| 光谱学与光谱分析 |
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| Analytical Performance of CID-ICP-AES for Alkaline-Earth Elements |
| XIN Ren-xuan |
| Institute of Nuclear Energy Technology, Tsinghua University, Beijing 100084, China |
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Abstract The plasma spectrometer composed of Charge Injection Device(CID) and echell grating has excellent analytical performance. In the present paper, analytical performance of CID-ICP-AES was studied for alkaline-earth elements. The results showed that the detection limits were 0.000 03 mg·L-1 for Ca, 0.000 2 mg·L-1 for Be, Sr and Ba, and 0.000 1 mg·L-1 for Mg. The self-absorption coefficient was less than 1 for all alkaline earth elements and 0.7-0.8 for Ca and Mg. The linear range of the determination was 104-105. The photometric precision was RSD＝1% when concentration was less than 1 mg·L-1.
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Received: 2002-12-18
Accepted: 2003-05-28
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Corresponding Authors:
XIN Ren-xuan
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[1] Sweedler T V, Bihon A B, Epperson P M et al. Anal. Chem.，1998, 60(4)：282，291A.
[2] ZHANG Zuo-yong, JIA Qiong, GUO Li-ping et al(张卓勇，贾 琼，郭黎平等).Spectroscopy and Spectral Analysis(光谱学与光谱分析)2001,21(2):230.
[3] XIN Ren-xuan，SONG Chong-li(辛仁轩，宋崇立). Chinese Journal of Analytical Chmistry(分析化学)，2000，28(8)：978.
[4] XIN Ren-xuan，ZHAO Yu-zhen，SHI Hong-jun(辛仁轩，赵玉珍，施洪钧). Chinese Journal of Analytical Chemistry(分析化学)，1998，26(1)：44.
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