| 光谱学与光谱分析 |
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| Simultaneous Resolution and Determination of Tyrosine, Tryptophan and Phenylalanine by Alternating Penalty Trilinear Decomposition Algorithm Coupled with 3D Emission-Excitation Matrix Fluorometry |
| XIAO Jin, REN Feng-lian*, SONG Ge, LIAO Lü, YU Wen-feng, ZENG Tao |
| College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, China |
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Abstract A new method using alternating penalty trilinear decomposition algorithm coupled with excitation-emission matrix fluorometry has been developed for simultaneous resolution and determination of tyrosine, phenylalanine and tryptophan. Their correlation coefficients were 0.9987, 0.9995and 0.9993 respectively. The contents of tyrosine, phenylalanine and tryptophan in Hibiscus syriacus L. leaves were also be determined by this method after being extracted by ultrasonic. The coefficients of variation and the recoveries of the three amino acids were 0.84%, 0.36%, 1.59% and 101.0%-92.7%, 106.5%-93.0%, 103.0%-95.0% respectively. All these show that this is a simple, fast and cridible method.
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Received: 2006-03-28
Accepted: 2006-06-28
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Corresponding Authors:
REN Feng-lian
E-mail: xj410001@yahoo.com.cn
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| Cite this article: |
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XIAO Jin,REN Feng-lian,SONG Ge, et al. Simultaneous Resolution and Determination of Tyrosine, Tryptophan and Phenylalanine by Alternating Penalty Trilinear Decomposition Algorithm Coupled with 3D Emission-Excitation Matrix Fluorometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(10): 2088-2092.
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| URL: |
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https://www.gpxygpfx.com/EN/Y2007/V27/I10/2088 |
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