光谱学与光谱分析 |
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Simultaneous Determination of Glucose, Fructose and Sucrose in Aqueous Solution by Short-Wavelength Near Infrared Spectroscopy |
RAO Zhen-hong1,LI Min-zan2,JI Hai-yan2* |
1. College of Science, China Agricultural University, Beijing 100094, China 2. College of Information and Electrical Engineering, China Agricultural University, Beijing 100083, China |
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Abstract The calibration model for simultaneous determination of glucose, fructose and sucrose in aqueous solution was built by partial least squares and short-wavelength near infrared spectroscopy(800-1 100 nm). Twenty five samples in calibration set and 9 samples in prediction set were designed by orthogonal design. Building models from calibration set and validation for prediction set obtained the better results. For concentrations of glucose, fructose and sucrose in the ranges of 12.23-61.14 mg·mL-1,12.50-62.50 mg·mL-1 and 12.09-60.44 mg·mL-1,the relative standard deviations in the calibration set are 1.43%, 4.51% and 1.59% respectively, and the relative standard deviations in the prediction set are 3.40%, 3.73% and 2.80% respectively. The advantages of the method are simple and effective, with low cost for the simultaneous determination of multi-component system. It may be applied in practice easily.
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Received: 2004-12-28
Accepted: 2005-05-10
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Corresponding Authors:
JI Hai-yan
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Cite this article: |
RAO Zhen-hong,LI Min-zan,JI Hai-yan. Simultaneous Determination of Glucose, Fructose and Sucrose in Aqueous Solution by Short-Wavelength Near Infrared Spectroscopy [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(04): 633-635.
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URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I04/633 |
[1] Clement A,Yong D, Brechet C. J. Liq. Chromatogr., 1992, 15(5): 805. [2] Donald A Burns, Emil W Ciurczak. Handbook of Near-Infrared Analysis. New York: Marcel Dekker, Inc., 1992. [3] WANG Duo-jia, ZHOU Xiang-yang, JIN Tong-ming, et al(王多加, 周向阳, 金同铭, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2004,24(4): 447. [4] YAN Yan-lu, ZHAO Long-lian, LI Jun-hui, et al(严衍禄, 赵龙莲, 李军会, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2000, 20(6): 777. [5] WEN Min, JI Hai-yan(闻 明, 吉海彦). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2004, 24(10): 1276. [6] SHI Yue-hua, LU Yong, ZHANG Rong, et al(史月华,陆 勇,张 荣,等). Chinese Journal of Analytical Chemistry(分析化学), 2001, 29(10): 1213.
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