| 光谱学与光谱分析 |
|
|
|
|
|
| Flow Injection Analysis of Ciprofloxacin by Terbium Sensitized Chemiluminescence Method |
| LIAN Ning1，2,WANG Jian-chao2,LENG Wen-hong3, CHANG Xi-jun1* |
1.Department of Chemistry and Chemical Engineering, Lanzhou University, Lanzhou 730000, China
2.Department of Chemistry, Qinghai Normal University, Xining 810008, China
3.Hospital of Qinghai Medical College, Xining 810001, China |
|
|
|
|
Abstract A new flow injection chemiluminescence (CL) method for the determination of Ciprofloxacin (CPLX) was described.The method was based on the weak CL reaction of Ce(Ⅳ)-SO2-3 sensitized by Tb3+-CPLX.The relative CL intensity was linear with the concentration of CPLX in the range of 9.0×10-9-1.0×10-6 mol·L-1.The detection limit is 2.2×10-11 mol·L-1.The relative standard deviation (RSD) for the determination of 5.0×10-8 mol·L-1 CPLX is 3.0% (n=11).The method has been successfully applied to the analysis of CPLX in tablet and capsule.An original mechanism was proposed to explain this phenomenon.
|
|
Received: 2004-02-02
Accepted: 2004-06-09
|
|
|
|
Corresponding Authors:
CHANG Xi-jun
|
|
| Cite this article: |
|
LIAN Ning,WANG Jian-chao,LENG Wen-hong, et al. Flow Injection Analysis of Ciprofloxacin by Terbium Sensitized Chemiluminescence Method [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(07): 1038-1041.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2005/V25/I07/1038 |
[1] Suchs Peter C.Am.J.Med., 1989, 87: 6.
[2] ZHANG Hua-an，ZHANG Qiu-xia，FENG Wei-yi(张华安，张秋霞，封卫毅).Chin.J.of Host.Pharm.(中国医院药学杂志), 1993, 13(3): 116.
[3] LIU Rui-ling, XU Jing-ren, LIU Yiu-gao(刘瑞玲，徐景仁，刘友皋).Chin.J.Pharm.Anal.(药物分析杂志), 1994, 14(1)： 45.
[4] Sultan S M, Suliman F E O.Analyst，1992, 117(9): 1523.[5] Rieutord A，Vazquez L.Anal.Chim.Acta.，1994, 290(1): 215.
[6] SHI Yao-guo, et al(施耀国，等).Chin.J.Antibiotics(中国抗生素杂志), 1993，18(3)： 206.
[7] Brkich G E, et al.Pharm.Chem.J., Volume Date，1999, 33(4): 219.
[8] Gau W, Ploschke H J, Schmidt K, Weber B.J.Liq.Chromatogr., 1985, 8(3): 485.
[9] WU Shu-qing, et al(吴淑清，等).Chinese J.of Anal.Chem.(分析化学), 2000，28(12)： 1462.
[10] YANG Jing-he, ZOU Hua-bin, JIE Nian-qin，GE Hong-mei(杨景和，邹华彬，揭念琴，葛红梅).Chem.J.Chinese Universities(高等学校化学学报), 1993, 14(3): 339.
[11] ZHANG Tie-li, ZHAO Hui-chun, JIN Lin-pei, et al.J.Photochem.Photobio.A，Chem., 1999, 121: 37.
[12] Paulls D A, Townshend A.Analyst, 1996, 121: 831.
[13] Veiopoulou C J, Ioannou P C, Lianidou E S.J.Pharm.Biomed.Anal., 1997, 15: 1839.
[14] WU Yue-ping, WANG Hao, HAO Yu-xia, XIE Ya-zhi(吴月萍, 王 浩, 郝玉霞, 谢亚芝).Chin.J.of Host.Pharm.(中国医院药学杂志), 1994, 14(1): 21.
[15] ZHANG Feng-qin, SONG Kun, LIN Fu-tian(张凤琴, 宋 坤, 林赴田).Chin.J.Antibiotics(中国抗生素杂志), 1991, 16(3): 203.
[16] LI Nian-bing, DUAN Jian-ping, CHEN Hong-qing, CHEN Guo-nan(李念兵，段建平，陈红青，陈国南).Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2004，24(1)： 15.
[17] WANG Yang, FAN Shi-hua(王 洋，范世华).Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2005，25(2)： 184.
|
| [1] |
YANG Jing1, LI Li1, LIANG Jian-dan1, HUANG Shan1, SU Wei1, WEI Ya-shu2, WEI Liang1*, XIAO Qi1*. Study on the Interaction Mechanism Between Thiosemicarbazide Aryl Ruthenium Complexes and Human Serum Albumin[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2761-2767. |
| [2] |
TANG Yan1, YANG Yun-fan1, HU Jian-bo1, 2, ZHANG Hang2, LIU Yong-gang3*, LIU Qiang-qiang4. Study on the Kinetic Process and Spectral Properties of the Binding of Warfarin to Human Serum Protein[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2099-2104. |
| [3] |
ZONG Zhi-fang1, XU Wei-cheng2, CHEN De-peng1*, TANG Gang1, ZHOU Xiao-hui1, DONG Wei1, WU Yu-xi2. Preparation Mechanism of Decylic Acid-Palmitic Acid/SiO2@TiO2
Photocatalytic Phase Change Microcapsules Based on
Multiple Spectrum Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1306-1313. |
| [4] |
REN Li-lei, PENG Yu-ling, WANG Shu-jun*, ZHANG Cheng-gen, CHEN Yu, WANG Xin-tong, MENG Xiao-ning. Fluorescence Spectroscopy for Studies on the Interaction Between Three Metalloporphyrins With Human Serum Albumin[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 806-813. |
| [5] |
ZHANG Bao-ping1, NING Tian1, ZHANG Fu-rong1, CHEN Yi-shen1, ZHANG Zhan-qin2, WANG Shuang1*. Study on Raman Spectral Characteristics of Breast Cancer Based on
Multivariable Spectral Data Analysis Methods[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(02): 426-434. |
| [6] |
LI Jin-zhi1, LIU Chang-jin1, 4*, SHE Zhi-yu2, ZHOU Biao2, XIE Zhi-yong2, ZHANG Jun-bing3, JIANG Shen-hua2, 4*. Antiglycation Activity on LDL of Clove Essential Oil and the Interaction of Its Most Abundant Component—Eugenol With Bovine Serum Albumin[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(01): 324-332. |
| [7] |
WANG Jun1, WANG Zhou-li2, CHENG Jing-jing1. Interaction Between Tartrazine and Bovine Serum Albumin Using Multispectral Method and Molecular Docking[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 904-909. |
| [8] |
XU Yang-biao, WANG Hai-shui*. The Removal of Water Peaks From IR Spectra of BSA Aqueous Solution by Two ATR Background Samples and Thermal Behavior of Proteins[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(02): 642-646. |
| [9] |
WANG Xiao-xia1,3*, WU Hao1, NIE Zhi-hua2, MA Li-tong1,3*, CUI Jin-long1, SAI Hua-zheng1, CHENG Jian-guo1. Study on the Interaction Between Fulvic Acid and Bovine Serum Albumin by Multispectral and Molecular Docking[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(09): 2904-2910. |
| [10] |
ZHANG Chuan-ying1, PENG Xin1*, RAO Heng-jun2, QI Wei2, SU Rong-xin2, HE Zhi-min2. Spectroscopic Studies on the Interaction Between Salvianolic Acid B and Bovine Serum Albumin[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(06): 1701-1707. |
| [11] |
TUO Xun1, SONG Ji-min1, FU Hao2, LÜ Xiao-lan1*. Study on Interaction Between Hexabromocyclododecane and Bovine Serum Albumin by Spectroscopy and Computer Simulation Methods[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(05): 1487-1492. |
| [12] |
HU Jing-jing, TONG Chang-lun*. Study on the Interaction Between Carbon Quantum Dots and Human Serum Albumin by Spectroscopic Methods[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(04): 1107-1113. |
| [13] |
ZHENG Pei-chao, ZHONG Chao, WANG Jin-mei*, LUO Yuan-jiang, LAI Chun-hong, WANG Xiao-fa, MAO Xue-feng. Evaluation of Flow Injection-Solution Cathode Glow Discharge With an Interference Filter Wheel for Spectral Discrimination[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 842-847. |
| [14] |
LI Xue1, WANG Li1, LIU Guang-xian1*, TU Zong-cai2. Effect of Urea on Glycosylation of BSA Based on Spectral Techniques[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(02): 478-483. |
| [15] |
FU Xing-hu, ZHAO Fei, WANG Zhen-xing, LU Xin, FU Guang-wei, JIN Wa, BI Wei-hong. Quantitative Analysis of Goat Serum Protein Content by Raman Spectroscopy Based on IABC-SVR[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(02): 540-545. |
|
|
|
|
