| 光谱学与光谱分析 |
|
|
|
|
|
| Determination of Trace Elements in Traditional Chinese Medicine from Changbai Mountain by ICP-MS |
| YAO Yan-hong1,XU Gui-hua2,ZHANG Jing-dong1,LI Cheng-fan1,LI Dong-hao1 |
1. Analysis and Inspection Center, Yanbian University，Yanji 133002, China
2. Department of Chemistry, College of Science, Yanbian University，Yanji 133002, China |
|
|
|
|
Abstract The effects of different digestives for the fritillaria and atractylodes were compared. Many trace elements in the planted and wild fritillaria and atractylodes were determined by ICP-MS. The results show that the RSD and recovery are better if the planted and wild fritillaria and atractylodes were digested with HNO3-H2O2. Among the many elements determined from the fritillaria and atractylodes, Cu, Zn, Fe, Mg and Mn are the dominant chemicals. The content of Fe was higher in the wild fritillaria and atractylodes than that in the planted fritillaria and atractylodes, while the contents of heavy metal Pb and Cd were lower in the wild fritillaria and atractylodes than those in the planted fritillaria and atractylodes. The wild fritillaria and atractylodes contain Co，which was not determined in the planted fritillaria and atractylodes. The experimental results showed that the detection limits were lower than 0.086 ng·g-1 with low RSD（n=7, 4.85%）for most metal chemicals determined, and the standard recoveries (n=7) ranged from 96.8 to 103.4%.
|
|
Received: 2007-01-08
Accepted: 2007-03-12
|
|
|
|
Corresponding Authors:
YAO Yan-hong
E-mail: yhyao@ybu.edu.cn
|
|
[1] ZHOU Tian-ze(周天泽). Chinese Traditional and Herbal Drugs(中草药), 1990，21(10)：27.
[2] LONG Pei-xia，WANG Dong(龙沛霞，王 东). Studies of Trace Elements and Health(微量元素与健康研究), 1997，14(1)：59.
[3] DONG Shun-fu, ZHU Zhi-guo，LIU Jie，et al(董顺福，朱志国，刘 洁，等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1999，19(3)：406.
[4] FANG Yan-xiong, WANG Ya-li, ZHENG Sui-hua，et al(方岩雄，王亚莉，郑穗华，等). Herald of Medicine(医药导报), 2003，22(5)：324.
[5] LI Feng, LIAO Zhen-huan, DING Jian-hua, et al(李 风，廖振环, 丁建华, 等). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 2000，20(1)：58.
[6] WANG Xiao-ru，ZHUANG Zhi-xia，SUN Da-hai, et al. Atomic Spectroscopy, 1999，20（3）：86.
[7] WANG Xin-ping(王新平). Spectroscopy and Spectral Analysis(光谱学与光谱分析 ), 2005，25（2）：293.
|
| [1] |
HE Yan1, TAO Ran1, YANG Ming-xing1, 2*. The Spectral and Technology Studies of Faience Beads Unearthed in Hubei Province During Warring States Period[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3700-3709. |
| [2] |
ZHANG Yu-hui1, 2, DING Yong-kang3, PEI Jing-cheng1, 2*, GU Yi-lu1, 2, YU Min-da1, 2. Chemical Constituents and Spectra Characterization of Monocrystal
Rhodonite From Brazil[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3504-3508. |
| [3] |
WANG Wei-en. Analysis of Trace Elements in Ophiocordyceps Sinensis From
Different Habitats[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(10): 3247-3251. |
| [4] |
WANG Yan1, HUANG Yi1, 2*, YANG Fan1, 2*, WU Zhong-wei2, 3, GUAN Yao4, XUE Fei1. The Origin and Geochemical Characteristics of the Hydrothermal Sediments From the 49.2°E—50.5°E Hydrothermal Fields of the Southwest Indian Ocean Ultra-Slow Spreading Ridge[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2868-2875. |
| [5] |
CHEN Chao-yang1, 2, LIU Cui-hong1, 2, LI Zhi-bin3, Andy Hsitien Shen1, 2*. Alexandrite Effect Origin of Gem Grade Diaspore[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(08): 2557-2562. |
| [6] |
SUN Da-wei1, 2, 3, DENG Jun1, 2*, JI Bing-bing4. Study on the Preparation Mechanism of Steel Slag-Based Biomass Activated Carbon by Special Steel Slag-Discard Walnut Shells Based on ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(07): 2308-2312. |
| [7] |
CHEN Di, SONG Chen, SONG Shan-shan, ZHANG Zhi-jie*, ZHANG Hai-yan. The Dating of 9 Batches of Authentic Os Draconis and the Correlation
Between the Age Range and the Ingredients[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(06): 1900-1904. |
| [8] |
BI Yan-qi1, 2 , YANG Ying-dong3, DU Jing4, TANG Xiang5, LUO Wu-gan1, 2*. A Study on Mineral Material Sources of Multi-Style Bronzes Collected by Cultural Relic Administration Center of Huili County, Sichuan Province With MC-ICP-MS[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1140-1146. |
| [9] |
HE Yan1, SU Yue1, YANG Ming-xing1, 2*. Study on Spectroscopy and Locality Characteristics of the Nephrites in Yutian, Xinjiang[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(12): 3851-3857. |
| [10] |
WANG Zi-min1, MAO Xiao-tian1, YIN Zuo-wei1*, CHEN Chang2, CHENG Tian-jia1. Study on the Spectral Characteristics and the Color-Change Effect of Spinel[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(11): 3541-3545. |
| [11] |
JUMAHONG Yilizhati1, 2, TAN Xi-juan1, 2*, LIANG Ting1, 2, ZHOU Yi1, 2. Determination of Heavy Metals and Rare Earth Elements in Bottom Ash of Waste Incineration by ICP-MS With High-Pressure Closed
Digestion Method[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(10): 3168-3173. |
| [12] |
LUO Heng, Andy Hsitien Shen*. Based on Color Calculation and In-Situ Element Analyze to Study the Color Origin of Purple Chalcedony[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(06): 1891-1898. |
| [13] |
YANG Yan-ling1, Andy Hsitien Shen1, FAN Yu-rong2, HUANG Wei-zhi1, PEI Jing-cheng1*. UV-Vis-NIR Spectroscopic Characteristics of Vanadium-Rich
Hydrothermal Synthetic Emeralds From Russia[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1199-1203. |
| [14] |
ZHONG Yuan, QU Meng-wen, Andy Hsitien Shen*. Comparison of Chemical Composition and Spectroscopy of Purple- Brownish Red Garnet From Zambia, Tanzania and Australia[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(01): 184-190. |
| [15] |
DU Jing1，JIN Tao2, HU Feng-dan1, ZHANG Chi1, ZHU Tie-quan3, ZHAN Chang-fa3, LI Nai-sheng1, JIA Zheng1, CHEN Yue1*. Desalination Monitoring of Wooden Shipwreck Components of the Qing Dynasty Marine Shipwreck，Xiaobaijiao No.1[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(10): 3294-3298. |
|
|
|
|
