| 光谱学与光谱分析 |
|
|
|
|
|
| Determination of Poly(Diallyldimethylammonium Chloride) via Spectrophotometric Titration with Coomassie Brilliant Blue G Dye |
| Alexander Shyichuk*, Dorota Ziókowska, Jan Lamkiewicz |
| UTP University of Science and Technology, Faculty of Chemical Technology and Engineering, Seminaryjna 3, 85-326 Bydgoszcz, Poland |
|
|
|
|
Abstract Poly(diallyldimethylammonium chloride) (PDDA) is used as organic coagulant in water purification and auxiliary agent in paper production. Determination of PDDA in aqueous solutions is carried out usually by means of polyelectrolyte titration using streaming current detector or o-Toluidine Blue dye for endpoint recognition. The proposed method of PDDA assay takes advantage of Coomassie Brilliant Blue G dye having strong affinity to cationic macromolecules. Titration of PDDA solution with the dye is carried out measuring absorbance at 585 nm. Inflection points of the obtained zigzag photometric curves have good repeatability provided that titration rate is low enough to attain endpoint for 1 hour or more. The method assures rectilinear calibration (R2=0.999 5) in the broad range of PDDA concentrations from 0.3 to 9.6 mg·dm-3.
|
|
Received: 2015-06-20
Accepted: 2015-08-10
|
|
|
|
Corresponding Authors:
Alexander Shyichuk
E-mail: szyjczuk@utp.edu.pl
|
|
[1] Wang S, Liu C, Li Q. Water Res., 2013, 47(13): 4538.
[2] Piazza G J, Lora J H, Garcia R A. Bioresour. Technol., 2014, 152: 548.
[3] Petzold G, Schwarz S, Lieske A. Wochenbl. Papierfabr., 2010, 138(2): 112.
[4] Chin S M, Youn H J, Ryu J, et al. Nord. Pulp Pap. Res. J., 2012, 27(5): 915.
[5] Cumming J L, Hawker D W, Matthews C, et al. Toxicol. Environ. Chem., 2010, 92(9): 1595.
[6] Masadome T. Talanta, 2003, 59(4): 659.
[7] Mocchiutti P, Zanuttini M A. BioResources, 2007, 2(3): 399.
[8] Cumming J, Hawker D, Chapman H, et al. Water Air Soil Pollut., 2011, 216(1-4): 441.
[9] Pelton R, Cabane B, Cui Y, et al. Anal. Chem., 2007, 79(21): 8114.
[10] Hubbe M A. Paper Technology, 2008, 49(6): 21.
[11] Gumbi B, Ngila J C, Ndungu P G. Phys. Chem. Earth, 2014, 67-69: 117.
[12] Gumbi B, Ngila J C, Ndungu P G. Anal. Methods, 2014, 6(17): 6963.
[13] Mwangi I W, Ngila C J, Ndungu P. Water SA, 2012, 38(5): 707.
[14] Zió?kowska D, Shyichuk A, ?elazko K. Polimery, 2012, 57(4): 303.
[15] Subrizi F, Crucianelli M, Grossi V, et al. ACS Catal., 2014, 4(3): 810.
[16] Zió?kowska D, Syrotynska I, Shyichuk A. Polimery, 2014, 59(2): 160.
[17] Aminian M, Nabatchian F, Vaisi-Raygani A, et al. Anal. Biochem., 2013, 434(2): 287. |
| [1] |
LIU Yan-de, WANG Shun. Research on Non-Destructive Testing of Navel Orange Shelf Life Imaging Based on Hyperspectral Image and Spectrum Fusion[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1792-1797. |
| [2] |
MA Ping1, 2, Andy Hsitien Shen1*, ZHONG Yuan1, LUO Heng1. Study on UV-Vis Absorption Spectra of Jadeite From Different Origins[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1827-1831. |
| [3] |
CAO Yao-yao1, 2, 4, LI Xia1, BAI Jun-peng2, 4, XU Wei2, 4, NI Ying3*, DONG Chuang2, 4, ZHONG Hong-li5, LI Bin2, 4*. Study on Qualitative and Quantitative Detection of Pefloxacin and
Fleroxacin Veterinary Drugs Based on THz-TDS Technology[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1798-1803. |
| [4] |
LI Shu-jie1, LIU Jie1, DENG Zi-ang1, OU Quan-hong1, SHI You-ming2, LIU Gang1*. Study of Germinated Rice Seeds by FTIR Spectroscopy Combined With Curve Fitting[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1832-1840. |
| [5] |
WEI Si-ye1, 2, FAN Xing-cheng3, MAO Han1, 2, CAO Tao4, 5, CHENG Ao3, FAN Xing-jun3*, XIE Yue3. Abundance and Spectral Characteristics of Molecular Weight Separated Dissolved Organic Matter Released From Biochar at Different Pyrolysis Temperatures[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1809-1815. |
| [6] |
WANG Gan-lin1, LIU Qian1, LI Ding-ming1, YANG Su-liang1*, TIAN Guo-xin1, 2*. Quantitative Analysis of NO-3，SO2-4，ClO-4 With Water as Internal Standard by Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1855-1861. |
| [7] |
XIE Yu-yu1, 2, 3, HOU Xue-ling1, CHEN Zhi-hui2, AISA Haji Akber1, 3*. Density Functional Theory Studies on Structure and Spectra of Salidroside Molecule[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1786-1791. |
| [8] |
YANG Lin-yu1, 2, 3, DING Yu1, 2, 3*, ZHAN Ye4, ZHU Shao-nong1, 2, 3, CHEN Yu-juan1, 2, 3, DENG Fan1, 2, 3, ZHAO Xing-qiang1, 2, 3. Quantitative Analysis of Mn and Ni Elements in Steel Based on LIBS and GA-PLS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1804-1808. |
| [9] |
HE Nian, SHAN Peng*, HE Zhong-hai, WANG Qiao-yun, LI Zhi-gang, WU Zhui. Study on the Fractional Baseline Correction Method of ATR-FTIR
Spectral Signal in the Fermentation Process of Sodium Glutamate[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1848-1854. |
| [10] |
WANG Bin1, 2, ZHENG Shao-feng2, LI Wei-cai2, ZHONG Kang-hua2, GAN Jiu-lin1, YANG Zhong-min1, SONG Wu-yuan3*. Determination of Rare Earth Elements in Imported Copper Concentrate by Inductively Coupled Plasma Mass Spectrometry With High Matrix
Injection System[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1822-1826. |
| [11] |
PENG Yan-fang1, WANG Jun1, WU Zhi-sheng2*, LIU Xiao-na3, QIAO Yan-jiang2*. NIR Band Assignment of Tanshinone ⅡA and Cryptotanshinone by
2D-COS Technology and Model Application Tanshinone Extract[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1781-1785. |
| [12] |
LI Qing1, 2, XU Li1, 2, PENG Shan-gui1, 2, LUO Xiao1, 2, ZHANG Rong-qin1, 2, YAN Zhu-yun3, WEN Yong-sheng1, 2*. Research on Identification of Danshen Origin Based on Micro-Focused
Raman Spectroscopy Technology[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1774-1780. |
| [13] |
TIAN Xue1, CHE Qian1, YAN Wei-min1, OU Quan-hong1, SHI You-ming2, LIU Gang1*. Discrimination of Millet Varieties and Producing Areas Based on Infrared Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1841-1847. |
| [14] |
WANG Yi-ya1, WANG Yi-min1*, GAO Xin-hua2. The Evaluation of Literature and Its Metrological Statistics of X-Ray Fluorescence Spectrometry Analysis in China[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1329-1338. |
| [15] |
FU Qiu-yue1, FANG Xiang-lin1, ZHAO Yi2, QIU Xun1, WANG Peng1, LI Shao-xin1*. Research Progress of Pathogenic Bacteria and Their Drug Resistance
Detection Based on Surface Enhanced Raman Technology[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1339-1345. |
|
|
|
|
