| 光谱学与光谱分析 |
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| Determination of Zinc in Relish by Derivate Flame Atomic Absorption Spectrometry with Microsampling Pulse Nebulization |
| JI Xue-ping1, 2, KANG Wei-jun2, REN Qing-yu3，ZHAO Jin-pei3，SUN Han-wen1 |
1. College of Chemistry & Environmental Science, Hebei University, Baoding 071002, China
2. College of Health Technology, Hebei Medical University, Shijiazhuang 050017, China
3. Military Medicine Institute of Beijing Military Command, Shijiazhuang 050081, China |
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Abstract A simple，rapid, microsampling method for the determination of zinc in relish by derivative FAAS is described. The influences of microsampling volume and other factors are discussed. The detection limit and sensitivity of the proposed method are 0.013 and 0.004 μg·mL-1, respectively. The samples were centrifugalized and diluled with 1.5% HCl solution, and then analysized directly. The method was applied to the determination of zinc in relish with a recovery of 93.3％-113.3% and relative standard deviation of 3.0%-4.4%.
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Received: 2002-10-20
Accepted: 2003-02-26
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Corresponding Authors:
JI Xue-ping
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| Cite this article: |
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JI Xue-ping,KANG Wei-jun,REN Qing-yu, et al. Determination of Zinc in Relish by Derivate Flame Atomic Absorption Spectrometry with Microsampling Pulse Nebulization [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(08): 1020-1022.
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| URL: |
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http://www.gpxygpfx.com/EN/Y2004/V24/I08/1020 |
[1] JI Xue-ping，LI Ｘinｇ-fa，LIU Man-ｙinｇ et al(籍雪平，李兴发, 刘满英等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1999, 19(1): 87.
[2] SUN Han-wen et al. Talanta, 1997, 44(11): 1979.
[3] SUN Han-wen et al. Fresenius J. Anal. Chem.，1997, 358: 646.
[4] KANG Wei-jun et al(康维钧等). China Public Health(中国公共卫生), 2002, 18(3): 367.
[5] SUN Han-wen(孙汉文编著). Atomic Spectrum Analysis(原子光谱分析). Beijing: Higher Education Press(北京: 高等教育出版社), 2002. 164.
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