| 光谱学与光谱分析 |
|
|
|
|
|
| Determination of Trace Cs, Th and U in Ten Kinds of Human Autopsy Tissues by ICP-MS |
| WANG Jing-yu1, ZHU Hong-da2, OUYANG Li1, LIU Ya-qiong1, WANG Xiao-yan1, HUANG Zhuo1, WANG Nai-fen1， LIU Hu-sheng1 |
1. College of Public Health, Peking University, Beijing 100083，China
2. Institute of Radiation Medicine, Chinese Academy of Medical Sciences, Tianjin 300192, China |
|
|
|
|
Abstract This paper studied the trace elements Cs, Th and U in ten kinds of human autopsy tissues by ICP-MS. The instrumental operating conditions were optimized for the measurement of Cs, Th and U. Rhodium (Rh) was used as an internal standard element to compensate matrix effect. Detection limits for Th, U and Cs were 5.7-17.8 pg·mL-1. The recoveries for spiking liver samples were 96%-107%, and their RSDs were 4.8%-8.9%. Reference materials of NIST SRM 8414 Bovine and NIST SRM 1 486 Bone Meal were analyzed by the described method, and the analytical results agreed well with the reference values. Human autopsy tissues samples were digested by mixed acid (HNO3+HClO4). The determination of Cs, Th and U in lung, liver, bone, heart, stomach, spleen, muscle, kidney, thyroid gland and intestinum tenue was performed by ICP-MS without separation and enrichment procedures. The obtained results indicated that this method is rapid, sensitive and accurate; the distribution of the three elements is different from one to another human organ sample; the main organ targets for Th and U are lungs and kidneys; and a coordinated variation of Cs, Th and U concentration in lungs was found in the samples collected from Hebei and Sichuan provinces.
|
|
Received: 2003-06-18
Accepted: 2003-10-25
|
|
|
|
Corresponding Authors:
WANG Jing-yu
|
|
| Cite this article: |
|
WANG Jing-yu,ZHU Hong-da,OUYANG Li, et al. Determination of Trace Cs, Th and U in Ten Kinds of Human Autopsy Tissues by ICP-MS [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2004, 24(09): 1117-1120.
|
|
|
|
| URL: |
|
http://www.gpxygpfx.com/EN/Y2004/V24/I09/1117 |
[1] Benes et al. Biological Trace Element Research, 2000, 75: 195.
[2] Igarashi Y, Kawamura H, Shiraishi Ｋ, Takaku Y J. Anal. At. Spectrom., 1989, 4: 571.
|
| [1] |
WANG Gan-lin1, LIU Qian1, LI Ding-ming1, YANG Su-liang1*, TIAN Guo-xin1, 2*. Quantitative Analysis of NO-3，SO2-4，ClO-4 With Water as Internal Standard by Raman Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1855-1861. |
| [2] |
LUO Heng, Andy Hsitien Shen*. Based on Color Calculation and In-Situ Element Analyze to Study the Color Origin of Purple Chalcedony[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1891-1898. |
| [3] |
LIU Jiang-qing1, YU Chang-hui2, 3, GUO Yuan2, 3, LEI Sheng-bin1*, ZHANG Zhen2, 3*. Interaction Between Dipalmityl Phosphatidylcholine and Vitamin B2
Studied by Second Harmonic Spectroscopy and Brewster Angle
Microscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1484-1489. |
| [4] |
GAO Sha1, YUAN Xi-ping1, 3, GAN Shu1, 2*, HU Lin1, BI Rui1, LI Rao-bo1, LUO Wei-dong1. UAV Image Matching Method Integrating SIFT Algorithm and Detection Model Optimization[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1497-1503. |
| [5] |
SHI Pei1, JIN Zhi-wei1, WANG Fen1*, LUO Hong-jie1, 2, ZHU Jian-feng1, YE Guo-zhen3, ZHANG Yu-feng4. Influence Mechanism of the Iron-Rich Raw Material on the Iron-Based Crystalline Glazes[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(05): 1628-1633. |
| [6] |
YANG Yan-ling1, Andy Hsitien Shen1, FAN Yu-rong2, HUANG Wei-zhi1, PEI Jing-cheng1*. UV-Vis-NIR Spectroscopic Characteristics of Vanadium-Rich
Hydrothermal Synthetic Emeralds From Russia[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1199-1203. |
| [7] |
DU Bao-lu, LI Meng, GUO Jin-jia*, ZHANG Zhi-hao, YE Wang-quan, ZHENG Rong-er. The Experimental Research on In-Situ Detection for Dissolved CO2 in
Seawater Based on Tunable Diode Laser Absorption Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1264-1269. |
| [8] |
YAO Shan1, ZHANG Xuan-ling1, CAI Yu-xin1, HE Lian-qiong1, LI Jia-tong1, WANG Xiao-long1, LIU Ying1, 2*. Study on Distribution Characteristics of Different Nitrogen and
Phosphorus Fractions by Spectrophotometry in Baiyangdian
Lake and Source Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1306-1312. |
| [9] |
FU Ying-ying, ZHANG Ping, ZHENG Da-wei , LIN Tai-feng*, WANG Hui-qin, WU Xi-hao, SONG Jia-chen. Preparation and SERS Performance of Au-Nylon Flexible Membrane Substrate[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 692-698. |
| [10] |
TANG Qian1, 3, HUANG Ting2, 3, GONG Ting-ting1, 3, CAO Hong-yu1, 3, WANG Ai-ling2, 3, WANG Li-hao2, 3, ZHENG Xue-fang1, 2, 3*. Spectroscopic Study on the Mechanism of Photoduction of Cytochrome b5 by Ultraviolet Light[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 821-827. |
| [11] |
XU Jia-yi1, 3, HUANG Xue2, 3, LUO Hua-ping1, 3*, LIU Jin-xiu1, 3, SUO Yu-ting1, 3, WANG Chang-xu1, 3. Effects of Orientation and Quality on Spatial Spectrum Characteristics of Fruits in Southern Xinjiang[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(03): 910-918. |
| [12] |
LI Zhao, WU Kun-yao, WANG Ya-nan, CAO Jing, WANG Yong-feng, LU Yuan-yuan. Synthesis and Luminescence Properties of Yellow-Emitting Phosphor Y2.93Al5O12∶0.07Ce3+ Under Blue Light Excitation[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(02): 381-385. |
| [13] |
WANG Yuan1, ZHANG Zhen2*, GUO Yuan2, 3. A Simplified Method of Microscopic Polarizability Tensor Differential of Hyper-Raman Spectroscopy Based on Experimental Correction Bond Additivity Model-C2v Symmetry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(01): 124-129. |
| [14] |
ZHONG Yuan, QU Meng-wen, Andy Hsitien Shen*. Comparison of Chemical Composition and Spectroscopy of Purple- Brownish Red Garnet From Zambia, Tanzania and Australia[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(01): 184-190. |
| [15] |
XIAO Shi-jie1, WANG Qiao-hua1, 2*, FAN Yi-kai3, LIU Rui3, RUAN Jian3, WEN Wan4, LI Ji-qi4, SHAO Huai-feng4, LIU Wei-hua5, ZHANG Shu-jun3*. Rapid Determination of αs1-Casein and κ-Casein in Milk Based on Fourier Transform Infrared Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(12): 3688-3694. |
|
|
|
|
