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Determination of Parameters of X-Ray Source Based on Tapered Glass Monocapillary X-Ray Condenser |
WANG Ya-bing1,2, SHAO Shang-kun1,2, SUN Xue-peng1,2, ZHANG Xiao-yun1,2, LI Hui-quan1,2, SUN Tian-xi1,2* |
1. Laboratory of Beam Technology of Ministry of Education, College of Nuclear Science and Technology, Beijing Normal University, Beijing 100875, China
2. China Beijing Radiation Center, Beijing 100875, China |
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Abstract The focal spot size and depth of the X-ray source are crucial parameters for X-ray spectroscopy, especially for micro X-ray diffraction and micro X-ray fluorescence. Determining these parameters efficiently and accurately is important for the application and development of the X-ray source. The existing methods for determining these paraments of X-ray source all have their limitations, especially for determining the micro focal spot X-ray source. The tapered glass monocapillary X-ray condenser (TGMXC) is a common X-ray focusing device. According to the filter property and the geometrical characteristics of the TGMXC, the conclusion that the energy upper limit of the focused X-ray of the TGMXC is affected by the focal spot size of the X-ray source can be obtained. The relation between the energy upper limit of the focused X-ray of the TGMXC andthe focal spot size of the X-ray source, and the distance between the TGMXC and the focal spot of the X-ray source was proposed. A method of determining parameters of the X-ray source based on TGMXC was designed. Measuring and determining the parameters of the TGMXC and placed the TGMXC in front of the measured X-ray source to form a focusing X-ray path. In the case that the focusing X-ray path is collimated and ensures that only the single reflected focused X-rays, TGMXC is detected, though changing the distance between the X-ray source and the TGMXC and using the energy spectrum detection system to obtain the corresponding focused X-ray energy spectrums. Though calculating and analyzing the energy spectrums, the maximum energy of each spectrum, namely the energy upper limit, is obtained. The focal spot size and the focal depth can be obtained simultaneously using the above relation and linear fitting. Parameters of a micro focal spot X-ray source with a Mo target were determined by this method. The manufacturer gave the focal spot size and focal depth as about 60 μm and 20 mm and were obtained by this method as 60.1 μm and 19.7 mm, respectively. The conventional pinhole imaging method was also used to determine this X-ray source, and the results were 60.3 μm and 20.1 mm, respectively. Compared with existing methods, this method can determining the micro focal spot X-ray source and has potential practical value and development for determining the high-energy X-ray source.
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Received: 2020-08-16
Accepted: 2020-12-29
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Corresponding Authors:
SUN Tian-xi
E-mail: stxbeijing@163.com
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[1] Bjeoumikhov A, et al. Review of Scientific Instruments,2005,76(6): 63115.
[2] Bjeoumikhov A, et al. Applied Physics Letters,2005,86(14):144102.
[3] Robinson A, Grimshaw G M. Br. J. Radiol., 1975,48(571): 572.
[4] GUO Qing-jiang, WANG Da-chun(郭清江,王大椿). Atomic Energy Science and Technology(原子能科学技术),1980, 14(4):385.
[5] Romanov A Yu. Measurement Techniques, 2004, 47(7): 670.
[6] Daniel Roemer. X-Ray Fluorescence With Doubly Curved Crystal Optics. Albany of New York (U. S. A.): University of Albany of State University of New York, 2007.
[7] SUN Tian-xi, DING Xun-liang, LIU Zhi-guo, et al(孙天希,丁训良,刘志国,等). Atomic Energy Science and Technology(原子能科学技术), 2008, 42(7): 633.
[8] Dubetsky B, Berman P R. Physical Review A, 1998, 58(3): 2413.
[9] Song Wei, et al. Journal of Raman Spectroscopy,2010,41(9): 907.
[10] Cornaby Sterling W. The Handbook of X-Ray Single-Bounce Monocapillary Optics, Including Optical Design and Synchrotron Applications. Cornell University, 2008.
[11] Wang Yabing, et al. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment,2019,934: 36.
[12] Wang Yabing, et al. Optics Communications,2020,464: 125544.
[13] Nakazawa Takashi, et al. Powder Diffraction,2011,26(2): 163.
[14] Matsuura Y, Oyama T, Miyagi M. Appl. Opt., 2005, 44(29): 6193. |
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