| 光谱学与光谱分析 |
|
|
|
|
|
| Flow-Injection Chemiluminescence Determination of Procaterol Hydrochloride |
| RAO Zhi-ming1,ZOU Ping1,CHEN Mei1,XIU Fu-rong1,CHEN Yu-lin2,HONG Ke-jun2 |
1. Department of Chemistry and Environmental Science, Zhangzhou Normal College, Zhangzhou 363000, China
2. Zhangzhou Institute of Drug Control, Zhangzhou 363000, China |
|
|
|
|
Abstract A new flow injection chemiluminescences method for the determination of procaterol hydrochloride has been developed. It is based on the chemiluminescence reaction of procaterol hydrochloride with Ce(Ⅳ)-rhodamine B in sulphuric-chlorhydric acid medium and the experimental fact of the enhancement of chemiluminescence by surfactant CTMAB. The concentration of the analyte shows a good linear relationship with the produced luminescence intensity in the range of 2.0×10-8g·mL-1 to 1.0×10-6g·mL-1. The detection limit of the proposed method is 6×10-9g·mL-1 and the RSD is 1.6％(n=11) at 2×10-7g·mL-1. This result is satisfactory compared with the method mentioned in the pharmacopoeia of People’s Republic of China.
|
|
Received: 2006-08-10
Accepted: 2006-12-20
|
|
|
|
Corresponding Authors:
RAO Zhi-ming
E-mail: raozhm@163.com
|
|
[1] WANG Zheng, LIU Chang-shan, ZHU Zhu, et al(王 峥, 刘长山, 朱 珠, 等). Journal of Chinese Modern Pediatrics(中华现代儿科学杂志),2005,2(3): 205.
[2] JIAO Shu-qing, YU Lian, HOU Wei(焦淑清, 于 莲, 侯 巍). Chinese Journal of Medical Writing(中华医学写作杂志),2002，9(17)：1380.
[3] XING Li-qing, HE Zhen-mei, ZHU Bao-yu, et al(邢莉清, 何振梅, 朱宝玉, 等). China Pharmacist(中国药师),2001，4(4)：284.
[4] Editorical Committee of the Pharmacopoeia of People’s Republic of China(中华人民共和国药典编委会编). The Pharmacopoeia of People’s Republic of China(Part Ⅱ)(中华人民共和国药典第二部). Beijing: Chemical Industry Press(北京：化学工业出版社),2000. 561.
[5] RAO Zhi-ming, ZHANG Wang-hua, LI Qiu-zhong, et al(饶志明, 张旺华, 李求忠, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2004，24(3)：278.
[6] Rao Zhi-ming, Zhang Xin-rong, Willy R G. Baeyens. Talanta,2002, 57: 993.
[7] ZHANG Fan, LIU Zhen-ming(张 帆, 刘振鸣). Chinese J. Anal. Chem.(分析化学), 1989, 17(11): 1051.
[8] ZHANG Fan, CHEN Guo-nan(张 帆，陈国南). Chemiluminescence and Bioluminescence-Theory and Application(化学发光与生物发光-理论及应用). Fuzhou: Fujian Science Technology Press(福州: 福建科学技术出版社), 1997. 261.
[9] Rao Yi, Zhang Xin-rong, Luo Guo-an, et al. Analytica Chimica Acta, 1999, 396: 273.
[10] RAO Zhi-ming, WU Qiu-lian, XIE Guo-ping, et al(饶志明，吴秋莲，谢国平，等). Chinese J. Anal. Chem.(分析化学)，2004，32(12)：1660.
[11] Yuming Huang, Chao Zhang, Xinrong Zhang, et al. Analytical Chimica Acta, 1999, 391: 95.
[12] Yuming Huang, Chao Zhang, Xiurong Zhang, et al. Phamaceutical and Biomedical Analysis, 1999,21: 817.
[13] Zhiming Rao, Qiaomei Lu, Liangzhou Fang, et al. Spectroscopy Letters,2006, 39(3): 249. |
| [1] |
ZHENG Pei-chao, ZHONG Chao, WANG Jin-mei*, LUO Yuan-jiang, LAI Chun-hong, WANG Xiao-fa, MAO Xue-feng. Evaluation of Flow Injection-Solution Cathode Glow Discharge With an Interference Filter Wheel for Spectral Discrimination[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(03): 842-847. |
| [2] |
XIA Xue, PAN Yun-xia*, LI Meng-zhu. Photocatalytic Degradation of RhB Dye by Copolymerization Modification g-C3N4-N Under Visible Light[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(02): 517-522. |
| [3] |
ZHOU Ying1, BAI Yong-hui1, SONG Xu-dong1*, YAO Min3, WANG Jiao-fei1, SU Wei-guang1, YU Guang-suo1,2*. Application of Chemiluminescence in Spectral Diagnosis: A Review[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(11): 3358-3364. |
| [4] |
WU Sheng-yang1,2, HU Ren-zhi1,2*, XIE Pin-hua1,2, LI Zhi-yan1,2, LIU Xiao-yan3, LIN Chuan1,4, CHEN Hao1,2, WANG Feng-yang1,2, WANG Yi-hui1,5, JIN Hua-wei1,2. Real-Time Measurement of NOy （Total Reactive Nitrogen Oxide） by Cavity Ring Down Spectrometer (CRDS)[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(06): 1661-1667. |
| [5] |
LIU Yao, TAN Jian-guo*, GAO Zheng-wang. College of Aerospace Science and Engineering, National University of Defense Technology, Changsha 410073, China[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(04): 1018-1022. |
| [6] |
WANG Zhong-yuan1, ZHANG Hong-kang2*, NI Zhi-xin1, LIU Jing-qin1, CHEN Xin1, LI Sheng-yong1, YANG Qi-jin2, ZHANG Can1. FI-KR-FAAS Twice Gas Isolation Elution Method for the Determination of Trace Lead in Marine Biological Samples[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(11): 3578-3582. |
| [7] |
ZHANG Lu-tao, ZHOU Guang-ming*, ZHANG Cai-hong, LUO Dan. The Preparation of the New Membrane-Like Gold Nanoparticles Substrate and the Study of Its Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(06): 1741-1746. |
| [8] |
Kariyemu·AIHAITI1, Mirzat·MAIMAITI2, Arkin·IBURAIM1, 3*. Study Comparative Light Intensity of Laser Light Source-Online Fluorescence Spectrum Detection[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(01): 134-138. |
| [9] |
CAO Xuan1,2, CHU Dong-zhi1,2, LIU Yan1,2*, MA Ran1,2, ZHANG Shu-wei1,2, WU Ning1,2, SHI Qian1,2, MA Hai-kuan1,2. An On-Line Microfluidic Analysis System for Seawater Chemical Oxygen Demand Using Ozone Chemiluminescence[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(12): 3698-3702. |
| [10] |
AN Xue-jing, LUO Yun-jing*, ZHANG Chen-yang. Research on the Reaction Dynamics between Peroxynitrite and Tyrosine Catalyzed with Mimic Enzyme through Flow Injection Analyzer[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2016, 36(12): 4052-4057. |
| [11] |
FAN Cai-ling1,2, XIE Pu-hui1, CUI Shu-min1, YANG Li-na1, SUN Qing1, AI Zhi-lu2，3* . The Fluorescence Enhancement of Mercury Detected in Food Based on Rhodamine Derivatives [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(05): 1300-1305. |
| [12] |
ZHENG Zhi-yuan1, 2, 3, DU Yu-zhi1, 2, ZHANG Ming1, 2, 3, YU Ming-jie1, 2, 3, LI Cen1, 2, 3, YANG Hong-xia1, 2, ZHAO Jing1, 2, 3, XIA Zheng-hua1, 2, 3, WEI Li-xin1, 2*. Study on Content Determination of Lead and Arsenic in Four Traditional Tibetan Medicine Prescription Preparations by Wet Digestion Flow Injection-Hydride Generation-Atomic Absorption Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(04): 1037-1042. |
| [13] |
NI Wei-quan1, HE Jian1*, LIU Guo-kun2, CHEN Hong-ju2, ZENG Yong-ming2, TIAN Zhong-qun2 . Instrumentation and Application of a Portable Pretreating System for a Speedy Plasmon-Enhanced Raman Spectroscopy Detection Towards Food Safety [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(04): 1107-1110. |
| [14] |
SONG Xiao-feng1, TAO Hong1*, CHEN Biao2, CHEN Liang-xia1, LI Liang1, SUN Yan1, PANG Tao1, WANG Yan-gang1 . Spectroscopic Analysis and Photocatalytical Activity of Carbon Nitride Materials [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(01): 242-244. |
| [15] |
CAO Jun-tao1, WANG Hui1, CHEN Yong-hong2, LIU Yan-ming1* . Sensitive Determination of Hemoglobin in Human Blood and Serum by Flow Injection Coupled with Chemiluminescence Detection [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(01): 241-245. |
|
|
|
|
