光谱学与光谱分析 |
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Determination of Thirteen Metal Elements in the Plant Foeniculum Vulgare Mill. by Flame Atomic Absorption Spectrophotometry |
XUE Guo-qing1, LIU Qing2, HAN Yu-qi1, WEI Hui-guang1, DONG Ting1 |
1. Department of Chemistry, Key Laboratory of Resources and Environment Chemistry of West China, Hexi University, Zhangye 734000, China 2. The 4th Geoteam of the Gansu Non-Ferrous Geoexploration Bureau, Zhangye 734012, China |
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Abstract The objective of the paper is to determine the amount of metal elements of Na, K, Mg, Ca, Cu, Zn, Mn, Fe, Co, Ni, Cd, Cr and Pb in the planted Foeniculum vulgare Mill. by flame atomic absorption spectrophotometry(FAAS), after the cinefaction and the digestion with HNO3-HClO4(φ 4∶1) at 90-95 ℃ and normal pressure. The optimum parameters of FAAS and the effects of solution medium on the results were investigated. The analytical results show that the amount of Na, K, Mg, Ca, Mn, Fe, Cu, Zn and Pb was 1 508.7, 27 653.0, 2 036.0, 4 848.1, 24.8, 323.5, 15.2, 23.7 and 10.8 μg·g-1,respectively, and that of Co, Ni, Cd and Cr was not checked out in the samples. The recovery of standard addition is 97.45%-102.50%, the relative standard deviation(n=9) was 0.34%-2.77%. The characteristic method is quick, simple and convenient and the results are satisfactory.
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Received: 2005-06-06
Accepted: 2005-09-28
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Corresponding Authors:
XUE Guo-qing
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Cite this article: |
XUE Guo-qing,LIU Qing,HAN Yu-qi, et al. Determination of Thirteen Metal Elements in the Plant Foeniculum Vulgare Mill. by Flame Atomic Absorption Spectrophotometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(10): 1935-1938.
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https://www.gpxygpfx.com/EN/Y2006/V26/I10/1935 |
[1] WANG Kui, TANG Ren-huan, XU Hui-bi(王 夔, 唐任寰,徐辉碧). Handbook of the Trace Element Analysis in Life Science and Data(生命科学中的微量元素分析与数据手册). BeiJing: China Measure Press(北京: 中国计量出版社),1998. 7. [2] Lippard S J, Berg J M. Translated by XI Zhen-feng, YAO Guang-qing, XIANG Si-fen, et al(Lippard S J, Berg J M著, 席振峰,姚光庆,项斯芬,等译). Principles of Bioinorganic Chemistry (生物无机化学原理). Beijing: Peking University Press(北京:北京大学出版社),2000. 2. [3] Chinese Academy of Sciences(中国科学院). 2004 Science Development Report(2004科学发展报告). Beijing: Science Press(北京:科学出版社), 2004. 80. [4] WANG Xiao-yi, Zhu W, Witkamp G T, et al(王小逸,Zhu W, Witkamp G T, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2003, 23(6): 1167. [5] XUE Guo-qing, LIU Qing, REN Xue-feng, et al(薛国庆,刘 青,任雪峰,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2004, 24(11): 1461. [6] YAN Ru-nan, WANG Jing-zhu, LIU Shu-ping, et al(阎汝南,王静竹,刘舒平,等). Science of Chinese Guangdong Trace Elements(广东微量元素科学), 1998, 5(9): 54. [7] Pharmacopoeia Committe of Ministry of Health, the People′s Republic of China(中华人民共和国药典委员会编). Pharmacopoeia of the People′s Republic of China (Part Ⅱ)(中华人民共和国药典,二部). Beijing: Chemical Industry Press(北京:化学工业出版社),2000. 163. [8] NIE Ling-yun, WU Mei-han(聂凌云,吴玫涵). Pharm. J. of Chinese People′s Liberation Army(解放军药学学报), 2001, 17(4): 198. [9] Irene Parejo, Francesc Viladomat, Jaume Bastida, et al. J. Agric. Food Chem., 2004, 52(7): 1890.
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