光谱学与光谱分析 |
|
|
|
|
|
Study of Laser Energy in Multi-Element Detection of Pulverized Coal Flow with Laser-Induced Breakdown Spectroscopy |
ZHENG Jian-ping1, LU Ji-dong1*, ZHANG Bo1, CHEN Shi-he2, YAO Shun-chun1, PAN Feng-ping2, DONG Xuan1, ZHANG Xi2 |
1. School of Electric Power of South China University of Technology, Guangzhou 510640, China 2. Electric Power Research Institute of Guangdong Power Grid Co. Ltd., Guangzhou 510080, China |
|
|
Abstract The logical range of laser power density and optimum laser power density were explored for multi-element analysis of pulverized coal flow with laser-induced breakdown spectroscopy in the present paper. The range of laser energy was chosen from 20 to 160 mJ in the experiment. Pulverized coal less than 200 μm in diameter of particles fell freely through feeder outlet and the rate of flow was controlled by screw feeder. Emissions were collected with pulse laser at 1 064 nm focusing on pulverized coal flow and plasma was generated. The intensity and cause of fluctuation of emission spectra at various laser energy levels were studied. A suitable range of laser power density is from 14.4 to 34.4 GW·cm-2, and the optimum laser power density is 19.5 GW·cm-2 for the determination of pulverized coal flow with LIBS.
|
Received: 2013-02-21
Accepted: 2013-05-14
|
|
Corresponding Authors:
LU Ji-dong
E-mail: jdlu@scut.edu.cn
|
|
[1] DONG Mei-rong,LU Ji-dong,YAO Shun-chun(董美容,陆继东,姚顺春). Journal of Engineering Thermophysics(工程热物理学报), 2012,33(1):175. [2] Gaft M,Dvir E,Modiano H,et al. Spectrochim. Acta Part B, 2008,57(1): 1. [3] Mateo M P,Nicolas G,Yanez A. Applied Surface Science, 2007, (254): 868. [4] Huang J S,Ke CB,Huang L S,et al. Spectrochimica Acta Part B, 2002,57(1):35. [5] Mao X L,Shannon M A,Femandez A J,et al. Applied Spectroscopy, 1995,49(7):1054. [6] Sarkar A,Shah R V,Alamelu D,et al. Journal of Atomic,Molecular, and Optical Physics, 2011,17:504. [7] ZHANG Lei,MA Wei-guang,YAN Xiao-juan(张 雷,马维光,闫晓娟). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2011,31(9):2355. [8] YAO Shun-chun,LU Ji-dong,LU Zhi-min(姚顺春,陆继东,卢志民). Acta Optica Sinica(光学学报), 2009,29(4):1126. [9] Tognoni E,Palleschi V,Corsi M. Spectrochimica Acta Part B, 2002, 57(1):1115. [10] Gaft M,Nagli L,Fasaki I,et al. Spectrochimica Acta Part B, 2009, 64:1098. [11] http://www.nist.gov. [12] Ottesen D K,Baxter L L,Radzienski L J,et al. Energy Fuels, 1991,5(2):304. [13] Mteo M P,Nicolas G,Yanez A. Applied Surface Science, 2007, (254) :868. [14] Handbook of Laser-Induced Breakdown Spectroscopy. New York: John Wiley & Sons Ltd. [15] Aguilera J A,Aragona C,Penalba F. Applied Surface Science, 1998, 127:309. [16] Lithgow G A,Robinson A L,Buckley S G. Atmospheric Environment, 2004,38:3319. |
[1] |
LIU Jia1, 2, GUO Fei-fei2, YU Lei2, CUI Fei-peng2, ZHAO Ying2, HAN Bing2, SHEN Xue-jing1, 2, WANG Hai-zhou1, 2*. Quantitative Characterization of Components in Neodymium Iron Boron Permanent Magnets by Laser Induced Breakdown Spectroscopy (LIBS)[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 141-147. |
[2] |
TIAN Fu-chao1, CHEN Lei2*, PEI Huan2, BAI Jie-qi1, ZENG Wen2. Study of Factors Influencing the Length of Argon Plasma Jets at
Atmospheric Pressure With Needle Ring Electrodes[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3682-3689. |
[3] |
YANG Wen-feng1, LIN De-hui1, CAO Yu2, QIAN Zi-ran1, LI Shao-long1, ZHU De-hua2, LI Guo1, ZHANG Sai1. Study on LIBS Online Monitoring of Aircraft Skin Laser Layered Paint Removal Based on PCA-SVM[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3891-3898. |
[4] |
SUN Cheng-yu1, JIAO Long1*, YAN Na-ying1, YAN Chun-hua1, QU Le2, ZHANG Sheng-rui3, MA Ling1. Identification of Salvia Miltiorrhiza From Different Origins by Laser
Induced Breakdown Spectroscopy Combined with Artificial Neural
Network[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3098-3104. |
[5] |
LIU Hong-wei1, FU Liang2*, CHEN Lin3. Analysis of Heavy Metal Elements in Palm Oil Using MP-AES Based on Extraction Induced by Emulsion Breaking[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3111-3116. |
[6] |
LIU Shu1, JIN Yue1, 2, SU Piao1, 2, MIN Hong1, AN Ya-rui2, WU Xiao-hong1*. Determination of Calcium, Magnesium, Aluminium and Silicon Content in Iron Ore Using Laser-Induced Breakdown Spectroscopy Assisted by Variable Importance-Back Propagation Artificial Neural Networks[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3132-3142. |
[7] |
LIU Pan1, 2, 3, DU Mi-fang1*, LI Bin1, LI Jing-bin1, ZENG Lei1, LIU Guo-yuan1, ZHANG Xin-yao1, 4, ZHA Xiao-qin1, 4. Determination of Trace Tellurium Content in Aluminium Alloy by
Inductively Coupled Plasma-Atomic Emission Spectrometry Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3125-3131. |
[8] |
ZHU Yu-qi1, 2, ZHANG Xin2, DU Pan-pan2, LIU Shu1, ZHANG Gui-xin1, 2, GUAN Song-lei2*, ZHENG Zhong1*. Infrared Spectroscopy and X-Ray Spectroscopy Combined With
Inductively Coupled Plasma Mass Spectrometry for Quality
Control of Mongolian Medicine Yu Grain Soil[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3163-3169. |
[9] |
YANG Fan1, HAO Liu-cheng1, KE Wei2, LIU Qing1, WANG Jun1, CHEN Min-yuan2, YUAN Huan2*, YANG Ai-jun2, WANG Xiao-hua2, RONG Ming-zhe2. Research on Effect of Laser Incident Angle on Laser-Induced Plasma at Low Pressure[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2740-2746. |
[10] |
ZHANG Zhi-fen1, LIU Zi-min1, QIN Rui1, LI Geng1, WEN Guang-rui1, HE Wei-feng2. Real-Time Detection of Protective Coating Damage During Laser Shock Peening Based on ReliefF Feature Weight Fusion[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2437-2445. |
[11] |
LI Chang-ming1, CHEN An-min2*, GAO Xun3*, JIN Ming-xing2. Spatially Resolved Laser-Induced Plasma Spectroscopy Under Different Sample Temperatures[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2032-2036. |
[12] |
LI Shi-lun1, LIU Tao2, SONG Wen-min3, WANG Tian-le2, LIU Wei1, CHEN Liang1, LI Zhi-gang2*, FENG Shang-shen1*. Study of Two-Dimensional Ordered Magnetic Co Nanosphere Array Film Construction and Its Optical Properties[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2037-2042. |
[13] |
ZHAO Yang1, ZHANG Lei2, 3*, CHENG Nian-kai4, YIN Wang-bao2, 3*, HOU Jia-jia5, BAI Cheng-hua1. Research on Space-Time Evolutionary Mechanisms of Species Distribution in Laser Induced Binary Plasma[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2067-2073. |
[14] |
YAN Ming-liang1, ZHANG Chen-long2, ZHAO Lian-xiang3, ZHAO Hua-he4, GAO Xun2*. Spectral Characteristics of Ge Plasma Induced by Femtosecond Pulsed Laser Ablation[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2095-2098. |
[15] |
WANG Bin1, 2, ZHENG Shao-feng2, GAN Jiu-lin1, LIU Shu3, LI Wei-cai2, YANG Zhong-min1, SONG Wu-yuan4*. Plastic Reference Material (PRM) Combined With Partial Least Square (PLS) in Laser-Induced Breakdown Spectroscopy (LIBS) in the Field of Quantitative Elemental Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2124-2131. |
|
|
|
|