光谱学与光谱分析 |
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Study on Rapid Determination and Analysis of Rocket Kerosene by Near Infrared Spectrum and Chemometrics |
XIA Ben-li1, CONG Ji-xin1, LI Xia2, WANG Xuan-jun2 |
1. Epidemic Prevention Team, Logistics Department, The General Equipment Logistics of CPLA, Beijing 100101, China 2. Section 503, Second Artillery Engineering University, Xi’an 710025, China |
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Abstract The rocket kerosene quality properties such as density, distillation range, viscosity and iodine value were successfully measured based on their near-infrared spectrum (NIRS) and chemometrics. In the present paper, more than 70 rocket kerosene samples were determined by near infrared spectrum,the models were built using the partial least squares method within the appropriate wavelength range. The correlation coefficients (R2) of every rocket kerosene’s quality properties ranged from 0.862 to 0.999. Ten unknown samples were determined with the model, and the result showed that the prediction accuracy of near infrared spectrum method accords with standard analysis requirements. The new method is well suitable for replacing the traditional standard method to rapidly determine the properties of the rocket kerosene.
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Received: 2010-08-30
Accepted: 2010-10-18
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Corresponding Authors:
XIA Ben-li
E-mail: xiaben88@163.com
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[1] Garrigues S, Andrade J M, de la Guardia M. Analytica Chimica Acta, 1995, 317: 95. [2] LI Xia, ZHOU You-jie, MU Xiao-gang(李 霞,周友杰,慕晓刚). Chemical Propellants & Polymeric Materials(化学推进剂与高分子材料), 2010, 8(2): 62. [3] Andrade J M, Soledad Muniategui, Mahia P L, et al. Fuel, 1997, 76(1): 51. [4] Carracedo M P G, Andrade J M, Calvino M, et al. Fuel, 2003, 82: 1211. [5] Smyth H E, Cozzolino D, Cynkar W U, et al. Anal. Bioanal. Chem., 2008, 390: 1913.
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