| 光谱学与光谱分析 |
|
|
|
|
|
| Fluorescence Spectra of Bletilla Striata Aqueous Extraction |
| SHI Xun-li,WEI Yong-ju*,ZHANG Ying-hua, WANG Ya-min, LIU Cui-ge |
| College of Chemistry and Material Science, Hebei Normal University, Shijiazhuang 050016, China |
|
|
|
|
Abstract Three-dimensional fluorescence spectrum and ultraviolet absorption spectrum of Bletilla striata extraction drawn by boiling water were reported. Three fluorescence peaks, located at λex/λem＝227/299 nm, 271/299 nm and 258/ 389 nm respectively, were observed in the three-dimensional fluorescence spectrum. Among them, the two former peaks having the same emission wavelengths were produced by one fluorescent component, while the latter peak was produced by another. Three-dimensional fluorescence spectrum is a characteristic mark of Bletilla striata, therefore it can be used in qualitative identification. The distance between emission wavelengths of the two components was 90 nm, so the fluorescence intensity of two components couuld be measured separately without pre-separation. For dilute solutions of Bletilla striata aqueous extraction, good linear relationships between fluorescence intensity and concentration of two components were obtained, thereby the quantitative determination of the two components may be carried out. In the range of pH 1.5 to pH 12.5, the fluorescence intensity of the two components changes with the increase in pH, indicating dissociable protons exist in the molecular structure of the two components.
|
|
Received: 2005-12-12
Accepted: 2006-03-28
|
|
|
|
Corresponding Authors:
WEI Yong-ju
E-mail: weiyju@heinfo.net
|
|
| Cite this article: |
|
SHI Xun-li,WEI Yong-ju,ZHANG Ying-hua, et al. Fluorescence Spectra of Bletilla Striata Aqueous Extraction[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(04): 769-772.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2007/V27/I04/769 |
[1] LUO Xin-gen, LIU Wen-yong, ZHANG Wei-dong, et al(罗新根，刘文庸，张卫东，等). The Journal of Pharmaceutical Practice(药学实践杂志), 1999, 17(6): 359.
[2] Shuzo T, Masae Y, Keiko I. Phytochemistry, 1983, 22(4): 1011.
[3] Masae Y, Li B, Keiko I, et al. Phytochemistry, 1990, 29(7): 2285.
[4] HAN Guang-xuan, WANG Li-xin, GU Zheng-bing, et al(韩广轩，王立新，顾正兵，等). Acta Pharmaceutica Sinica(药学学报), 2002, 37(3): 194.
[5] WANG Li-xin, HAN Guang-xuan, SHU Ying, et al(王立新，韩广轩，舒 莹，等). China Journal of Chinese Materia Medica(中国中药杂志), 2001, 26(10): 690.
[6] HAN Guang-xuan, WANG Li-xin, WANG Mai-li, et al(韩广轩，王立新，王麦莉，等). The Journal of Pharmaceutical Practice (药学实践杂志), 2001, 19(6): 360.
[7] HAN Guang-xuan, WANG Li-xin, ZHANG Wei-dong, et al(韩广轩，王立新，张卫东，等). Acad. J. Sec. Mil. Med. Univ.(第二军医大学学报), 2002, 23(9): 1029.
[8] XU Mu-gen, ZHU Shan-yin(徐木根，朱山寅). China Pharmaceuticals(中国药业), 2013, 12(7): 60.
[9] LI Ji, ZHANG Li-xin, ZHOU Shi-yu(李 及，张立新，周世玉). Journal of Chengdu University of Tradlitional Chinese Medicine(成都中医药大学学报), 2005, 28(2): 57.
[10] WEI Yong-ju, LI Na, QIN Shen-jun(魏永巨，李 娜，秦身钧). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2004, 24(6): 647.
[11] LIU Cui-ge, XU Yi-Zhuang, WEI Yong-ju, et al(刘翠格，徐怡庄，魏永巨，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2005, 25(4): 584.
[12] LIU Cui-ge, XU Yi-Zhuang, WEI Yong-ju, et al(刘翠格，徐怡庄，魏永巨，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2005, 25(9): 1446.
|
| [1] |
LEI Hong-jun1, YANG Guang1, PAN Hong-wei1*, WANG Yi-fei1, YI Jun2, WANG Ke-ke2, WANG Guo-hao2, TONG Wen-bin1, SHI Li-li1. Influence of Hydrochemical Ions on Three-Dimensional Fluorescence
Spectrum of Dissolved Organic Matter in the Water Environment
and the Proposed Classification Pretreatment Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 134-140. |
| [2] |
GU Yi-lu1, 2，PEI Jing-cheng1, 2*，ZHANG Yu-hui1, 2，YIN Xi-yan1, 2，YU Min-da1, 2, LAI Xiao-jing1, 2. Gemological and Spectral Characterization of Yellowish Green Apatite From Mexico[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 181-187. |
| [3] |
SONG Yi-ming1, 2, SHEN Jian1, 2, LIU Chuan-yang1, 2, XIONG Qiu-ran1, 2, CHENG Cheng1, 2, CHAI Yi-di2, WANG Shi-feng2，WU Jing1, 2*. Fluorescence Quantum Yield and Fluorescence Lifetime of Indole, 3-Methylindole and L-Tryptophan[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3758-3762. |
| [4] |
YANG Ke-li1, 2, PENG Jiao-yu1, 2, DONG Ya-ping1, 2*, LIU Xin1, 2, LI Wu1, 3, LIU Hai-ning1, 3. Spectroscopic Characterization of Dissolved Organic Matter Isolated From Solar Pond[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3775-3780. |
| [5] |
XUE Fang-jia, YU Jie*, YIN Hang, XIA Qi-yu, SHI Jie-gen, HOU Di-bo, HUANG Ping-jie, ZHANG Guang-xin. A Time Series Double Threshold Method for Pollution Events Detection in Drinking Water Using Three-Dimensional Fluorescence Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3081-3088. |
| [6] |
JIA Yu-ge1, YANG Ming-xing1, 2*, YOU Bo-ya1, YU Ke-ye1. Gemological and Spectroscopic Identification Characteristics of Frozen Jelly-Filled Turquoise and Its Raw Material[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2974-2982. |
| [7] |
YANG Xin1, 2, XIA Min1, 2, YE Yin1, 2*, WANG Jing1, 2. Spatiotemporal Distribution Characteristics of Dissolved Organic Matter Spectrum in the Agricultural Watershed of Dianbu River[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2983-2988. |
| [8] |
ZHU Yan-ping1, CUI Chuan-jin1*, CHENG Peng-fei1, 2, PAN Jin-yan1, SU Hao1, 2, ZHANG Yi1. Measurement of Oil Pollutants by Three-Dimensional Fluorescence
Spectroscopy Combined With BP Neural Network and SWATLD[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2467-2475. |
| [9] |
QIU Cun-pu1, 2, TANG Xiao-xue2, WEN Xi-xian4, MA Xin-ling2, 3, XIA Ming-ming2, 3, LI Zhong-pei2, 3, WU Meng2, 3, LI Gui-long2, 3, LIU Kai2, 3, LIU Kai-li4, LIU Ming2, 3*. Effects of Calcium Salts on the Decomposition Process of Straw and the Characteristics of Three-Dimensional Excitation-Emission Matrices of the Dissolved Organic Matter in Decomposition Products[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2301-2307. |
| [10] |
SHI Chuan-qi1, LI Yan2, HU Yu3, YU Shao-peng1*, JIN Liang2, CHEN Mei-ru1. Fluorescence Spectral Characteristics of Soil Dissolved Organic Matter in the River Wetland of Northern Cold Region, China[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(05): 1517-1523. |
| [11] |
LI Yuan-jing1, 2, CHEN Cai-yun-fei1, 2, LI Li-ping1, 2*. Spectroscopy Study of γ-Ray Irradiated Gray Akoya Pearls[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1056-1062. |
| [12] |
LIU Xia-yan1, CAO Hao-xuan1, MIAO Chuang-he1, LI Li-jun2, ZHOU Hu1, LÜ Yi-zhong1*. Three-Dimensional Fluorescence Spectra of Dissolved Organic Matter in Fluvo-Aquic Soil Profile Under Long-Term Composting Treatment[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(03): 674-684. |
| [13] |
LÜ Yang1, PEI Jing-cheng1*, ZHANG Yu-yang2. Chemical Composition and Spectra Characteristics of Hydrothermal Synthetic Sapphire[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(11): 3546-3551. |
| [14] |
ZHANG Yong-bin1, ZHU Dan-dan1, CHEN Ying1*, LIU Zhe1, DUAN Wei-liang1, LI Shao-hua2. Wavelength Selection Method of Algal Fluorescence Spectrum Based on Convex Point Extraction From Feature Region[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3031-3038. |
| [15] |
PAN Hong-wei, TONG Wen-bin, LEI Hong-jun*, YANG Guang, SHI Li-li. Spectral Analysis of the Effect of Organic Fertilizer Application on the
Evolution of Organic Matter and Nitrogen in Farmaland[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3116-3123. |
|
|
|
|
