| 光谱学与光谱分析 |
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| Synthesis of 4-(Benzeneazo) Salicyladelhyde Hydrazones and Study on Their Spectral Properties |
| WU Bo-wan,ZHANG Bing,YU Xin-qiao,LIU Jian-ning |
| Department of Chemistry, Longdong University, Qingyang 745000, China |
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Abstract 4-(benzeneazo) salicyladelhyde was synthesized with aniline and salicylaldehyde. Benzoylhydrazine and p-hydroxybenzoylhydrazine were synthesized using the reaction of ethyl benzoate and methyl p-hydraxy benzoate with hydrazine hydrate. Four novel 4-(benzeneazo) salicyladelhyde hydrazones were synthesized using the reaction of 4-(benzeneazo) salicyladelhyde with benzoylhydrazine, p-hydroxybenzoylhydrazine, phenylhydrazine, and isonicotinyl hydrazine respectively. IR, UV and the fluorescence spectrum of 4-(benzeneazo) salicyladelhyde hydrazones were studied.
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Received: 2004-10-15
Accepted: 2005-01-16
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Corresponding Authors:
WU Bo-wan
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| Cite this article: |
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WU Bo-wan,ZHANG Bing,YU Xin-qiao, et al. Synthesis of 4-(Benzeneazo) Salicyladelhyde Hydrazones and Study on Their Spectral Properties [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(01): 106-108.
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| URL: |
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https://www.gpxygpfx.com/EN/Y2006/V26/I01/106 |
[1] JIANG Chong-qiu, TANG Bo, WANG Rong-ying, et al. Talanta, 1997, 44: 197.
[2] JIANG Chong-qiu, TANG Bo, WANG Chen, et al. Analyst, 1996，121(3): 317.
[3] JIANG Chong-qiu, WANG Jing-zheng, XU Xiu-fang, et al(江崇球, 王敬政, 许秀芳，等). Chinese J. Anal. Chem.(分析化学), 1998, 26(2): 129.
[4] JIANG Chong-qiu, TANG Bo, FU Hong-yan, et al(江崇球, 唐 波, 傅红燕，等). Chem. J. of Chinese Universities(高等学校化学学报), 1996, 17(1): 49.
[5] LIU Jian-ning, ZHANG Bing, SHANG Hong, et al(刘建宁, 张 兵, 尚 虹, 等). Chinese Journal of Health Laboratory Technology(中国卫生检验杂志), 2002, 12(2): 147.
[6] LIU Jian-ning, ZHANG Bing, SHANG Hong, et al(刘建宁, 张 兵, 尚 虹, 等). Chinese J. Anal. Chem.(分析化学), 2003, 31(5): 636.
[7] WANG Shao-ling, LU Wen-guan, LIU Hong-wen, et al(王少玲, 卢文贯, 刘宏文, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2003, 23(1): 54.
[8] LIU Jian-ning, ZHANG Bing, WU Bo-wan, et al(刘建宁, 张 兵, 仵博万, 等). Chemical Reagents(化学试剂), 2002, 24(5): 294.
[9] NING Yong-cheng(宁永成). Structural Identification of Organic Compounds and Organic Spectroscopy(有机化合物结构鉴定与有机波谱学). Beijing: Science Press(北京：科学出版社), 2001. 322.
[10] CHEN Guo-zhen, HUANG Xian-zhi, ZHENG Zhu-zi, XU Jin-gou, WANG Zun-ben(陈国珍, 黄贤智, 郑朱梓，许金钩, 王尊本). Fluorescence Analysis Method(荧光分析法). Beijing: Science Press(北京：科学出版社), 1990. 31.
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