光谱学与光谱分析 |
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Kinetic-Spectrophotometric Determination of Trace Manganese by IO-4-Tetrabase New System and the Mechanism |
LI Jian-guo, ZHANG Min, ZHAO Kang |
School of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215006, China |
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Abstract A new kinetic-spectrophotometric method for the determination of trace amounts of manganese(Ⅱ) has been proposed. The method is based on the manganese(Ⅱ) catalyzing the coloring reaction of tetrabase[4,4’-bis(dimethylamino)-diphenylmethane] oxidized by sodium periodate in HAc-NaAc(pH≈5.0) medium. The linear range of the determination of manganese is 0-4 μg·L-1, and the detection limit is 4.6×10-11 g·mL-1. The method is not only simple, rapid and with good sensitivity but also without heating. It has been used for the determination of trace amounts of manganese in water sample with satisfactory results. The mechanism of the reaction is discussed in detail.
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Received: 2002-09-26
Accepted: 2003-02-16
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Corresponding Authors:
LI Jian-guo
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Cite this article: |
LI Jian-guo,ZHANG Min,ZHAO Kang. Kinetic-Spectrophotometric Determination of Trace Manganese by IO-4-Tetrabase New System and the Mechanism [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(07): 870-872.
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URL: |
http://www.gpxygpfx.com/EN/Y2004/V24/I07/870 |
[1] LUO Qing-yao et al(罗庆尧等). Spectrophotometric Analysis(分光光度分析). Beijing:Science Press(北京:科学出版社), 1998. 274. [2] CHEN Guo-shu(陈国树). Catalytic Kinetic Analysis and Applications(催化动力学分析及其应用). Nanchang: Jiangxi College Press(南昌:江西高校出版社), 1991. 76. [3] Grases F. Anal. Chim. Acta, 1983, 155: 229. [4] ZHOU Hua-fang et al (周华方等). Chinese Chemistry Bulletin(化学通报), 1994, 4. 42. [5] CHEN Guo-shu(陈国树). Chinese J. Anal. Chem.(分析化学), 1987, 15(10): 920. [6] WU He-zhou et al(吴和舟等). Chinese J. Anal. Chem.(分析化学), 1996, 24(9): 1085. [7] JIA Xin-xin,QIN Yong-hui(贾欣欣,秦永惠). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1999, 19(3): 499. [8] LI Jian-guo et al (李建国等). Chinese J. Anal. Chem.(分析化学), 2003,31(7):812.
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