光谱学与光谱分析 |
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Study on the Speciation of Calcium in Baihu Decoction |
Lü Pei, LI Xiang*, CHEN Jian-wei |
College of Pharmacy, Nanjing University of Traditional Chinese Medicine, Nanjing 210046, China |
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Abstract A method for speciation analysis of calcium in Baihu decoction was presented. The six different forms of Ca in the filtrate including free ions, non-free ions, exchangeable, non-exchangeable, organic and inorganic were separated by using ion-exchange resin (IER), chelating resin and organic solvent extraction. Various forms of Ca were determined by inductively coupled plasma atomic emission spectrometry (ICP-AES). The recovery for the method is 90.0%-110.0%. The result showed that Baihu decoction extract was a kind of complex solution, in which 83.25% of Ca existed in free ions form and 23.79% of Ca existed in organic form in the soluble filtrate.
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Received: 2009-11-02
Accepted: 2010-02-06
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Corresponding Authors:
LI Xiang
E-mail: Lixiang_8182@163.com
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