| 光谱学与光谱分析 |
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| Determination of Trace Elements in Hollyhock by Microwave Digestion-FAAS |
| LI Yin-ping1, GAO Li2, LI Jin1, ZHOU Xiao-ying3,LIU Cong1* |
1. Chemical Department of College of Life and Science, Xinjiang Normal University, Urumqi 830054, China
2. College of Basic Medicine, Xinjiang Medical University, Urumqi 830011, China
3. College of Pharmacy, Xinjiang Medical University, Urumqi 830011, China |
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Abstract Hollyhock powder was digested by microwave digestion before determination.The eight trace elements, Fe, Cu, Zn, Mn，K，Ni，Ca and Mg, in hollyhock were determined by microwave FAAS. Standard curves method was used for the determination. The samples were digested with HNO3. The conditions of digestion were optimized. The effect of different microwave digestion conditions on the analysis results was reviewed, and the optimal condition for using atomic absorption spectrophotometry was determined. The experiments indicated that the content of trace elements of human needs, Mg, Ca, Fe, K etc. are highly enriched, the content of Mn and Zn is middling, and the content of Cu and Ni is low. The method is highly sensitive, convenient and speedy. The recovery (n=6) is 92.25%-110.50%, and the RSDs (n=6) are lower than 5%. The results are satisfactory.
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Received: 2008-10-22
Accepted: 2009-01-26
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Corresponding Authors:
LIU Cong
E-mail: Lyp-0522@xjnu.edu.cn
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[1] LIU Yong-min(刘勇民). Pharmcography of Uigur(维吾尔药志). Urumqi：Xinjiang People’s Publishing House(乌鲁木齐：新疆人民出版社), 1999. 880.
[2] ZHOU Xiao-ying, SU Zhi(周晓英，粟 智). Journal of Xinjiang Normal University(Natural Sciences Edition)(新疆师范大学学报·自然版), 2007, 21(3): 31.
[3] LONG Pei-xia, WANG Dong, MENG Xian-sheng，et al(龙沛霞, 王 东, 孟宪生, 等). Studies of Trace Elements and Health(微量元素与健康研究), 1997, 14(1): 59.
[4] YING Chun, SU Du, XIAO Tian-mei, et al(迎 春, 苏 都, 肖田梅, 等). Science of Guangdong Trace Elements(广东微量元素科学), 2008, 15(2): 67.
[5] SUN Chun-xiang(孙春香). Journal of Changshu Institute of Technology(常熟理工学院学报), 2007, 21(2): 53.
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