光谱学与光谱分析 |
|
|
|
|
|
Constant-Energy Synchronous Fluorescence Spectrometry for Simultaneous Determination of Anthracene and 9,10-Dimethylanthracene |
HE Li-fang1,2, LIN Dan-li1, LI Yao-qun1* |
1. Department of Chemistry, the MOE Key Laboratory of Analytical Sciences, Xiamen University, Xiamen 361005, China 2. Department of Chemistry, Longyan College, Longyan 364000, China |
|
|
Abstract A new method of constant-energy synchronous fluorimetry to determine anthracene and 9,10-dimethylanthracene simultaneously is suggested. The spectral resolution of the constant-energy synchronous fluorescence spectra of these two compounds was much higher than that of conventional spectra. The linear ranges for anthracene and 9,10-dimethylanthracene were 0-2 μg·mL-1 and 0-5 μg·mL-1 respectively. The detection limits of anthracene and 9,10-dimethylanthracene were 2.2 ng·mL-1 and 1.7 ng·mL-1 respectively,and the relative standard deviation was less than 2%. When the new method was used for the determination of anthracene and 9,10-dimethylanthracene in water samples, the recoveries were in the range of 85% to 103%. This method has proved to be simple and rapid.
|
Received: 2003-08-26
Accepted: 2004-02-11
|
|
Corresponding Authors:
LI Yao-qun
|
|
Cite this article: |
HE Li-fang,LIN Dan-li,LI Yao-qun. Constant-Energy Synchronous Fluorescence Spectrometry for Simultaneous Determination of Anthracene and 9,10-Dimethylanthracene [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(11): 1384-1387.
|
|
|
|
URL: |
http://www.gpxygpfx.com/EN/Y2004/V24/I11/1384 |
[1] Sorrell R. J. Chromatogr., 1997, 185: 655. [2] Dipak K. Enviromental Science & Technology. 1978, 12: 7. [3] Rubio S, Gomer-Hens A, Ualcarcel M. Talanta, 1986, 33: 633. [4] LI Yao-qun, HUANG Xian-zhi, CHEN Guozhen(李耀群,黄贤智,陈国珍). Chinese Science Bulletin(科学通报), 1991, 36(17): 1312. [5] LI Yao-qun, HUANG Xian-zhi(李耀群,黄贤智). Chinese J. Anal. Chem. (分析化学), 1989, 17: 1154. [6] LI Yao-qun, HUANG Xian-zhi(李耀群,黄贤智). Chinese J. Anal. Chem. (分析化学), 1990, 18(9) : 827. [7] HE Wen-qi, YAO Wei-xi, XIE Xue-peng(何文琪,姚渭溪,谢学鹏). Spectroscopy and Spectral Analysis (光谱学与光谱分析), 1996, 16(4): 100. [8] LI Yao-qun, SHI Ning, QIAN Fang(李耀群,时 宁,钱 方). Chem. J. Chinese Universities (高等学校化学学报), 1997, 18(4): 538. [9] Li Y Q, Huang X Z, Xu J G, Chen G Z. Anal. Chim. Acta, 1992, 256: 285. [10] Eiroa A A, Blanco E V, Machia P L. Analyst, 2000, 125(7): 1321. [11] Eiroa A A, Huckins S R, Blanco E V. Appl. Spectrosc., 2000, 54(10): 1534. [12] Eiroa A A, Blanco E V, Machia P L. Talanta, 2000, 51(4): 677.
|
[1] |
ZHU Xiang1, 2*, YUAN Chao-sheng1, CHENG Xue-rui1, LI Tao1, ZHOU Song1, ZHANG Xin1, DONG Xing-bang1, LIANG Yong-fu2, WANG Zheng2. Study on Performances of Transmitting Pressure and Measuring Pressure of [C4mim][BF4] by Using Spectroscopic Techniques[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1674-1678. |
[2] |
XU Lei, ZHU Lin, ZHANG Chun, YE Chang-qing*, CHEN Shuo-ran, LI Lin, LIANG Zuo-qin, WANG Xiao-mei*. Study on Properties of Azaanthracene Derivatives With Triplet-Triplet Annihilation Upconversion and One-Photon Hot Band Absorption
Upconversion[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1761-1768. |
[3] |
WANG Yi-ya1, WANG Yi-min1*, GAO Xin-hua2. The Evaluation of Literature and Its Metrological Statistics of X-Ray Fluorescence Spectrometry Analysis in China[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1329-1338. |
[4] |
YAN Ling-tong, LI Li, SUN He-yang, XU Qing, FENG Song-lin*. Spectrometric Investigation of Structure Hydroxyl in Traditional Ceramics[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1361-1365. |
[5] |
HAN Bing1, SUN Dan-dan2*, WAN Wei-hao1, WANG Hui3, DONG Cai-chang2, ZHAO Lei3, WANG Hai-zhou3*. Element Segregation of Cast-Rolled 7B05 Aluminum Alloy Based on
Microbeam X-Ray Fluorescence[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1413-1419. |
[6] |
YAN Peng-cheng1, 2, ZHANG Chao-yin2*, SUN Quan-sheng2, SHANG Song-hang2, YIN Ni-ni1, ZHANG Xiao-fei2. LIF Technology and ELM Algorithm Power Transformer Fault Diagnosis Research[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1459-1464. |
[7] |
ZHANG Yu-yang, CHEN Mei-hua*, YE Shuang, ZHENG Jin-yu. Research of Geographical Origin of Sapphire Based on Three-Dimensional Fluorescence Spectroscopy: A Case Study in Sri Lanka and Laos Sapphires[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1508-1513. |
[8] |
JIANG Xiao-yu1, 2, LI Fu-sheng2*, WANG Qing-ya1, 2, LUO Jie3, HAO Jun1, 2, XU Mu-qiang1, 2. Determination of Lead and Arsenic in Soil Samples by X Fluorescence Spectrum Combined With CARS Variables Screening Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1535-1540. |
[9] |
BAI Lu1, 2, XU Xiong1, LIU Quan-zhen1, 2, DU Yan-jun1, 2, 3, WANG Dong-hong1, 2*. Characterization and Analysis of Dissolved Organic Matter in Different
Types of Natural Water in Wuhan by Three-Dimensional
Fluorescence Spectra[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1642-1647. |
[10] |
LI Xiao-li1, GAO Xin-hua2, WANG Yi-min3*, DENG Sai-wen3, WANG Yi-ya3, LI Song3. Review on the Application of X-Ray Fluorescence Spectrometry in Halogen Elements Analysis in Geological Materials[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 997-1009. |
[11] |
ZHANG Zhao1, 2, 3, 4, YAO Zhi-feng1, 3, 4, WANG Peng1, 3, 4, SU Bao-feng1, 3, 4, LIU Bin3, 4, 5, SONG Huai-bo1, 3, 4, HE Dong-jian1, 3, 4*, XU Yan5, 6, 7, HU Jing-bo2. Early Detection of Plasmopara Viticola Infection in Grapevine Leaves Using Chlorophyll Fluorescence Imaging[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1028-1035. |
[12] |
OUYANG Zhou-xuan, MA Ying-jie, LI Dou-dou, LIU Yi. The Research of Polarized Energy Dispersive X-Ray Fluorescence for Measurement Trace Cadmium by Geant4 Simulation[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1064-1069. |
[13] |
ZHANG Rui1, 2, 3, TANG Xin-yi1, 2, ZHU Wen-qing1, 2, 3. Research on Shortwave Infrared Multispectral Fluorescence Imaging of Mouse Vein[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1109-1116. |
[14] |
NI Zi-yue1, CHENG Da-wei2, LIU Ming-bo2, YUE Yuan-bo2, HU Xue-qiang2, CHEN Yu2, LI Xiao-jia1, 2*. The Detection of Mercury in Solutions After Thermal Desorption-
Enrichment by Energy Dispersive X-Ray Fluorescence[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1117-1121. |
[15] |
ZHAO Yue2, MA Feng-xiang2, WANG An-jing1*, LI Da-cheng1, SONG Yu-mei2, WU Jun1, CUI Fang-xiao1, LI Yang-yu1, CAO Zhi-cheng1. Research on Electric Breakdown Fault Diagnosis Model of Transformer Insulated Oil Based on Fluorescent Double-Color Ratio[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1134-1138. |
|
|
|
|