Abstract:The present study investigated the possibility of using near-infrared reflectance spectroscopy (NIRS) for quantitative determination of oligosaccharides, including sucrose, raffinose and stachyose in soybean products. One hundred and sixty samples (de-hulled soybean meal, extruded soybean meal, extruded full-fat soybean and fermented soybean meal) were collected and screened, and furthermore forty artificial soybean meal samples were prepared. Calibrations were performed by partial least squared algorithm with different derivatives, multiplicative scatter correction or normalization vector spectral pretreatment. The coefficients of determination for calibration (R2cal), coefficients of determination for cross validation (R2cv) and RPDcv in models were 0.99, 0.95, 0.98; 0.98, 0.94, 0.97; 7.24, 4.13, 5.98; respectively. The results supposed that NIRS can be a quantitative determination method of oligosaccharides in soybean products except fermented soybean meal.
王潇潇,李军涛,孙祥丽,韩苗苗,陈义强,张丽英. 近红外反射光谱快速测定四种大豆制品中寡糖含量的研究[J]. 光谱学与光谱分析, 2018, 38(01): 58-61.
WANG Xiao-xiao, LI Jun-tao, SUN Xiang-li, HAN Miao-miao, CHEN Yi-qiang, ZHANG Li-ying. Study on Rapid Determination of Oligosaccharides in Soybean Products by Near-Infrared Reflectance Spectroscopy. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(01): 58-61.
[1] Karr-Lilienthal L K,Kadzere C T,Grieshop C M,et al. Livestock Production Science,2005,97:12.
[2] Tanaka M,Thananumkul D,Lee T C,et al. Journal of Food Science,1975,40:1087.
[3] ZHANG Li-ying,QIAO Shi-yan,LI De-fa,et al(张丽英,谯仕彦,李德发,等). Chinese Journal of Animal Nutrition(动物营养学报),2004,16:20.
[4] WANG Yu-jun,JI Wei-dong,LI Yong-ping,et al(王玉军,纪伟东,李永平,等). Modern Food Science and Technology(现代食品科技),2010,26:750.
[5] Givens D I,DeBoever J L,Deaville E R. Nutrition Research Reviews,1997,10:83.
[6] Zhou L J,Zhang L Y,Zhang E X,et al. Animal Feed Science and Technology,2012,175:198.
[7] Garnsworthy P C,Wiseman J,Fegeros K. Journal of Agricultural Science,2000,135:409.
[8] Chen G L,Zhang B,Wu J G,et al. Animal Feed Science and Technology,2011,165:111.
[9] Montes J M,Utz H F,Schipprack W,et al. Plant Breeding,2006,125:591.
[10] Kovalenko I G,Rippke G R,Hurburgh C R. Journal of Agirculture and Food Chemistry,2006,54(10):3485.
[11] AACC,Near-Infrared Methods-Guidelines for Model Development and Maintenance. AACC 39-00.
[12] HU Ting,LU Wen-qing,WANG Xiang,et al(胡 婷,陆文清,王 翔,等). Feed and Husbandry(饲料与畜牧),2008,10:30.
[13] Norris K H,Williams P C. Cereal Chemistry,1984,61(2):158.
[14] Norris K H,Barnes R F,Moore J E,et al. Journal of Animal Science,1976,43:889.
[15] Windham W R,Morrison W H. Journal of Near Infrared Spectroscopy,1998,6:229.