| 光谱学与光谱分析 |
|
|
|
|
|
| CAIS Correction for Blood Matrix Effect on Determination of Lead Concentration and Isotope Ratio by ICP-MS |
| ZENG Jing1,WANG Xiao-yan1, 2,LIU Hu-sheng1,DUN Zhe3,ZHAI Lei3,WANG Jing-yu1, 2* |
1. School of Public Health, Peking University, Beijing 100083, China
2. Laboratory of Biometallomics, Center of Medical & Health Analysis, Peking University, Beijing 100083, China
3. Haidian District of Beijing Centers for Disease Prevention and Control, Beijing, 100037, China |
|
|
|
|
Abstract The research studied the influence of matrix effect on the determination of lead concentration and isotope ratio through simulating blood matrix, and its correction by common analyte internal standardization (CAIS) method. The experiment results showed that CAIS method was suitable for the multi-element-matrix. The relative errors between the determined and the true concentration values are 20%(without correction), 8%(by conventional internal reference correction) and 2% (by CAIS correction), respectively. Otherwise, the influence of matrix effect and its correction for isotope ratio determination are not that obvious. Similarity of the mass number and properties between internal reference and analyte elements seems not important for CAIS correction, since very close correction results were obtained by using Tl and Dy as internal reference elements. Besides, correction results are not affected by different matrix dilution. Reliability and practicality of CAIS were proved by bovine blood standard material determination.
|
|
Received: 2005-11-16
Accepted: 2006-05-26
|
|
|
|
Corresponding Authors:
WANG Jing-yu
E-mail: wjy@bjmu.edu.cn
|
|
| Cite this article: |
|
ZENG Jing,WANG Xiao-yan,LIU Hu-sheng, et al. CAIS Correction for Blood Matrix Effect on Determination of Lead Concentration and Isotope Ratio by ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(02): 374-377.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2007/V27/I02/374 |
[1] Scott Clark, Joann Grote. Environmental Research, 2004, 96: 196.
[2] Roberto H Gwiazda, Donald R Smith. Environmental Health Perspectives, 2003, 108(11): 1091.
[3] Robert Kurkjian, A Russell Flegal. Environmental Research, 2003, 93: 308.
[4] Ians Begley, Barry L Sharp. Journal of Analytical Atomic Spectrometry, 1997, 12: 395.
[5] Assad S Al-Ammar, Ramon M Barnes. Spectrochimica Acta, Part B, 1999, 54: 1849.
[6] Assad S Al-Ammar, Ramon M Barnes. Journal of Analytical Atomic Spectrometry, 2001, 16: 327.
[7] XIE Ming-yong, NIE Shao-ping, FU Bo-qiang, et al(谢明勇，聂少平，傅博强，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2006，26(9)：1710.
|
| [1] |
YI Min-na1, 2, 3, CAO Hui-min1, 2, 3*, LI Shuang-na-si1, 2, 3, ZHANG Zhu-shan-ying1, 2, 3, ZHU Chun-nan1, 2, 3. A Novel Dual Emission Carbon Point Ratio Fluorescent Probe for Rapid Detection of Lead Ions[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3788-3793. |
| [2] |
AN Bai-song1, 2, WANG Xue-mei1, 2*, HUANG Xiao-yu1, 2, KAWUQIATI Bai-shan1, 2. Hyperspectral Estimation of Soil Lead Content Based on Random Frog Band Selection Algorithm[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3302-3309. |
| [3] |
CHAI Lin-lin, Areyi Mulati, Shawket Abliz*. Analysis the Adsorption Behaviors of Acetic Acid Modified Sand Grains for Lead Ions by Atomic Absorption Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2775-2778. |
| [4] |
CHENG Fang-beibei1, 2, GAN Ting-ting1, 3*, ZHAO Nan-jing1, 4*, YIN Gao-fang1, WANG Ying1, 3, FAN Meng-xi4. Rapid Detection of Heavy Metal Lead in Water Based on Enrichment by Chlorella Pyrenoidosa Combined With X-Ray Fluorescence Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2500-2506. |
| [5] |
ZHANG Chao1*, SU Xiao-yu1, XIA Tian2, YANG Ke-ming3, FENG Fei-sheng4. Monitoring the Degree of Pollution in Different Varieties of Maize Under Copper and Lead Stress[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1268-1274. |
| [6] |
LAI Si-han1, LIU Yan-song1, 2, 3*, LI Cheng-lin1, WANG Di1, HE Xing-hui1, LIU Qi1, SHEN Qian4. Study on Hyperspectral Inversion of Rare-Dispersed Element Cadmium Content in Lead-Zinc Ores[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1275-1281. |
| [7] |
ZHU Gui-jun, WANG Gan-zhen, PENG Jun*, TIAN Zong-ping, HOU Zhi-hua. The Mineralogical and Spectroscopic Characteristics of Phosphohedyphane From Chenzhou of Hunan Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3017-3023. |
| [8] |
HUANG Xiao-juan1, 2, YAN Jing1, ZHANG Yang-li-zheng1, WANG Li-qin2*, XU Wei-hong1. Technological Analysis of the Chess Pieces of Liubo Uncovered From the Warring States Tomb in Shaanxi Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3187-3192. |
| [9] |
WANG Ruo-su1, SUN Feng1, 2*, XIAN Yi-heng1. Study on the Composition and Weathered Layer of a Silicate Bead
Excavated From Ma-Jia-Yuan Cemetery M21[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3193-3197. |
| [10] |
HOU Ya-ru, LU Ji-long*, FAN Yu-chao, Abudusalamu·KADIER, TANG Xiao-dan, WEI Qiao-qiao, GUO Jin-ke, ZHAO Wei. Uncertainty Evaluation and Method Improvement of Determination of Copper, Lead, and Zinc in Rocks by Atomic Absorption Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(07): 2101-2106. |
| [11] |
GUO Jin-ke, LU Ji-long, SI Jun-shi, ZHAO Wei, LIU Yang, WANG Tian-xin, LAI Ya-wen*. Study on Heavy Metal in Soil by Portable X-Ray Fluorescence
Spectrometry Based on Matrix Effect Correction and
Correspondence Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(07): 2309-2314. |
| [12] |
FAN Chun-hui1, 2, ZHENG Jin-huan3, LIU Hong-xin1. FTIR, 2D-IR and XPS Analyses on the Mechanism of Protoplast Derived From Calendula Officinalis in Response to Lead and Cadmium in Soil[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1420-1425. |
| [13] |
LUO Wei, TIAN Peng, DONG Wen-tao, HUANG Yi-feng, LIU Xue-mei, ZHAN Bai-shao, ZHANG Hai-liang*. Detection of Pb Contents in Soil Using LIBS Coupled With Univariate Calibration Curve Methods[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 886-891. |
| [14] |
LIU Qun-wei, SHAO Yong-ni, CHEN Xiao-wan, JIANG Lin-hua*. Study on the Changes of Material in Scenedesmus Obliquus Based on Fourier Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(12): 3890-3894. |
| [15] |
LI Chao1, 2, LI Bin2, 3*, ZHANG Li-qiong2, YE Da-peng1*, ZHENG Shu-he1. Terahertz Spectrum Inversion Modeling of Lead Content in Different pH Soils[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(08): 2397-2402. |
|
|
|
|
