| 光谱学与光谱分析 |
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| Analysis of the Adsorption Properties of Lead Ion onto Natural Sand Particles by Flame Atomic Absorption Spectrometry |
| Shawket Abliz, Abderyim Sopahun, Ismayil Nurulla* |
| College of Chemistry and Engineering, Xinjiang University, Urumqi 830046, China |
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Abstract The present research was aimed at the study of adsorption properties of lead ion on natural sand particle (NSP) by FAAS and at the development of NSP as an adsorbent used in the removal and preconcentration of lead(Ⅱ) ion in aqueous solution by adsorption. Particle structure and size distribution, surface morphology, specific surface area, functional radical of NSP and adsorption properties of lead ion onto NSP and factors which affect the adsorption capacity were analyzed using FTIR, SEM, NSA and FAAS. The adsorption condition such as acidity of solution, flow rate and time etc were optimized. The 5.0 cm×5 mm i.d. separation column was prepared by filling with the NSP as adsorbent. The experimental results showed that under the optimal adsorption conditions, such as the procedure was carried out at room temperature, pH of solution was 6, the flow rate was 2.55 mL·min-1, the maximum adsorption of Pb(Ⅱ) onto NSP as adsorbent was 24.9 mg·g-1. Adsorption rate was 91.5%. Specific surface area and pore size were 7.60 m2·g-1 and 3.91 nm respectively. Using 0.10 mol·L-1 chloride acid for desorption of Pb(Ⅱ), the desorption rate reached 99%. At the same time the adsorption mechanism of Pb(Ⅱ) was studied.
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Received: 2011-02-01
Accepted: 2011-06-20
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Corresponding Authors:
Ismayil Nurulla
E-mail: ismayilnu@sohu.com
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[1] Shuman L M. Soil Sci. Soc. Am., 1976, 40(3): 349.
[2] Shuman L M. Soil Sci. Soc. Am., 1977, 41(4): 703.
[3] Oliver B G. viron. Sci. Technol., 1973, 7(2): 135.
[4] SUN Wei-ling, NI Jin-ren(孙卫玲，倪晋仁). J. Sediment Reseach(泥沙研究)，2002, 6: 53.
[5] LI Li-min, GUO Yi-qun, HU Qing(李利民，郭益群，胡 清). Research of Environmental Sciences(环境科学研究)，1994, 7(5): 13.
[6] Zhou Aimin, Tang Hongxiao, Wang Dongsheng. Water Research, 2005, 39: 1245.
[7] Dali-Youcel N, Ouddane B, Derriche Z. Journal of Hazardous Materials, A, 2006, 137: 1263.
[8] Bajracharya K, Barry D A, Vigneswaran S. Water Quality Hydrology, Vol. 3. Kluwer Academic Publishers, The Netherlands, 1996. 19.
[9] LUO Shi-di, LIU Zhi-rong, CHEN Xiao-song, et al(罗世地，刘峙嵘，陈小松，等). Uranium Mining and Metallurgy(铀矿冶)，2008, 27(5): 92.
[10] Solener M, Tunali S, Ozcan A S, et al. Desalination, 2008, 223: 308.
[11] Madejova J. Vib. Spectroscopy, 2003, 31(1): 10. |
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