| 光谱学与光谱分析 |
|
|
|
|
|
| Preparation of Lomefloxacin-Tb3+ Nanoparticles Modified by PVP via Microwave-Assistance and Its Properties of Fluorescence |
| HE Hua1,2,YE Hai-ying1,LIU Xuhui3 |
1. Division of Analytical Chemistry，China Pharmaceutical University，Nanjing 210009, China
2. Key Laboratory of Drug Quality Control and Pharmacovigilance, China Pharmaceutical University, Ministry of Education，Nanjing 210009, China
3. Unite de Recherche INSERM 602，GroupeHospitalier Paul Brousse，12 Avenue Paul Vaillant Couturier，94807 Villejuif Cedex France |
|
|
|
|
Abstract Polyvinylpyrrolidone(PVP)-modified LFLX-Tb3+ nanoparticles were prepared by microwave radiation method. The obtained products were characterized by means of SEM, FTIR and fluorescence spectra. The surface-modified LFLX-Tb3+ nanoparticles showed a narrow size distribution and enhanced luminescence property compared with that of the unmodified ones. These results were attibuted to the surface passivation of the LFLX-Tb3+ nanoparticles by the PVP molecules. It is confirmed that the addition dosage of PVP is an important factor in the preparation of the LFLX-Tb3+ nanoparticles. The reasons for luminescence enhancement were discussed.
|
|
Received: 2006-04-04
Accepted: 2006-08-02
|
|
|
|
Corresponding Authors:
HE Hua
E-mail: dochehua@163.com
|
|
| Cite this article: |
|
HE Hua,YE Hai-ying,LIU Xuhui. Preparation of Lomefloxacin-Tb3+ Nanoparticles Modified by PVP via Microwave-Assistance and Its Properties of Fluorescence [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(06): 1164-1167.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2007/V27/I06/1164 |
[1] Grisaru H, Palchik O, Gedanken A, et al. Inorg. Chem., 2003, 42(22): 7148.
[2] Shanmugasundaram M, Manikandan S, Raghunathan R. Tetrahedron, 2002, 58(5): 997.
[3] Masaaki T, Koichiro O, Seijiro M. Tetrahedron Letters, 2003, 44(51): 9201.
[4] Sudhir K, Tulsi M. Chem. Phys. Lett., 2003, 370: 83.
[5] Sun Y, Gates B, Mayers B, et al. Nano. Lett., 2002, 2: 165.
[6] Kopeikin V V, Valueva S V, Kipper A I. Polymer Science Series A, 2003, 45: 374.
[7] Chandler Robin R, Coffer L. J. Phys. Chem., 1993, 97: 9767.
[8] Qian X F，Yin J，Fang S. J. Mater. Char., 2001，11: 2504.
[9] Sooklal K, Harms L H，Ploehn H J, et al. Adv. Mater., 1998，10: 1083.
[10] HE Hua，YE Hai-ying，DAI Li，et al (何 华，叶海英 , 戴 丽, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2006，26(3)：480.
[11] Rosendo A, Hores M, Aroyo R. Materials Lett., 2003, 57: 2885.
[12] QI Xue-yong，HE Hua，GU Fei，et al(戚雪勇，何 华，顾 飞，等). Chin. Pharm. J.(中国药学杂志)，2005，40(19): 1500.
[13] HE Hua，WANG Ling-li，LIU Xu-hui，et al(何 华，王羚郦，刘旭辉，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2006，26(8): 1516.
[14] Rieutord A, Prognon P, Brion F, et al. Analyst，1997，122：59R. |
| [1] |
LEI Hong-jun1, YANG Guang1, PAN Hong-wei1*, WANG Yi-fei1, YI Jun2, WANG Ke-ke2, WANG Guo-hao2, TONG Wen-bin1, SHI Li-li1. Influence of Hydrochemical Ions on Three-Dimensional Fluorescence
Spectrum of Dissolved Organic Matter in the Water Environment
and the Proposed Classification Pretreatment Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 134-140. |
| [2] |
XIA Ming-ming1, 2, LIU Jia3, WU Meng1, 2, FAN Jian-bo1, 2, LIU Xiao-li1, 2, CHEN Ling1, 2, MA Xin-ling1, 2, LI Zhong-pei1, 2, LIU Ming1, 2*. Three Dimensional Fluorescence Characteristics of Soluble Organic Matter From Different Straw Decomposition Products Treated With Calcium Containing Additives[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 118-124. |
| [3] |
GU Yi-lu1, 2，PEI Jing-cheng1, 2*，ZHANG Yu-hui1, 2，YIN Xi-yan1, 2，YU Min-da1, 2, LAI Xiao-jing1, 2. Gemological and Spectral Characterization of Yellowish Green Apatite From Mexico[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 181-187. |
| [4] |
HAN Xue1, 2, LIU Hai1, 2, LIU Jia-wei3, WU Ming-kai1, 2*. Rapid Identification of Inorganic Elements in Understory Soils in
Different Regions of Guizhou Province by X-Ray
Fluorescence Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 225-229. |
| [5] |
LIU Wei1, 2, ZHANG Peng-yu1, 2, WU Na1, 2. The Spectroscopic Analysis of Corrosion Products on Gold-Painted Copper-Based Bodhisattva (Guanyin) in Half Lotus Position From National Museum of China[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3832-3839. |
| [6] |
WANG Hong-jian1, YU Hai-ye1, GAO Shan-yun1, LI Jin-quan1, LIU Guo-hong1, YU Yue1, LI Xiao-kai1, ZHANG Lei1, ZHANG Xin1, LU Ri-feng2, SUI Yuan-yuan1*. A Model for Predicting Early Spot Disease of Maize Based on Fluorescence Spectral Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3710-3718. |
| [7] |
CHENG Hui-zhu1, 2, YANG Wan-qi1, 2, LI Fu-sheng1, 2*, MA Qian1, 2, ZHAO Yan-chun1, 2. Genetic Algorithm Optimized BP Neural Network for Quantitative
Analysis of Soil Heavy Metals in XRF[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3742-3746. |
| [8] |
SONG Yi-ming1, 2, SHEN Jian1, 2, LIU Chuan-yang1, 2, XIONG Qiu-ran1, 2, CHENG Cheng1, 2, CHAI Yi-di2, WANG Shi-feng2，WU Jing1, 2*. Fluorescence Quantum Yield and Fluorescence Lifetime of Indole, 3-Methylindole and L-Tryptophan[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3758-3762. |
| [9] |
WANG Zhi-qiang1, CHENG Yan-xin1, ZHANG Rui-ting1, MA Lin1, GAO Peng1, LIN Ke1, 2*. Rapid Detection and Analysis of Chinese Liquor Quality by Raman
Spectroscopy Combined With Fluorescence Background[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3770-3774. |
| [10] |
YI Min-na1, 2, 3, CAO Hui-min1, 2, 3*, LI Shuang-na-si1, 2, 3, ZHANG Zhu-shan-ying1, 2, 3, ZHU Chun-nan1, 2, 3. A Novel Dual Emission Carbon Point Ratio Fluorescent Probe for Rapid Detection of Lead Ions[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3788-3793. |
| [11] |
YANG Ke-li1, 2, PENG Jiao-yu1, 2, DONG Ya-ping1, 2*, LIU Xin1, 2, LI Wu1, 3, LIU Hai-ning1, 3. Spectroscopic Characterization of Dissolved Organic Matter Isolated From Solar Pond[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3775-3780. |
| [12] |
QI Guo-min1, TONG Shi-qian1, LIN Xu-cong1, 2*. Specific Identification of Microcystin-LR by Aptamer-Functionalized Magnetic Nanoprobe With Laser-Induced Fluorescence[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3813-3819. |
| [13] |
HE Yan-ping, WANG Xin, LI Hao-yang, LI Dong, CHEN Jin-quan, XU Jian-hua*. Room Temperature Synthesis of Polychromatic Tunable Luminescent Carbon Dots and Its Application in Sensitive Detection of Hemoglobin[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3365-3371. |
| [14] |
LIN Hong-jian1, ZHAI Juan1*, LAI Wan-chang1, ZENG Chen-hao1, 2, ZHAO Zi-qi1, SHI Jie1, ZHOU Jin-ge1. Determination of Mn, Co, Ni in Ternary Cathode Materials With
Homologous Correction EDXRF Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3436-3444. |
| [15] |
LI Xiao-li1, WANG Yi-min2*, DENG Sai-wen2, WANG Yi-ya2, LI Song2, BAI Jin-feng1. Application of X-Ray Fluorescence Spectrometry in Geological and
Mineral Analysis for 60 Years[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 2989-2998. |
|
|
|
|
