| 光谱学与光谱分析 |
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| Determination and Comparison of Metal Elements in Huai Radix Rehmanniae at Different Grades by ICP-MS |
| WANG Guo-qing1, WEI Li-fang1, DONG Chun-hong2, FU De-xue2, SUN Yu-an1, HOU Xiao-jie1 |
1. Key Lab of Surface & Interface Science of Henan Province, Zhengzhou University of Light Industry, Zhengzhou 450002, China
2. Research Center for Huai Chinese Medicines, Jiaozuo University, Jiaozuo 454003, China |
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Abstract The Huai radix rehmanniae at different grades was pretreated by wet digestion, and then the metal elements in the radix rehmanniae and the prepared sample by steaming method were determined using ICP-MS. The results indicate that there is no obvious difference in the metal elements between the different grades and between the dried radix rehmanniae and its corresponding prepared product. There are elements Zn, Cu, Cr, Fe, Mn, Sn, Ni, Mo, Go, etc. in radix rehmanniae, among which the contents of Ca，Fe，Al，Zn and Cu are higher; the metal elements beneficial to human body in dried radix rehmanniae are relative lower than that in the prepared one. The elements such as Co, Ni, Cr, Mn, etc. in radix rehmanniae have poison effects on human body when their contents are more than a certain threshold value, although they are human essential elements. Element Pb is harmful to human body, which should be controlled and reduced/eliminated in the processing procedure. The determination and comparison of the metal elements in radix rehmanniae at different grades can provide useful information about the comprehensive evaluation of dried radix rehmanniae and their prepared products.
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Received: 2008-11-06
Accepted: 2009-02-08
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Corresponding Authors:
WANG Guo-qing
E-mail: gqwang@zzuli.edu.cn
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[1] NI Mu-yun，BIAN Bao-lin(倪慕云，边宝林). China Journal of Chinese Materia Medica(中国中药杂志), 1989, 14(7): 41.
[2] NI Mu-yun，BIAN Bao-lin(倪慕云，边宝林). Bulletin of Chinese Materia Medica(中药通报)，1988，13(4): 18.
[3] LIU Wen-sheng, LUO Wei-zao, ZHANG Zhi-rong, et al(刘文胜，罗维早，张志荣，等). West China Journal of Pharmaceutical Sciences(华西药学杂志), 2001, 16(4): 293.
[4] WANG Fu-li, LUO Yue-e, LIU Bin(王富丽, 罗跃娥, 刘 斌). Lishizhen Medicine and Maieria Medical Research(时珍国医国药)，2004, 15(7): 68.
[5] LI Geng-sheng, YU Zhen, WANG Hui-sen(李更生，于 震，王慧森). International Journal of Traditional Chinese Medicine(国外医学：中医中药分册)，2004, 26 (2): 74.
[6] ZHAO Jun, JIN Ri-guang, LUO Lu(赵 军, 金日光, 罗 璐). Journal of Beijing University of Chemical Technology(Natural Science Edition)(北京化工大学学报·自然科学版), 2007, 34(5): 467.
[7] SHI Yan-zhi, WANG Yan-ze, WANG Ying-feng, et al(施燕支, 王艳泽, 王英锋, 等). Chinese Journal of Analytical Laboratory(分析试验室), 2007, 26(3): 47.
[8] FANG Fu-yong, MIAO Yan-li, SONG Wen-dong(方富永, 苗艳丽, 宋文东). Food Science and Technology(食品科技), 2007, (2): 218.
[9] LEI Lian-di, OUYANG Li, LIU Ya-qiong, et al(雷连娣, 欧阳荔, 刘雅琼, 等). China Journal of Chinese Materia Medica(中国中药杂志), 2008, 33(3): 32.
[10] SHAO You-yan, CAI Bi-shuang, LIN Ji-yun, et al(邵幼岩, 蔡碧双, 林纪昀, 等). China Journal of Chinese Materia Medica(中国中药杂志), 2007, 32(19): 57.
[11] WEN Hui-min, HUO Yan-shuang, ZHANG Yuan-yuan, et al(温慧敏, 霍艳霜, 张园园, 等). Journal of Shenyang Pharmaceutical University(沈阳药科大学学报), 2007, 24(12): 40.
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