| 光谱学与光谱分析 |
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| Preconcentration with Crosslinked Chitosan for Determination of Trace Manganese in Waters by Flame Atomic Absorption Spectrometry |
| XUE Ai-fang, CHEN Hao*, LUO Xing-cai, WU Yu-qiong, XIE Jin-song |
| Sciences College, Huazhong Agricultural University, Wuhan 430070, China |
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Abstract A novel method for the preconcentration with crosslinked chitosan(CCTS) and determination of trace manganese in waters by flame atomic absorption spectrometry has been presented. The absorption rate of manganese(Ⅶ) by CCTS was 98% at pH 3.00. The effect of preconcentration time, dosage of CCTS, temperature, sample volume and co-existing elements have been investigated. The mechanism of adsorption of CCTS for Mn(Ⅶ) was also discussed. The detection limit of the method was 1.86 μg·L-1, and the relative standard deviation (RSD) was 2.0%(n=10). The method has been applied to the determination of trace manganese in south lake and changjiang water with satisfactory results.
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Received: 2005-05-18
Accepted: 2004-10-09
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Corresponding Authors:
CHEN Hao
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| Cite this article: |
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XUE Ai-fang,CHEN Hao,LUO Xing-cai, et al. Preconcentration with Crosslinked Chitosan for Determination of Trace Manganese in Waters by Flame Atomic Absorption Spectrometry [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(09): 1514-1517.
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| URL: |
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https://www.gpxygpfx.com/EN/Y2005/V25/I09/1514 |
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