光谱学与光谱分析 |
|
|
|
|
|
Determination of Pb and Cd in Environmental Water Sample by On-Line Mini-Column Preconcentration and Flow Injection-Flame Atomic Absorption Spectrometry |
WANG Ai-xia, GUO Li-ping, WU Dong-mei |
Analysis and Testing Center, Northeast Normal University, Changchun 130024, China |
|
|
Abstract Trace Pb and Cd in environmental water samples were preconcentrted and determined by on-line mini-column field sampling and flow injection-flame atomic absorption spectrometry(FI-FAAS), and the adsorption materials of the column were activated carbon loaded 8-HQ,DDTC and APDC. Satisfactory results of the determination of Pb and Cd in the certified reference materials(trace elements in water GBW 08608) and the South lake water were obtained by using the above method. The detection limit of 10 mL enrichment of Pb and Cd was 1.58 and 0.062 μg·L-1, respectively, and the relative standard deviation of Pb and Cd was 1.62% and 1.96% respectively.
|
Received: 2005-03-18
Accepted: 2005-06-28
|
|
Corresponding Authors:
WANG Ai-xia
|
|
Cite this article: |
WANG Ai-xia,GUO Li-ping,WU Dong-mei. Determination of Pb and Cd in Environmental Water Sample by On-Line Mini-Column Preconcentration and Flow Injection-Flame Atomic Absorption Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(07): 1345-1348.
|
|
|
|
URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I07/1345 |
[1] QIU Hai-ou, ZHENG Hong-tao, TANG Zhi-yong(邱海鸥, 郑洪涛, 汤志勇). Analytical Laboratory(分析实验室), 2003, 22(1): 101. [2] YUAN Dong-xing, et al(袁东星, 等). Journal of Instrumental Analysis(分析测试通报),1992,11(6):90. [3] CHEN Shu-yu, SUN Mei(陈树榆, 孙 梅). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2001, 21(3): 377. [4] Yebra-Biurrun M C, Moreno-Cid A, Puig L. Analytica Chimica Acta 2004, 524: 73. [5] Yebra M C, Carro N, Moreno-Cid A. Spectrometry Acta Part B, 2002, 57: 85. [6] Yebra M C,Garcia A,Carro N. Talanta, 2002, 56: 777. [7] YU Ti-fang(余体芳). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1997,17(6): 118. [8] Giacomellia Maria B O, Ganzarollib Edgard M, Curtiusb Adilson J. Spectrochimica Acta Part B,2000 ,55:525. [9] Cerutti S, Silva M F, Gasquez J A, et al. Spectrochimica Acta Part B, 2003, 58:43. |
[1] |
YI Min-na1, 2, 3, CAO Hui-min1, 2, 3*, LI Shuang-na-si1, 2, 3, ZHANG Zhu-shan-ying1, 2, 3, ZHU Chun-nan1, 2, 3. A Novel Dual Emission Carbon Point Ratio Fluorescent Probe for Rapid Detection of Lead Ions[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3788-3793. |
[2] |
AN Bai-song1, 2, WANG Xue-mei1, 2*, HUANG Xiao-yu1, 2, KAWUQIATI Bai-shan1, 2. Hyperspectral Estimation of Soil Lead Content Based on Random Frog Band Selection Algorithm[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3302-3309. |
[3] |
CHAI Lin-lin, Areyi Mulati, Shawket Abliz*. Analysis the Adsorption Behaviors of Acetic Acid Modified Sand Grains for Lead Ions by Atomic Absorption Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2775-2778. |
[4] |
CHENG Fang-beibei1, 2, GAN Ting-ting1, 3*, ZHAO Nan-jing1, 4*, YIN Gao-fang1, WANG Ying1, 3, FAN Meng-xi4. Rapid Detection of Heavy Metal Lead in Water Based on Enrichment by Chlorella Pyrenoidosa Combined With X-Ray Fluorescence Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2500-2506. |
[5] |
ZHANG Chao1*, SU Xiao-yu1, XIA Tian2, YANG Ke-ming3, FENG Fei-sheng4. Monitoring the Degree of Pollution in Different Varieties of Maize Under Copper and Lead Stress[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1268-1274. |
[6] |
LAI Si-han1, LIU Yan-song1, 2, 3*, LI Cheng-lin1, WANG Di1, HE Xing-hui1, LIU Qi1, SHEN Qian4. Study on Hyperspectral Inversion of Rare-Dispersed Element Cadmium Content in Lead-Zinc Ores[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1275-1281. |
[7] |
ZHU Gui-jun, WANG Gan-zhen, PENG Jun*, TIAN Zong-ping, HOU Zhi-hua. The Mineralogical and Spectroscopic Characteristics of Phosphohedyphane From Chenzhou of Hunan Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3017-3023. |
[8] |
HUANG Xiao-juan1, 2, YAN Jing1, ZHANG Yang-li-zheng1, WANG Li-qin2*, XU Wei-hong1. Technological Analysis of the Chess Pieces of Liubo Uncovered From the Warring States Tomb in Shaanxi Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3187-3192. |
[9] |
WANG Ruo-su1, SUN Feng1, 2*, XIAN Yi-heng1. Study on the Composition and Weathered Layer of a Silicate Bead
Excavated From Ma-Jia-Yuan Cemetery M21[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3193-3197. |
[10] |
HOU Ya-ru, LU Ji-long*, FAN Yu-chao, Abudusalamu·KADIER, TANG Xiao-dan, WEI Qiao-qiao, GUO Jin-ke, ZHAO Wei. Uncertainty Evaluation and Method Improvement of Determination of Copper, Lead, and Zinc in Rocks by Atomic Absorption Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(07): 2101-2106. |
[11] |
FAN Chun-hui1, 2, ZHENG Jin-huan3, LIU Hong-xin1. FTIR, 2D-IR and XPS Analyses on the Mechanism of Protoplast Derived From Calendula Officinalis in Response to Lead and Cadmium in Soil[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1420-1425. |
[12] |
FAN Chun-hui1,2, ZHENG Jin-huan3, WANG Yu-fei3, SU Zhe3, LIN Long-jian3, YANG Chen3. Adsorption of Cadmium on Fe-Mn Nodules Derived From Soil by Spectral Methods[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(02): 616-621. |
[13] |
LUO Wei, TIAN Peng, DONG Wen-tao, HUANG Yi-feng, LIU Xue-mei, ZHAN Bai-shao, ZHANG Hai-liang*. Detection of Pb Contents in Soil Using LIBS Coupled With Univariate Calibration Curve Methods[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 886-891. |
[14] |
ZHANG Xin-bo1, CONG Long-zhuang1, YANG Lan-lan1, DU Zhong-lin1, WANG Yao1, WANG Yan-xin1, HUANG Lin-jun1, GAO Fan1, Laurence A. Belfiore2, TANG Jian-guo1*. Optimal Fluorescence Property of CdSe Quantum Dots and Electrospinning Polyvinylpyrrolidone Hybrid Microfibers[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 990-996. |
[15] |
LIU Qun-wei, SHAO Yong-ni, CHEN Xiao-wan, JIANG Lin-hua*. Study on the Changes of Material in Scenedesmus Obliquus Based on Fourier Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(12): 3890-3894. |
|
|
|
|