光谱学与光谱分析 |
|
|
|
|
|
Determination of Main Components in Nd-Fe-B Magnetic Materials by ICP-AES |
LIU Yong-ming |
College of Chemistry, Yantai University, Yantai 264005,China |
|
|
Abstract The method for direct determination of neodymium,iron and boron in Nd-Fe-B permanent magnetic materials by inductively coupled plasma-atomic emission spectroscopy (ICP-AES) was studied and suitable analytical lines were selected. The interference from matrix elements in samples was diminished by matrix matching method. The memory effect of the determination of boron by ICP-AES was discussed and was eliminated by way of detecting and subtracting blank value from testing result of samples frequently. The method was applied to the determination of Nd,Fe and B in Nd-Fe-B permanent magnetic materials samples with a precision of RSD 0.62%,0.56% and 0.90%,respectively.
|
Received: 2003-03-06
Accepted: 2003-08-28
|
|
Corresponding Authors:
LIU Yong-ming
|
|
[1] LI Fei(李 飞). Chinese Journal of Rare Earth(稀土),1999,20(2):63. [2] ZHAO Yu-zheng,Lü Pei-de(赵玉珍,吕佩德). Chinese Journal of Analysis Laboratory(分析试验室),1997,16(6):25. [3] SUN Zhen-hua,LI Bing,SUN Da-hai, ZHANG Zhi-gang, YING Hai, GU Sheng, WANG Xiao-ru(孙振华,李 冰,孙大海,张志刚,应 海,谷 胜,王小如). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2001,21(1):57. [4] WANG Chun-mei,ZHU Lian-qing,ZHANG Shu-zheng, Lü Qiong, WANG Jin-gang(王春梅,褚连青,张淑珍,吕 琼,王金钢). Chinese Journal of Rare Metal(稀有金属),1999,(2):159.
|
[1] |
LIAN Xiao-qin1, 2,LIU Yu1, 2,CHEN Yan-ming1, 2,HUANG Jing1, 2,GONG Yong-gang1, 2,HUO Liang-sheng1, 2. Research on Multi-Peak Spectral Line Separation Method Based on Adaptive Particle Swarm Optimization[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(05): 1452-1457. |
[2] |
ZHA Ling-yan1,2, ZHANG Yu-bin1,2, LI Zong-geng1,2, LIU Wen-ke1,2*. Effect of Continuous Red/Blue LED Light and Its Light Intensity on Growth and Mineral Elements Absorption of Lettuce[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(08): 2474-2480. |
[3] |
LIU Bing-bing, LIU Jia, ZHANG Chen-ling, HAN Mei, JIA Na, LIU Sheng-hua*. Preconcentration and Determination of Heavy Metals in Water Samples by Ion Exchange Resin Solid Phase Extraction with Inductively Coupled Plasma Atomic Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(12): 3917-3922. |
[4] |
TIAN Ying-gang, HU Qing-qing, XIE Ming-yong. Comparison of Mineral Element Contents in Silky Fowl and Non-Medicinal Chicken[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(11): 3563-3566. |
[5] |
LIU Jia, LIU Bing-bing, HAN Mei, JIA Na, ZHANG Chen-ling*. Methodology Research for Determination of Total Phosphorus in Water by Inductively Coupled Plasma-Atomic Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(06): 1880-1883. |
[6] |
CHEN Hua-zhou1, 2, XU Li-li3, CAI Ken4*, LIU Zhen-yao2, 5, CHEN An1, LIANG Yuan-yuan2. Performance Diagnosis of ICP-AES Combined with SVDV Technology for Quality Analysis of Drinking Water[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(05): 1558-1562. |
[7] |
ZHANG Wen-li1, 2, 3, LONG Ping1, 2, 3*, WU Jian1, 2, 3, CHEN Xiu-min1, 2, 3, XIONG Heng1, 2, 3, YANG Bin1, 2, 3. Determination of Sulfur in Solid and Solution of Phosphate Ore Pulp Flue Gas Desulfurization Agent with ICP-AES[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(05): 1535-1539. |
[8] |
QI Li-jie, WANG Ying*, MENG Qing-zhu, ZHAO Zhen . Study on the Element Composition of Ancient Fossils and Meteorites [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(01): 247-249. |
[9] |
XIAN Yi-heng1, LI Yan-xiang1, TAN Yu-chen1, WANG Wei-lin2, YANG Qi-huang2, CUI Jian-feng3 . Application of LA-ICP-AES to Distinguish the Different Turquoise Mines [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2016, 36(10): 3313-3319. |
[10] |
CAO Lei1, CHEN Wei-wei2, GAO Xiao-li1, LIAO Qi-lin1 . Research on the Matrix Interference on Major and Minor Elements in Soil Samples with ICP-AES [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2016, 36(07): 2260-2265. |
[11] |
CHEN Xi1, DU Peng1, GUAN Qing2, FENG Xu3, XU Dong-qun1*, LIN Shao-bin1* . Application of ICP-MS and ICP-AES for Studying on Source Apportionment of PM2.5 during Haze Weather in Urban Beijing[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(06): 1724-1729. |
[12] |
LIU Bing-bing, HAN Mei*, JIA Na, LIU Sheng-hua . Determination of SiO2 in Groundwater and Mineral Water by Inductively Coupled Plasma-Atomic Emission Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(05): 1388-1391. |
[13] |
QIN Wen-xia, GONG Qi*, LI Min, DENG Li-xin, MO Li-shu, LI Yan-lin . Determination of Arsenic in Food Package Aluminum by Ultrasound Assisted Solid Phase Extraction/ICP-AES[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(04): 1043-1047. |
[14] |
ZHAI Yu-xin1, CHEN Jun1, LI Ti1*, LIU Ji-yan2, WANG Xie-yi1, CHENG Chao1, LIU Cheng-mei1 . Determination of Mineral Elements in Choerospondias Axillaris and Its Extractives by ICP-AES [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(04): 1052-1055. |
[15] |
WANG Li-ping1, 2, FENG Hai-tao1, DONG Ya-ping1*, PENG Jiao-yu1, 2, LI Wu1, SHI Hai-qin3, WANG Yong4 . Standard Addition Determination of Impurities in Na2CrO4 by ICP-AES [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(02): 523-526. |
|
|
|
|