光谱学与光谱分析 |
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Study on Different Proportion Formulas of Activating Blood Circulation by FTIR |
XU Mao-ling1,LI Hui-fen3,ZHOU Qun2,YIN Quan1,SUN Su-qin2*,WU Xian-zhong4 |
1. Tianjin University of Traditional Chinese Medicine,Tianjin 300193, China2. Department of Chemistry,Tsinghua University,Beijing 100084, China3. College of Pharmacy,Tianjin Medical University,Tianjin 300070, China4. Tianjin Nankai Hospital,Tianjin 300100, China |
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Abstract Fourier transform spectroscopy (FTIR) and two-dimensional correlation spectroscopy were used to analyze different compatibility forms of sargentgloryvine stem, radix paeoniae rubra and cortex moutan in order to study the FTIR spectra of different proportion formulas. The results indicate that different proportion formulas have distinct change regularity in FTIR spectra, second derivative spectra and synchronous 2D. Key components of sargentgloryvine stem’s characteristic absorption band are 1 610, 1 518 and 1 446 cm-1 which are characteristic absorption band of aromatic material, and in the original formula, that shows stronger peak than others, suggesting that original formula can make the best of composition of drug action. In the different proportion formulas, 1 614 cm-1 is nearer to 1 610 cm-1, which is sargentgloryvine stem’s characteristic absorption band, than to 1 706 cm-1, illustrating that sargentgloryvine stem is more influential formula than others. According to identification and ascription of characteristic absorption band, it was initially revealed that different proportion of drug dosage can affect pharmacodynamic action of integral formula.
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Received: 2009-03-12
Accepted: 2009-06-16
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Corresponding Authors:
SUN Su-qin
E-mail: sunsq@mail.tsinghua.edu.cn
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[1] WANG Yu-xin,LI Hui-fen,ZHOU Jing,et al(王宇歆, 李惠芬, 周 静, 等). Chinese Journal of Surgery of Integrated Traditional and Western Medicine(中国中西医结合外科杂志), 2008,14(4):410. [2] Noda I. Appl. Spectrosc., 1990,44:550. [3] Noda I. Appl. Spectrosc., 1993,47:1329. [4] Noda I, Dowrey A E, Marcott C, et al. Appl. Spectrosc., 2000,54:236A. [5] LI Y J. Journal of Chinese Medicinal Materials, 2002,25(9):669. [6] Noda I, Ozaki Y. Two-Dimensional Correlation Spectroscopy-Application in Vibrational and Optical Spectroscopy, Wiley, Chichester,2004. [7] NI S F, FU C, WU P. Chinese Wild Plant Resources, 2004,23(4):8. [8] Pharmacopeia Committee of Ministry of Health, the People’s Republic of China(中华人民共和国卫生部药典委员会编). Pharmacopoeia of the People’s Republic of China(中华人民共和国药典). Beijing: Chemical Industry Press(北京: 化学工业出版社), 2005. 15,134. [9] WU W, SUN S Q, ZHOU Q, et al. Journal of Pharmaceutical and Biomedical Analysis, 2008,46:498. [10] Noda I, Mol J. Struct., 2006,799:2. [11] Noda I. J. Am. Chem. Soc., 1989,111:8116. [12] ZHOU Q, SUN S Q, ZUO L. Vibrational Spectroscopy, 2004, 36(2):207.
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