光谱学与光谱分析 |
|
|
|
|
|
Online Detection System on Acetylene with Tunable Diode Laser Absorption Spectroscopy Method |
HE Qi-xin1, LIU Hui-fang1, LI Bin1, PAN Jiao-qing2, WANG Li-jun2, ZHENG Chuan-tao1*, WANG Yi-ding1* |
1. State Key Laboratory on Integrated Optoelectronics, College of Electronic Science and Engineering, Jilin University, Changchun 130012, China2. Institute of Semiconductors, Chinese Academy of Sciences, Beijing 100083, China |
|
|
Abstract Based on tunable diode laser absorption spectroscopy (TDLAS) technique, an acetylene (C2H2) online detection system was developed by using the absorption band at the wavelength of 1.534 μm of C2H2 molecule. The sensing system consists of four modules including a distributed feedback (DFB) laser, a DFB laser driver, a gas cell with single optical path and a data processing module. With the prepared standard C2H2 gas sample, detailed measurements were carried out to study the detection performance of the system. Experimental results reveal that, the limit of the system (LOD) is about 0.02%; a good linear relationship is observed between C2H2 gas concentration and the amplitude of the 2f signal is within the range of 0.02%~1%. A long-term measurement lasting for 20 h on a 0.5% C2H2 gas sample was carried out to test the stability of the system. Compared with the C2H2 detection systems utilizing quantum cascaded lasers (QCLs) and wideband incandescence, this system has great advantage due to the capability of using long-distance and low-loss optical fiber for remote monitoring. With self-developed DFB laser driver and lock-in amplifier, the system has good prospects in industrial field because of its simple structure, low price and capability of easy to be integrated.
|
Received: 2015-10-05
Accepted: 2016-02-06
|
|
Corresponding Authors:
ZHENG Chuan-tao, WANG Yi-ding
E-mail: zhengchuantao@jlu.edu.cn; wangyiding48@yahoo.com.cn
|
|
[1] Wagner S, Klein M, Kathrotia T, et al. Applied Physics B, 2012, 107: 585. [2] XIA Hua, WU Bian, ZHANG Zhi-rong, et al(夏 滑,吴 边,张志荣,等). Acta Phys. Sinica(物理学报), 2013, 62: 214208. [3] Kluczynski P, Jahjah M, Nahle L, et al. Applied Physics B, 2011, 105: 427. [4] Xia H, Liu W, Zhang Y, et al. Chinese Optics Letters,2008, 6: 440. [5] Scherer J J, Paul J B, Jost H J, et al. Applied Physics B, 2013, 110: 271. [6] Ye W L, Zheng C T, Yu X, et al. Sensors and Actuators B: Chemical, 2011, 155: 37. [7] Durry G, Lij S, Vinogradov I, et al. Applied Physics B, 2010, 99: 339. [8] Huang J Q, Zheng C T, Gao Z L, et al. Spectroscopy Letters, 2014, 47: 197. [9] Cao Y, Jin W, Ho H L, et al. Applied Physics B, 2012, 109: 359. [10] Zheng C T, Ye W L, Huang J Q, et al. Sensors and Actuators B: Chemical, 2014, 190: 249. [11] Viciani S, Siciliani de Cumis M, Borr S, et al. Applied Physics B, 2015, 119: 21. [12] YE Wei-lin, ZHENG Chuan-tao, WANG Yi-ding(叶玮琳,郑传涛,王一丁). Acta Optica Sinica(光学学报), 2014, 34: 273. |
[1] |
ZHONG Qian1, 2, 3, WU Qiong2, 3, LIAO Zong-ting1, 2, 3*, ZHOU Zheng-yu1, 2, 3. Vibrational Spectral Characteristics of Ensignia Actinolite Jade from Guangxi, China[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(06): 1786-1792. |
[2] |
CHEN Quan-li, WANG Qian-xiang, JIN Wen-jing, YU Yi-tong. Study on the Composition and Structure Characteristics of “Lvlongjing” from Russia[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(07): 2225-2229. |
[3] |
CHEN Quan-li1, AI Su-jie1, WANG Qian-xiang1, LIU Xian-yu1,2,3*, DING Xin-rong1, YIN Zuo-wei1 . The Gemological Characteristics of One Kind Turquoise Imitation [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2016, 36(08): 2629-2633. |
[4] |
YAN Jun1, 2, WANG Xiao-xiang2, TAO Jin-bo1, ZHANG Jian3*, HU Xian-chao4 . Preliminary Study on the Unique Spectroscopic Characteristics of Natural and Synthetic Diamonds [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(10): 2723-2729. |
[5] |
PEI Jing-cheng1, FAN Lu-wei2, XIE Hao3*. Study on the Vibrational Spectra and XRD Characters of Huanglong Jade from Longling County, Yunnan Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(12): 3411-3414. |
[6] |
CHEN Quan-li, XU Ya-lan, AI Su-jie, HE An-qi, YIN Zuo-wei*. Vibrational Spectra of Caesious Nephritefrom Qinghai Province[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(08): 2017-2020. |
[7] |
CHENG Si-yang, GAO Min-guang, XU Liang*, JIN Ling, LI Sheng, TONG Jing-jing, WEI Xiu-li, LIU Jian-guo, LIU Wen-qing. Remote Sensing of Seasonal Variation in Column Concentration of Atmospheric CO2 and CH4 in Hefei[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(03): 587-591. |
[8] |
CHEN Quan-li, BAO De-qing, YIN Zuo-wei* . Study on XRD and Infrared Spectroscopy of Nephrites from Xinjiang and Xiuyan, Liaoning [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2013, 33(11): 3142-3146. |
[9] |
CHEN Quan-li, BAO De-qing, YIN Zuo-wei*, YAO Wei . Study on the Vibrational Spectra Characterization of the “She tai cui” Jade [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2013, 33(10): 2787-2790. |
[10] |
CHEN Quan-li1, ZHOU Guan-min2, YIN Zuo-wei1. Infrared Spectroscopy and XRD Studies of Coral Fossils[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2012, 32(08): 2246-2249. |
[11] |
SHI Xiu-min1, 2, JIANG Rui1, SONG Wei2, ZHAO Bing2*. Spectroscopy of Ag(Ⅰ), Cd (Ⅱ) Complexes with 4-Mercaptopyridine [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2012, 32(06): 1588-1591. |
[12] |
CHEN Jin1, 2, DUAN Fa-jie1, TONG Ying2, GAO Qiang3 . Genetic Programming Used for the Measurement of CO Concentration Based on Nondispersive Infrared Absorption Spectroscopy [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2011, 31(07): 1758-1761. |
[13] |
CHEN Quan-li, YUAN Xin-qiang, JIA Lu . Study on the Vibrational Spectra Characters of Taiwan Blue Chalcedony [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2011, 31(06): 1549-1551. |
[14] |
ZHU Ling-jian1,2, TANG Xiao-jun1, QIU Zong-ming2,LIU Jun-hua1,ZHANG Zhong-hua3,ZHANG Yong1 . A Method for Quantitative Analysis System of Alkane Gaseous Mixture with Near Infrared Spectroscopy [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2011, 31(01): 69-72. |
[15] |
ZHANG Xian-hui1,2,FENG Ke-cheng1,SUN Yue1,WANG Xing-quan1,SUN Xiu-ping1,YANG Si-ze2. The Study of Infrared Absorption Spectrum of Diamond during Growth by FTIR[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2008, 28(05): 1049-1051. |
|
|
|
|