| 光谱学与光谱分析 |
|
|
|
|
|
| Spectroscopic Analysis Studies of Organo-Attapulgite/Nylon 6 Composites |
| SHI Jian-she, ZHANG Chun-xiang, YANG Xu-jie*, LU Lu-de, WANG Xin |
| Key Laboratory for Soft Chemistry and Fuctional Material of the Ministry of Education, Nanjing University of Science and Technology, Nanjing 210094, China |
|
|
|
|
Abstract The surface organic modification of attapulgite with silane coupling reagent was studied by Fourier transform infrared spectroscopy (FTIR) and X-ray photoelectron spectroscopy (XPS). Qrgano-attapulgite/nylon 6 composites with different content of attapulgite were prepared by means of melt blending, and the crystal structure and morphology were investigated. The results show that the surface content of Si, N and C of the modified attapulgite increased. Combined with the FTIR results, it was confirmed that an organic coating layer was formed on the surface of attapulgite. The adding of attapulgite does not change the crystal structure of nylon 6, but changes the crystallite size of nylon 6. The modified attapulgite was well dispersed in nylon 6 and the silane coupling coating on the attapilgite enhanced the interfacial adhesion.
|
|
Received: 2010-04-16
Accepted: 2010-07-18
|
|
|
|
Corresponding Authors:
YANG Xu-jie
E-mail: yangxj1210@163.com
|
|
[1] Chen Chengho, Li Hsiangyuan, Chien Chienyuan, et al. Journal of Applied Polymer Science, 2009, 112: 1063.
[2] Chen Guangxin, Kim Hunsik, Park Byunghyun, et al. Polymer, 2006, 47(13): 4760.
[3] Misra Rahul, Fu Bruce X, Plagge Andreas, et al. Journal of Polymer Science: Part B: Polymer Physics, 2009, 47(11): 1088.
[4] LU Hui-min, LI Xiao-hong, XU Xiang-min, et al(卢会敏, 李小红, 徐翔民, 等). Chinese Polymer Bulletin(高分子通报), 2006, (11): 63.
[5] Fabienne Samyn, Serge Bourbigot, Charafeddine Jama, et al. Polymer Degradation and Stability, 2008, 93(11): 2019.
[6] Wang Lihua, Sheng Jing. Polymer, 2005, 46(16): 6243.
[7] YAO Chao, ZENG Yong-bin, CHEN Zhi-gang, et al(姚 超, 曾永斌, 陈志刚, 等). Journal of the Chinese Ceramic Society(硅酸盐学报), 2009, 37(4): 485.
[8] Pan Bingli, Yue Qunfeng, Ren Junfang, et al. Polymer Testing, 2006, 25: 384.
[9] Shen Liang, Lin Yijian, Du Qiangguo, et, al. Polymer, 2005, 46: 5758.
[10] Xu Xiangmin, Li Binjie, Lu Huimin, et, al. Applied Surface Science, 2007, 254: 1456.
|
| [1] |
FAN Ping-ping，LI Xue-ying，QIU Hui-min，HOU Guang-li，LIU Yan*. Spectral Analysis of Organic Carbon in Sediments of the Yellow Sea and Bohai Sea by Different Spectrometers[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 52-55. |
| [2] |
YANG Chao-pu1, 2, FANG Wen-qing3*, WU Qing-feng3, LI Chun1, LI Xiao-long1. Study on Changes of Blue Light Hazard and Circadian Effect of AMOLED With Age Based on Spectral Analysis[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 36-43. |
| [3] |
BAO Hao1, 2，ZHANG Yan1, 2*. Research on Spectral Feature Band Selection Model Based on Improved Harris Hawk Optimization Algorithm[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 148-157. |
| [4] |
LI Qi-chen1, 2, LI Min-zan1, 2*, YANG Wei2, 3, SUN Hong2, 3, ZHANG Yao1, 3. Quantitative Analysis of Water-Soluble Phosphorous Based on Raman
Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(12): 3871-3876. |
| [5] |
LIANG Jin-xing1, 2, 3, XIN Lei1, CHENG Jing-yao1, ZHOU Jing1, LUO Hang1, 3*. Adaptive Weighted Spectral Reconstruction Method Against
Exposure Variation[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(11): 3330-3338. |
| [6] |
MA Qian1, 2, YANG Wan-qi1, 2, LI Fu-sheng1, 2*, CHENG Hui-zhu1, 2, ZHAO Yan-chun1, 2. Research on Classification of Heavy Metal Pb in Honeysuckle Based on XRF and Transfer Learning[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2729-2733. |
| [7] |
HUANG Chao1, 2, ZHAO Yu-hong1, ZHANG Hong-ming2*, LÜ Bo2, 3, YIN Xiang-hui1, SHEN Yong-cai4, 5, FU Jia2, LI Jian-kang2, 6. Development and Test of On-Line Spectroscopic System Based on Thermostatic Control Using STM32 Single-Chip Microcomputer[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2734-2739. |
| [8] |
ZHENG Yi-xuan1, PAN Xiao-xuan2, GUO Hong1*, CHEN Kun-long1, LUO Ao-te-gen3. Application of Spectroscopic Techniques in Investigation of the Mural in Lam Rim Hall of Wudang Lamasery, China[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2849-2854. |
| [9] |
WANG Jun-jie1, YUAN Xi-ping2, 3, GAN Shu1, 2*, HU Lin1, ZHAO Hai-long1. Hyperspectral Identification Method of Typical Sedimentary Rocks in Lufeng Dinosaur Valley[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2855-2861. |
| [10] |
WANG Jing-yong1, XIE Sa-sa2, 3, GAI Jing-yao1*, WANG Zi-ting2, 3*. Hyperspectral Prediction Model of Chlorophyll Content in Sugarcane Leaves Under Stress of Mosaic[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2885-2893. |
| [11] |
WANG Yu-qi, LI Bin, ZHU Ming-wang, LIU Yan-de*. Optimizations of Sample and Wavelength for Apple Brix Prediction Model Based on LASSOLars Algorithm[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(05): 1419-1425. |
| [12] |
LI Shuai-wei1, WEI Qi1, QIU Xuan-bing1*, LI Chuan-liang1, LI Jie2, CHEN Ting-ting2. Research on Low-Cost Multi-Spectral Quantum Dots SARS-Cov-2 IgM and IgG Antibody Quantitative Device[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1012-1016. |
| [13] |
JIN Cui1, 4, GUO Hong1*, YU Hai-kuan2, LI Bo3, YANG Jian-du3, ZHANG Yao1. Spectral Analysis of the Techniques and Materials Used to Make Murals
——a Case Study of the Murals in Huapen Guandi Temple in Yanqing District, Beijing[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1147-1154. |
| [14] |
DING Kun-yan1, HE Chang-tao2, LIU Zhi-gang2*, XIAO Jing1, FENG Guo-ying1, ZHOU Kai-nan3, XIE Na3, HAN Jing-hua1. Research on Particulate Contamination Induced Laser Damage of Optical Material Based on Integrated Spectroscopy[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(04): 1234-1241. |
| [15] |
ZHANG Bao-ping1, NING Tian1, ZHANG Fu-rong1, CHEN Yi-shen1, ZHANG Zhan-qin2, WANG Shuang1*. Study on Raman Spectral Characteristics of Breast Cancer Based on
Multivariable Spectral Data Analysis Methods[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(02): 426-434. |
|
|
|
|
