| 光谱学与光谱分析 |
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| Determination of Thirteen Metal Elements in the Plant Foeniculum Vulgare Mill. by Flame Atomic Absorption Spectrophotometry |
| XUE Guo-qing1, LIU Qing2, HAN Yu-qi1, WEI Hui-guang1, DONG Ting1 |
1. Department of Chemistry, Key Laboratory of Resources and Environment Chemistry of West China, Hexi University, Zhangye 734000, China
2. The 4th Geoteam of the Gansu Non-Ferrous Geoexploration Bureau, Zhangye 734012, China |
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Abstract The objective of the paper is to determine the amount of metal elements of Na, K, Mg, Ca, Cu, Zn, Mn, Fe, Co, Ni, Cd, Cr and Pb in the planted Foeniculum vulgare Mill. by flame atomic absorption spectrophotometry(FAAS), after the cinefaction and the digestion with HNO3-HClO4(φ 4∶1) at 90-95 ℃ and normal pressure. The optimum parameters of FAAS and the effects of solution medium on the results were investigated. The analytical results show that the amount of Na, K, Mg, Ca, Mn, Fe, Cu, Zn and Pb was 1 508.7, 27 653.0, 2 036.0, 4 848.1, 24.8, 323.5, 15.2, 23.7 and 10.8 μg·g-1,respectively, and that of Co, Ni, Cd and Cr was not checked out in the samples. The recovery of standard addition is 97.45%-102.50%, the relative standard deviation(n=9) was 0.34%-2.77%. The characteristic method is quick, simple and convenient and the results are satisfactory.
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Received: 2005-06-06
Accepted: 2005-09-28
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Corresponding Authors:
XUE Guo-qing
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| Cite this article: |
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XUE Guo-qing,LIU Qing,HAN Yu-qi, et al. Determination of Thirteen Metal Elements in the Plant Foeniculum Vulgare Mill. by Flame Atomic Absorption Spectrophotometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(10): 1935-1938.
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| URL: |
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https://www.gpxygpfx.com/EN/Y2006/V26/I10/1935 |
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