光谱学与光谱分析 |
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Determination of Six Metal Elements in Plant Bupleurum Scorzonerifolium Willd. by Flame Atomic Absorption Spectrophotometry(FAAS) |
XUE Guo-qing1, LIU Qing2, HAN Xiao-mei3, HAN Yu-qi1, WAN Yin-sheng1 |
1. Department of Chemistry, Hexi University, Zhangye 734000, China 2. The 4th Geoteam of the Gansu Nonfero Geoexploration Bureau, Zhangye 734000, China 3. Zhangye Medical College, Zhangye 734000, China |
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Abstract The objective in this paper was to determine the amount of metal elements in the Plant Bupleurum scorzonerifolium Willd. by flame atomic absorption spectrophotometry(FAAS). FAAS method was established for the determination of Ca, Mg, Fe, Cu, Zn and Pb in the Plant Bupleurum scorzonerifolium Willd. after digestion with HNO3-HClO4(V∶V=4∶1) at 90-95 ℃ and at normal pressure. In the meantime, the optimum parameters of FAAS and the effects of solution medium on the results were studied. The analytical results of Ca, Mg, Fe, Cu and Zn were 5 588.9, 1 790.5, 869.3, 78.4, 44.3 μg·g-1 respectively, and Pb was not checked out in the samples. The results showed that the recovery of standard addition was 99.57%-102.10%, the relative standard deviation (n=9) was 0.18%-2.26%. The method is quick, simple and convenient,and the results are satisfactory.
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Received: 2005-01-13
Accepted: 2005-04-26
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Corresponding Authors:
XUE Guo-qing
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Cite this article: |
XUE Guo-qing,LIU Qing,HAN Xiao-mei, et al. Determination of Six Metal Elements in Plant Bupleurum Scorzonerifolium Willd. by Flame Atomic Absorption Spectrophotometry(FAAS) [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2006, 26(06): 1173-1175.
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URL: |
https://www.gpxygpfx.com/EN/Y2006/V26/I06/1173 |
[1] WANG Kui(王 夔主编).Handbook of the Trace Element in Life Science Analysis and Data(生命科学中的微量元素分析与数据手册). Beijing: China Measure Press(北京:中国计量出版社), 1998. 7. [2] XI Zhen-feng, YAO Guang-qing, XIANG Si-fen, et al(席振峰,姚光庆,项斯芬,等译). Principles of Bioinorganic Chemistry(生物无机化学原理). Beijing: Peking University Press(北京:北京大学出版社), 2000. 2. [3] GONG Ji-yu, XU Tian-yang, YU Peng, et al(贡济宇,许天阳,于 澎, 等). Studies of Trace Elements and Health(微量元素与健康研究),2002,19(4):68. [4] YAN Ru-nan, WANG Jing-zhu, LIU Shu-ping, et al(阎汝南,王静竹,刘舒平, 等). Science of Guangdong Trace Elements(广东微量元素科学),1998,5(9):54. [5] The Pharmacopoeia Committee of PRC. Ch P(中国药典). Beijing: Chemical Industry Press(北京: 化工出版社), 2000, Vol.1, 232. [6] XUE Guo-qing, LIU Qing, REN Xue-feng, et al(薛国庆,刘 青,任雪峰,等). Spectroscopy and Spectral Analysis(光谱学与光谱分析),2004,24(11):1461. [7] YU Yu-hong, LI Xue-chun, WU Tao,et al(禹玉洪,李雪春,吴 涛, 等). China Journal Chinese Materia Medica(中国中药杂志),2004,29(6):521. [8] MAO Ren-gang, LIN Dong-hao, WANG Zhi-hua, et al(茅仁刚,林东昊,王智华, 等). Chinese Traditional and Herbal Drugs(中草药),2002,33(5):412. [9] SHAN Yu, FENG Xu, DONG Yun-fa, et al(单 宇,冯 煦,董云发, 等). Chinese Wild Plant Resources(中国野生植物资源),2004,23(4):5.
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