| 光谱学与光谱分析 |
|
|
|
|
|
| Determination of Trace Elements in Niuhuang Jiedu Tablets by Microwave Digestion and ICP-AES |
| ZHENG Yong-jun, ZHAO Bin, YOU Jin-mao |
| College of Chemistry, Qufu Normal University, Qufu 273165, China |
|
|
|
|
Abstract Niuhuang Jiedu tablets were digested with HNO3-H２O２ system by microwave digestion. The fourteen trace elements of As, Ca, Mg, Al, Mn, Sr, Ba, Se, Ni, Cd, Cu, Zn, Mo and Pb in the solution were determined by ICP-AES. The ICP-AES result proved to be reliable by adding standard recovery experiment to the process. By comparison with the result of chemical experiment, thr present method was accurate, quickly-accessible, and convenient. It was used for Niuhuang Jiedu tablets with result satisfactory.
|
|
Received: 2005-04-08
Accepted: 2005-07-16
|
|
|
|
Corresponding Authors:
ZHENG Yong-jun
|
|
| Cite this article: |
|
ZHENG Yong-jun,ZHAO Bin,YOU Jin-mao. Determination of Trace Elements in Niuhuang Jiedu Tablets by Microwave Digestion and ICP-AES [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(06): 1155-1157.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2006/V26/I06/1155 |
[1] MENG Xian-shu, CHEN Fa-kui(孟宪纾，陈发奎). Chinese Traditional Patent Medicine Analysis(中成药分析). Beijing: The People Hygiene Press(北京: 人民卫生出版社)，1990. 237.
[2] CHEN Li-na, WU Li-lan(陈丽娜，吴丽兰). China Journal of Chinese Material Medicine(中国中药杂志)，2002，27(4)：315.
[3] LIU Yan-ming(刘彦明). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2000，20(3)：373.
[4] ZHANG Qi-feng, PENG Shan-shan, LI Li, et al(张奇凤, 彭珊珊, 李 丽, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，1999，19(3)：392.
[5] XING Xiao-mei, MEI Jian-ming(邢晓梅, 梅建鸣). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2003，23(5)：995.
[6] Charles B Boss, Kenneth J Fredeen. Concepts Instrmentation and Techniques in Inductively Coupled Plasma Optical Emission Spectrometry, Norwalk: The Perkin-Elmer Corporation, 1999. 36.
|
| [1] |
HE Yan1, TAO Ran1, YANG Ming-xing1, 2*. The Spectral and Technology Studies of Faience Beads Unearthed in Hubei Province During Warring States Period[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3700-3709. |
| [2] |
WANG Wei-en. Analysis of Trace Elements in Ophiocordyceps Sinensis From
Different Habitats[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3247-3251. |
| [3] |
WANG Yan1, HUANG Yi1, 2*, YANG Fan1, 2*, WU Zhong-wei2, 3, GUAN Yao4, XUE Fei1. The Origin and Geochemical Characteristics of the Hydrothermal Sediments From the 49.2°E—50.5°E Hydrothermal Fields of the Southwest Indian Ocean Ultra-Slow Spreading Ridge[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2868-2875. |
| [4] |
CHEN Chao-yang1, 2, LIU Cui-hong1, 2, LI Zhi-bin3, Andy Hsitien Shen1, 2*. Alexandrite Effect Origin of Gem Grade Diaspore[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2557-2562. |
| [5] |
CHEN Di, SONG Chen, SONG Shan-shan, ZHANG Zhi-jie*, ZHANG Hai-yan. The Dating of 9 Batches of Authentic Os Draconis and the Correlation
Between the Age Range and the Ingredients[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(06): 1900-1904. |
| [6] |
HE Yan1, SU Yue1, YANG Ming-xing1, 2*. Study on Spectroscopy and Locality Characteristics of the Nephrites in Yutian, Xinjiang[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(12): 3851-3857. |
| [7] |
CHEN Xiao-li1, WANG Li-chun1, LI You-li1, GUO Wen-zhong1, 2*. Effects of Alternating Light Spectrum on the Mineral Element Level of Lettuce[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(09): 2813-2817. |
| [8] |
LIAN Xiao-qin1, 2，LIU Yu1, 2，CHEN Yan-ming1, 2，HUANG Jing1, 2，GONG Yong-gang1, 2，HUO Liang-sheng1, 2. Research on Multi-Peak Spectral Line Separation Method Based on Adaptive Particle Swarm Optimization[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(05): 1452-1457. |
| [9] |
CHEN Chao-yang1，HUANG Wei-zhi1，SHAO Tian1，LI Zhi-bin2，Andy Hsitien Shen1*. Characteristics of Visible Spectrum of Apatite With Alexandrite Effect[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(05): 1483-1486. |
| [10] |
LIU Yan-de, GAO Xue, JIANG Xiao-gang, GAO Hai-gen, LIN Xiao-dong, ZHANG Yu, ZHENG Yi-lei. Detection of Anthracnose in Camellia Oleifera Based on Laser-Induced Breakdown Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(09): 2815-2820. |
| [11] |
LU Xiao-ke1, LI Wei-dong1, LI Xin-wei2. Spectroscopic Analysis of Relics Unearthed from Xipo Site[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(04): 1186-1194. |
| [12] |
ZHA Ling-yan1,2, ZHANG Yu-bin1,2, LI Zong-geng1,2, LIU Wen-ke1,2*. Effect of Continuous Red/Blue LED Light and Its Light Intensity on Growth and Mineral Elements Absorption of Lettuce[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(08): 2474-2480. |
| [13] |
LIANG Piao-piao1, ZHOU Shan-shan1, XING Yun-xin1, LIU Ying1, 2*. Quantification of Trace Elements in Hair Samples from 156 Women Living in the Low-Selenium Region of Inner Mongolia by ICP-AES and AFS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(07): 2217-2222. |
| [14] |
HAO Xiao-jian*, TANG Hui-juan, HU Xiao-tao. Detection Sensitivity Improvement Study of LIBS by Combining Au-Nanoparticles and Magnetic Field[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(05): 1599-1603. |
| [15] |
LIU Bing-bing, LIU Jia, ZHANG Chen-ling, HAN Mei, JIA Na, LIU Sheng-hua*. Preconcentration and Determination of Heavy Metals in Water Samples by Ion Exchange Resin Solid Phase Extraction with Inductively Coupled Plasma Atomic Emission Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(12): 3917-3922. |
|
|
|
|
