qingdao 266071, China
5. Laboratory for Marine Mineral Resources, Qingdao National Laboratory for Marine Science and Technology, Qingdao 266071, China
6. University of Chinese Academy of Sciences, Beijing 100094, China
|
|
|
|
|
Abstract The sample’s elemental and isotopic content information can be obtained by inductively coupled plasma mass and optical emission spectrometry analysis of excimer laser ablated products. Excimer laser ablation coupled mass and optical emission spectrometry are among the most important analytical techniques suitable for in situ microanalyses. Excimer laser ablation based sampling technique coupled with either ICP mass spectrometry or optical emission spectrometry techniques have witnessed widely applications in geology, materials science, environmental science, and even life science research. The combination of excimer laser ablation sampling technique and plasma analysis techniques fully demonstrates their respective advantages: the former’s in-situ sampling solid surface feature satisfying both the needs of evaluating elemental or isotopic concentration with high space-resolution and avoidance of polluted problem during sample pretreatment, furthermore, high-energy laser of pulse width ranging from nanosecond to femtosecond, low thermal effect resulting from ablation of solid sample surface and leading to less elemental or isotopic fractionation effects in laser ablation products which can fully represent the original elemental or isotopic information in analytes; either ICP mass spectrometry or optical emission spectrometry-based techniques have been applied successfully to investigate elemental or isotopic information in analytes, and the tandem of laser sampling technique with ICP mass technique have already produced various in-situ elemental and isotopic concentrations data in solid surface samples with high quality; simultaneously integrated ICP mass spectrometry with optical emission spectrometry has been recently proposed for chemical analysis in analyte, aiming at improve elemental and isotopic analysis accuracy and precision based on ICP mass and OES techniques. This paper introduces our instrumental construction solution of excimer laser ablation coupled with plasma mass and optical emission spectrometry analysis techniques, and the technical problems and key experimental verification of independent research and relevant developments have been summarized and prospected.
|
|
Received: 2020-12-24
Accepted: 2021-02-04
|
|
|
|
[1] Richard E Russo, Xianglei Mao, Jhhanis J Gonzalez, et al. Analytical Chemistry, 2013, 85(13): 6162.
[2] Richard E Russo, Xianglei Mao, Samuel Mao. Analytical Chemistry, 2002, 74(3): 70A.
[3] Zhang Bochao, He Miaohong, Hang Wei, et al. Analytical Chemistry, 2013, 85(9): 4507.
[4] Lazarov M, Horn I. Spectrochimica Acta Part B: Atomic Spectroscopy, 2015, 111: 64.
[5] Prasoon K Diwakar, Sivanandan S Harilal, Nicole L Lahaye, et al. Journal of Analytical Atomic Spectrometry, 2013, 28(9): 1420.
[6] Kuhn H R, Günther D. Journal of Analytical Atomic Spectrometry, 2004, 19(9): 1158.
[7] Lahaye N L, Harilal S S, Diwakar P K, et al. Journal of Applied Physics, 2013, 114(2): 023103.
[8] Nicole L Lahaye, Sivanandan S Harilal, Prasoon K Diwakar, et al. Journal of Analytical Atomic Spectrometry, 2013, 28(11): 1781.
[9] Koch J, Günther D. Applied Spectroscopy, 2011, 65(5): 155A.
[10] Masaki Ohata, Daniel Tabersky, Reto Glaus, et al. Journal of Analytical Atomic Spectrometry, 2014, 29(8): 1345.
[11] Kimura J I, Chang Q, Tani K. Geochemical Journal, 2011, 45(4): 283.
[12] Poitrasson F, François-Xavier d’Abzac. Journal of Analytical Atomic Spectrometry, 2017, 32: 1075.
[13] Horn I, Blanckenburg F V. Spectrochimica Acta Part B: Atomic Spectroscopy, 2007, 62(4): 410.
[14] Ohata M, Nonose N, Dorta L, et al. Analytical Sciences, 2015, 31(12): 1309.
[15] Garcia C C, Lindner H, Niemax K. Journal of Analytical Atomic Spectrometry, 2009, 24(1): 14.
[16] Deng Wenfeng, Liu Ying, Wei Gangjian, et al. Journal of Analytical Atomic Spectrometry, 2010, 25(1): 84.
[17] Gong Gelian, Sun Saijun, Zhou Jibin, et al. Journal of Analytical Atomic Spectrometry, 2017, 32: 2246.
|
| [1] |
TIAN Fu-chao1, CHEN Lei2*, PEI Huan2, BAI Jie-qi1, ZENG Wen2. Study of Factors Influencing the Length of Argon Plasma Jets at
Atmospheric Pressure With Needle Ring Electrodes[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3682-3689. |
| [2] |
LIU Hong-wei1, FU Liang2*, CHEN Lin3. Analysis of Heavy Metal Elements in Palm Oil Using MP-AES Based on Extraction Induced by Emulsion Breaking[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3111-3116. |
| [3] |
LIU Pan1, 2, 3, DU Mi-fang1*, LI Bin1, LI Jing-bin1, ZENG Lei1, LIU Guo-yuan1, ZHANG Xin-yao1, 4, ZHA Xiao-qin1, 4. Determination of Trace Tellurium Content in Aluminium Alloy by
Inductively Coupled Plasma-Atomic Emission Spectrometry Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3125-3131. |
| [4] |
ZHU Yu-qi1, 2, ZHANG Xin2, DU Pan-pan2, LIU Shu1, ZHANG Gui-xin1, 2, GUAN Song-lei2*, ZHENG Zhong1*. Infrared Spectroscopy and X-Ray Spectroscopy Combined With
Inductively Coupled Plasma Mass Spectrometry for Quality
Control of Mongolian Medicine Yu Grain Soil[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3163-3169. |
| [5] |
YANG Fan1, HAO Liu-cheng1, KE Wei2, LIU Qing1, WANG Jun1, CHEN Min-yuan2, YUAN Huan2*, YANG Ai-jun2, WANG Xiao-hua2, RONG Ming-zhe2. Research on Effect of Laser Incident Angle on Laser-Induced Plasma at Low Pressure[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2740-2746. |
| [6] |
ZHANG Zhi-fen1, LIU Zi-min1, QIN Rui1, LI Geng1, WEN Guang-rui1, HE Wei-feng2. Real-Time Detection of Protective Coating Damage During Laser Shock Peening Based on ReliefF Feature Weight Fusion[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2437-2445. |
| [7] |
LI Shi-lun1, LIU Tao2, SONG Wen-min3, WANG Tian-le2, LIU Wei1, CHEN Liang1, LI Zhi-gang2*, FENG Shang-shen1*. Study of Two-Dimensional Ordered Magnetic Co Nanosphere Array Film Construction and Its Optical Properties[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2037-2042. |
| [8] |
YAN Ming-liang1, ZHANG Chen-long2, ZHAO Lian-xiang3, ZHAO Hua-he4, GAO Xun2*. Spectral Characteristics of Ge Plasma Induced by Femtosecond Pulsed Laser Ablation[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2095-2098. |
| [9] |
YUAN Shu, WU Ding*, WU Hua-ce, LIU Jia-min, LÜ Yan, HAI Ran, LI Cong, FENG Chun-lei, DING Hong-bin. Study on the Temporal and Spatial Evolution of Optical Emission From the Laser Induced Multi-Component Plasma of Tungsten Carbide Copper Alloy in Vacuum[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(05): 1394-1400. |
| [10] |
LIN Jing-tao, XIN Chen-xing, LI Yan*. Spectral Characteristics of “Trapiche-Like Sapphire” From ChangLe, Shandong Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1199-1204. |
| [11] |
ZHANG Liang1, ZHANG Ran2, CUI Li-li3, LI Tao1, GU Da-yong4, HE Jian-an2*, ZHANG Si-xiang1*. Rapid Modification of Surface Plasmon Resonance Sensor Chip by
Graphene Oxide[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 795-800. |
| [12] |
YU Cheng-hao, YE Ji-fei*, ZHOU Wei-jing, CHANG Hao*, GUO Wei. Characteristics of the Plasma Plume and Micro-Impulse Generated by
Irradiating the Aluminum Target With a Nanosecond Laser Pulse at
Oblique Incidence[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 933-939. |
| [13] |
ZHENG Li-na1, 2, XUAN Peng1, HUANG Jing1, LI Jia-lin1. Development and Application of Spark-Induced Breakdown Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 665-673. |
| [14] |
LI Ru, YANG Xin, XING Qian-yun, ZHANG Yu. Emission Spectroscopy Study of Remote Ar Plasma[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(02): 394-400. |
| [15] |
LIAN Xiao-qin1, 2, CHEN Yan-ming1, 2, WANG Yu-qiao1, 2, LIU Yu1, 2. Research on ICP-AES Spectral Baseline Correction Method Based on DE Algorithm and NURBS Curve[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(01): 260-267. |
|
|
|
|
