| 光谱学与光谱分析 |
|
|
|
|
|
| Determination of Gold in Copper Matte and Sintered Copper Material |
| GE Yu-wei1, XIAO Li-mei2, SUO Jin-ling3, WANG Cheng4*, HU Xiao-min5, ZHAO Shu-yun6 |
1. GanFeng Lithium industry Co., Ltd.(China), Xinyu 338000, China
2. XinJiang ZhongHe Co., Ltd.(China), Urumqi 830021, China
3. Xinjiang Alashankou Entry-Exit Inspection and Quarantine Bureac, Alashankou 833418, China
4. Xinjiang Entry-Exit Inspection and Quarantine Bureau, Urumqi 830063, China
5. China Certification and Inspection Group Xinjiang Alashankou Co. Ltd., Alashankou 833418, China
6. College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, China |
|
|
|
|
Abstract Ore sample, pretreated at 650 ℃, was decomposed with aqua regia. Gold in the sample solution was then pre-concentrated by adsorbing with polyurethane foam plastic, released with thiourea solution, and determined by inductively coupled plasma-atomic emission spectrometry and flame atomic absorption spectrometry. Based on the characteristic of the copper matte and sinter containing copper, the effects of sample dissolving condition, matrix effect and interference of coexisting elements were investigated. The accuracy, precision and detection limit were discussed. The results of test show that both of the two methods were suitable for determining the contents of gold in copper matte and sintered copper material.
|
|
Received: 2010-07-14
Accepted: 2010-10-10
|
|
|
|
Corresponding Authors:
WANG Cheng
E-mail: ciqwangcheng@126.com
|
|
[1] XUE Guang(薛 光). Polyurethane Foam Preconcentration(聚氨酯泡沫塑料富集金). Beijing：Peking University Press(北京：北京大学出版社), 1990. 23.
[2] JIANG Shui-ying, XIAO Hua-yun, WU Sheng-dong(江水英，肖化云，吴声东). Rock and Mineral Analysis(岩矿测试), 2008, 27(4): 299.
[3] WANG Shi-hui, YE Xue-jun, HU Min(王世辉，叶雪均，胡 敏). Metallurgical Analysis(冶金分析), 2008, 28(1): 71.
[4] GAN Jian-zhuang, GUAN You-xiang, LI Kai-zhong(甘建壮，管有祥，李楷中). Precious Metals(贵金属), 2008, 29(4): 34.
[5] PANG Xiao-hui(庞晓辉). Physical Testing and Chemical Analysis(Part B:Chemical Analysis)(理化检验-化学分册), 2008, 44(4): 348.
[6] HU Qiu-fen, GUO Hong, HUANG Qi-lin(胡秋芬，郭 红，黄齐林). Physical Testing and Chemical Analysis(Part B:Chemical Analysis)(理化检验-化学分册), 2009, 45(5): 561.
[7] LI Yong(李 勇). Rock and Mineral Analysis(岩矿测试), 2008, 27(4): 305.
[8] YANG Jian(阳 健). Metal Mine(金属矿山), 2008, (6): 152.
[9] LUO Fu-xing(罗付兴). Chinese Journal of Anaiysis Laboratory(分析试验室), 2009, 28(5): 249.
[10] SONG Li-hua, JIN Yi(宋丽华，金 一). Physical Testing and Chemical Analysis(Part B: Chemical Analysis)(理化检验-化学分册), 2009, 45(6): 692.
[11] XUE Guang, SUN Peng(薛 光, 孙 鹏). Gold(黄金), 2006, 27(3): 51.
[12] LI Kun(李 锟). Geology of Chemical Minerals(化工矿产地质),2007, 29(4): 243.
[13] MENG Hong, JIN Li(孟 红, 金 丽). Gold(黄金), 2009, 30(8): 54.
[14] LI Cheng-yuan, LI Rong, ZHAO Gang(李承元, 李 蓉, 赵 刚). Gold(黄金), 2005，26(12): 48.
[15] ZENG Nian-hua(曾念华). Physical Testing and Chemical Analysis(Part B:Chemical Analysis)(理化检验-化学分册)，2003，39(6)：347.
|
| [1] |
LI Ling1, 2, 3, NAI Xue-ying1, 2*, CHAI Xiao-li1, 2, 3, LIU Xin1, 2, GAO Dan-dan1, 2, DONG Ya-ping1, 2. Optimization of Determination Method of Lithium in Oil-Field Water Based on DOE[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(08): 2617-2621. |
| [2] |
LINGYUN Xia-fei1, 2, GAO Chao1, 2, FAN Jing-shuang1, 2, Lü Hai-xia1, 2*, YU Yan1, 2. Synthesis of Hyperbranched Polyamidoamine (PAMAM) Grafted Chitosan and Its Adsorption for Heavy Metal and Dyes Studied with Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(11): 3583-3587. |
| [3] |
YAO Shi-xiang1, 2, XIE Jiao1, ZENG Kai-fang1, 2*. Comparative Analysis of Several Mineral Elements Contents in Vascular Bundle of Satsuma Mandarin and Ponkan Mandarin Fruit[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(04): 1250-1253. |
| [4] |
ZHAO Fang-biao2, SONG Nai-zhong1, NING Wei-kun2, JIA Qiong1* . Synthesis of Magnetic Metal Organic Framework Fe3O4@NH2-MIL-53(Al) Materials and Application to the Adsorption of Lead [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(09): 2439-2443. |
| [5] |
ZHAI Yu-xin1, CHEN Jun1, LI Ti1*, LIU Ji-yan2, WANG Xie-yi1, CHENG Chao1, LIU Cheng-mei1 . Determination of Mineral Elements in Choerospondias Axillaris and Its Extractives by ICP-AES [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(04): 1052-1055. |
| [6] |
Medine Abduwayit, Ismayil Nurulla, Shawket Abliz* . Preparation of Polyacrylonitrile/Natural Sand Composite Materials and Analysis of Adsorption Properties of Pb(Ⅱ) on It by FAAS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2015, 35(02): 539-542. |
| [7] |
LI Hua1, LIU Jing1, 2, FU Mei-hong1, KANG Chen1, FANG Jing1, YANG Bin1*. Analysis of Dissolution Characteristics and Content of Metal Elements in Scutellaria Baicalensis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2014, 34(08): 2264-2267. |
| [8] |
LIN Jian-mei, YAO Jun-xue*, ZHAO Wen-yan . Determination of Trace Lead in Water and Milk Tea Powder Samples with Organic Coprecipitation-Flame Atomic Absorption Spectrometric [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2013, 33(05): 1357-1359. |
| [9] |
Shawket Abliz, Abderyim Sopahun, Ismayil Nurulla*. Analysis of the Adsorption Properties of Lead Ion onto Natural Sand Particles by Flame Atomic Absorption Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2011, 31(11): 3126-3129. |
| [10] |
NING Xun-an, ZHOU Yun, LIU Jing-yong, WANG Jiang-hui, LI Lei, MA Xiao-guo . Determination of Metals in Waste Bag Filter of Steel Works by Microwave Digestion-Flame Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2011, 31(09): 2565-2568. |
| [11] |
LI Chun-li1, 2，ZHOU Guo-ying1, 3*，HU Feng-zu1，XU Wen-hua1, 3，CHEN Gui-chen1, 3 . Determination of Trace Determination of Elements in Medicinal Materials of Cultivated and Wild Rhizoma et Radix Notopterygii Vegetated in Different Months by Flame Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2011, 31(04): 1122-1125. |
| [12] |
WU Jun，FU Hao，LI Bin-jian，ZHU Xia-shi* . Hydrophobic Ionic Liquid Extraction-Flame Atomic Absorption Spectrophotometry for Separation/Analysis Trace Gold [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2011, 31(01): 260-262. |
| [13] |
NING Peng-bo1, GONG Chun-mei2, ZHANG Yan-ming1*, GUO Kang-kang1 . Analysis of Rare Earth Elements in Pu’er Tea of Yunnan by ICP-AES [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2010, 30(10): 2830-2833. |
| [14] |
XIONG Wei1，CAI Miao-zhen1，WANG Hong1，YU Rui-peng2，CHENG Cun-gui1* . Analysis and Comparison of Trace Elements of Herba Euphorbiae Humifusae in Different Periods by Microwave Digestion-Atomic Absorption Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2010, 30(07): 1975-1978. |
| [15] |
LIU Jin1, 2，ZHANG Huai-gang1* . Determination of Nine Mineral Elements in Hulless Barley by Ultraviolet Spectrophotometry and Flame Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2010, 30(04): 1126-1129. |
|
|
|
|
