| 光谱学与光谱分析 |
|
|
|
|
|
| Determination of Trace Elements in Radix Ophiopogonis by HG-ICP-AES |
| LOU Qi-zheng1,XU Run-sheng2 |
1. Department of Biology and Chemistry, Jinhua Education College, Jinhua 321000, China
2. Department of Chemistry，Zhejiang Normal University，Jinhua 321004，China |
|
|
|
|
Abstract In this paper, a method of microwave digestion technique for the contents determination of trace elements Ni，Zn，Mn，Cu，Mg，Fe，Ca and Pb in radix ophiopogonis by hydride generation inductively coupled plasma atomic emition spectrometry (HG-ICP-AES) was reported. Its recovery ratio obtained by standard addition method ranged between 97.8% and 102.5%, and its RSD was lower than 4.0%. The results of the determination show that radix ophiopogonis is rich in the inorganic elements such as Fe, and the content of Zn in radix ophiopogonis of Zhejiang is much higher in radix ophiopogonis of Sichun. The result will provide scientific data for the study on the elements in radix ophiopogonis and on their relativity of medicine efficacy.
|
|
Received: 2006-12-06
Accepted: 2007-02-16
|
|
|
|
Corresponding Authors:
LOU Qi-zheng
E-mail: qizhengl@hotmail.com
|
|
| Cite this article: |
|
LOU Qi-zheng,XU Run-sheng. Determination of Trace Elements in Radix Ophiopogonis by HG-ICP-AES[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(06): 1218-1221.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2007/V27/I06/1218 |
[1] SONG Li-ren, HONG Xun, DING Xu-liang, et al(宋立人，洪 恂，丁绪亮, 等). Modern Lexicon of Traditional Chinese Pharmacology(现代中药学大辞典). Beijing: People’s Health Publishing House(北京：人民卫生出版社), 2001. 951.
[2] The Official Committee of Hygine Department of the People′s Republic of China(中华人民共和国卫生部药典委员会). Pharmacopoeia of the People′s Republic of China(中华人民共和国药典，2005年，一部). Beijing：Chemical Industral Press(北京：化学工业出版社)，2005. 106.
[3] JIANG Feng-rong, ZHANG Xu, FAN Jun, et al(蒋凤荣，张 旭，范 俊，等). Archives of Traditional Chinese Medicine(中医药学刊)，2006，24(2)：236.
[4] ZHAO Yan-yan, LI Hui, ZHANG Qiu-yan(赵燕燕，李 挥，张秋燕). Chinese Traditional Patent Medicine(中成药)，2006，28(6)：886.
[5] FAN Jun, ZHANG Xu(范 俊，张 旭). Journal of Nanjing Traditional Chinese Medicine University(南京中医药大学学报)，2006，22(7)：270.
[6] FAN Jun, ZHANG Xiao-yan, GONG Jie-ning, et al(范 俊，张小燕，龚婕宁，等). Archives of Traditional Chinese Medicine(中医药学刊). 2006，24(5)：816.
[7] CHENG Cun-gui，HONG Qing-hong，LI Dan-ting，et al(程存归，洪庆红，李丹婷，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2006，26(9)：1735.
[8] CHENG Cun-gui，LI Dan-ting，LIU Xing-hai，et al(程存归，李丹婷，刘幸海，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2006，26(1)：156.
[9] ZHAO Ai-hong，WANG Jian-hua，SONG Zhi-gang，et al(赵爱红，王建华，宋志刚，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2006，26(11)：2137.
[10] XIE Jian-xin, DENG Bi-yang(谢建新，邓必阳). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2005，25(8)：1347.
[11] SUN Lian, LIU Hai, CHANG Jun-min, et al(孙 莲，刘 海，常军民，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2005，25(8)：1351.
[12] DU Bao-an, YANG Yu-hua, LI Zheng-ping(杜宝安，杨玉华，李正平). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2006，26(1)：140.
[13] HU Hao-bin，CAO Hong，LIU Jian-xin，et al(胡浩斌，曹 宏，刘建新，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2006，26(11)：2130.
[14] E Er-deng-sang，BAO Yin-da-lai，Na Ren-ge-rile(额尔登桑，宝音达来，娜仁格日乐). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2006，26(11)：2134.
[15] ZHAO Ai-hong, WANG Jian-hua, SONG Zhi-gang, et al(赵爱红，王建华，宋志刚，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析)，2006，26(11)：2137.
|
| [1] |
HE Yan1, TAO Ran1, YANG Ming-xing1, 2*. The Spectral and Technology Studies of Faience Beads Unearthed in Hubei Province During Warring States Period[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3700-3709. |
| [2] |
WANG Wei-en. Analysis of Trace Elements in Ophiocordyceps Sinensis From
Different Habitats[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3247-3251. |
| [3] |
WANG Yan1, HUANG Yi1, 2*, YANG Fan1, 2*, WU Zhong-wei2, 3, GUAN Yao4, XUE Fei1. The Origin and Geochemical Characteristics of the Hydrothermal Sediments From the 49.2°E—50.5°E Hydrothermal Fields of the Southwest Indian Ocean Ultra-Slow Spreading Ridge[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2868-2875. |
| [4] |
CHEN Chao-yang1, 2, LIU Cui-hong1, 2, LI Zhi-bin3, Andy Hsitien Shen1, 2*. Alexandrite Effect Origin of Gem Grade Diaspore[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2557-2562. |
| [5] |
CHEN Di, SONG Chen, SONG Shan-shan, ZHANG Zhi-jie*, ZHANG Hai-yan. The Dating of 9 Batches of Authentic Os Draconis and the Correlation
Between the Age Range and the Ingredients[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(06): 1900-1904. |
| [6] |
HE Yan1, SU Yue1, YANG Ming-xing1, 2*. Study on Spectroscopy and Locality Characteristics of the Nephrites in Yutian, Xinjiang[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(12): 3851-3857. |
| [7] |
CHEN Chao-yang1，HUANG Wei-zhi1，SHAO Tian1，LI Zhi-bin2，Andy Hsitien Shen1*. Characteristics of Visible Spectrum of Apatite With Alexandrite Effect[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(05): 1483-1486. |
| [8] |
LIU Yan-de, GAO Xue, JIANG Xiao-gang, GAO Hai-gen, LIN Xiao-dong, ZHANG Yu, ZHENG Yi-lei. Detection of Anthracnose in Camellia Oleifera Based on Laser-Induced Breakdown Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(09): 2815-2820. |
| [9] |
LU Xiao-ke1, LI Wei-dong1, LI Xin-wei2. Spectroscopic Analysis of Relics Unearthed from Xipo Site[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(04): 1186-1194. |
| [10] |
LIANG Piao-piao1, ZHOU Shan-shan1, XING Yun-xin1, LIU Ying1, 2*. Quantification of Trace Elements in Hair Samples from 156 Women Living in the Low-Selenium Region of Inner Mongolia by ICP-AES and AFS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(07): 2217-2222. |
| [11] |
HAO Xiao-jian*, TANG Hui-juan, HU Xiao-tao. Detection Sensitivity Improvement Study of LIBS by Combining Au-Nanoparticles and Magnetic Field[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(05): 1599-1603. |
| [12] |
LIU Hong-wei, NIE Xi-du*. Analysis of Trace Elements in Wild Artemisia Selengensis Using Inductively Coupled Plasma Tandem Mass Spectrometry[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(12): 3923-3928. |
| [13] |
CAI Shi-shi1，ZHANG En1, 2*. Trace Elements and U-Pb Ages of Zircons from Myanmar Jadeite-Jade by LA-ICP-MS: Constraints for Its Genesis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(06): 1896-1903. |
| [14] |
JIANG Bo1, 3, HUANG Jian-hua2*, LIU Wei2. Multi-Element Analysis of Wild Chinese Honeylocust Fruit by Inductively Coupled Plasma Tandem Mass Spectrometry (ICP-MS/MS)[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(12): 3859-3864. |
| [15] |
PENG Chuan-yi, ZHU Xiao-hui, XI Jun-jun, HOU Ru-yan, CAI Hui-mei*. Macro- and Micro-Elements in Tea (Camellia sinensis) Leaves from Anhui Province in China with ICP-MS Technique: Levels and Bioconcentration[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(06): 1980-1986. |
|
|
|
|
