| 光谱学与光谱分析 |
|
|
|
|
|
| Synthesis and Character of Megastigmatrienone |
| WANG Jian-lin,YANG Shao-long,XU Yan-mei, ZHAO Qing-hua, QIAN Lan |
| Material and Chemical Engineering College of Zhengzhou University of Light Industry, Zhengzhou 450002, China |
|
|
|
|
Abstract In this synthetic route, the raw materials are obtained easily and the conditions of reactions are smoothly. The products in some main procedures of the route have high yieds. This synthetic route is a new way of the compound，there hasn’t been reported anywhere. It needs further studies to be practically applied. According to this synthetic routes, the authors studied technolygical conditions of the reactions of every step. Some products are analyzed by refractive index, IR, HNMR, and MS and confirmed its structure.
|
|
Received: 2004-03-06
Accepted: 2004-05-28
|
|
|
|
Corresponding Authors:
WANG Jian-lin
|
|
| Cite this article: |
|
WANG Jian-lin,YANG Shao-long,XU Yan-mei, et al. Synthesis and Character of Megastigmatrienone [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(03): 467-469.
|
|
|
|
| URL: |
|
https://www.gpxygpfx.com/EN/Y2005/V25/I03/467 |
[1] Roberts Ｄ Ｌ，Rhode Ｗ Ａ. Tobacco Ｓcience，1972, 16: 107.
[2] Demole Ｅ，Berthet Ｄ. Helvetica Chimica Acta，1972, 55: 1866.
[3] Rowland Ｋ Ｌ, USPat, 3, 211, 157(October12, 1965) & 3, 268, 589(August).
[4](a)Aasen Ａ Ｊ, Kimland Ｂ, Almquist Ｓ Enzell. Acta Chem., Scandinavica，1972, 26: 2573.
(b)Aasen Ａ Ｊ, Kimland Ｂ，Renzell Ｃ. Acta Chem., Scandinavica，1973, 27: 2107.
[5] Demole Ｅ，Enggist Ｐ. Helvetica Chimica Acta，1974, 57: 2087.
[6] Demole Ｅ，Enggist Ｐ. Helvetica Chimica Acta，1974, 57: 2089.
[7] Takazawa Ｏ, Tamura Ｈ, Kogami Ｋ，Hayshi Ｋ. Bull. Chem., Soc. Japan, 1982，55：1907.
[8] Max Ｊ Ｎ，Sondheimer Ｆ. Tetrahedron, Suppl. 8, Part Ⅰ, 1966，1.
[9] Ｉsler Ｏ, Montavon Ｍ, Ruegg Ｒ, Sauey Ｇ，Ｚeller Ｐ, US, Pat，1９５８，March, 18, 2，８2７，4８1.
[10] Dr P Edouard. Demole, Coppet, CH Pat 549961(11, 1, 1972).
[11] Sekiguchi A，Ando W. Chem. Lett.，1978: 1385.
|
| [1] |
LIU Jia1, 2, GUO Fei-fei2, YU Lei2, CUI Fei-peng2, ZHAO Ying2, HAN Bing2, SHEN Xue-jing1, 2, WANG Hai-zhou1, 2*. Quantitative Characterization of Components in Neodymium Iron Boron Permanent Magnets by Laser Induced Breakdown Spectroscopy （LIBS）[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2024, 44(01): 141-147. |
| [2] |
ZHANG Peng1, 3, YANG Yi-fan1, WANG Hui1, TU Zong-cai1, 2, SHA Xiao-mei2, HU Yue-ming1*. A Review of Structural Characterization and Detection Methods of Glycated Proteins in Food Systems[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(09): 2667-2673. |
| [3] |
LI Zhi1, WANG Xia1*, XU Can1*, LI Peng2, HUO Yu-rong1, FU Jing-yu1, WANG Pei1, FENG Fei3. Review of Spectral Characterization and Identification of Unresolved Space Objects[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2023, 43(05): 1329-1339. |
| [4] |
WANG Zhi-hao, YIN Yong*, YU Hui-chun, YUAN Yun-xia, XUE Shu-ning. Early Warning Method of Apple Spoilage Based on 2D Hyperspectral
Information Representation With Pixel Mean and Variance[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(07): 2290-2296. |
| [5] |
XU Heng-shan2, GONG Guan-qun1, 2*, ZHANG Ying-jie1, 2, YUAN Fei2, ZHANG Yong-xia2. The Spectroscopic Characteristics of Fulvic Acid Complexed With Copper Ion and the Construction of the Mechanism of Action[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2022, 42(04): 1010-1016. |
| [6] |
KONG Hui-hua1, 2, LIAN Xiang-yuan1, CHEN Ping2, PAN Jin-xiao1, 2. Research on Color Characterization of Material Components Based on Spectral CT[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(11): 3612-3617. |
| [7] |
YAO Jing-jing1, 2, YAN Yue-er3, ZHANG Ruo-hong1, LUO Chan1, LIU Jun1, BI Ning1*, TANG Yi2*. Spectroscopic Detection and Analysis for Micro Structure of Aged Traditional Handmade Paper[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2021, 41(05): 1559-1565. |
| [8] |
ZENG Jian-hua, MENG Yan, LIU Lin-lin, YANG Yang, LI Mei-ying, WANG Zi-yue, ZHU Xiu-qing*, SHI Yan-guo*. Characterization and Effects of pH on the Conformation of Hemp Protein Isolate Based on Multi-Spectroscopic Technique[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2020, 40(12): 3748-3754. |
| [9] |
SONG Si-yue, LIU Xu-wei, LIN Hong-xiao, WANG Xue-jin*，HE Zhi-wei. Spectral Characterization of Electrodeposited Cu2ZnSnS4 Thin Films on Fluorine-Doped Tin Oxide[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(09): 2940-2945. |
| [10] |
HE Jiang-long, HUANG Ming-li, LI Ling-yu, NIE Zhao-guang, GENG Cun-zhen, YAN Dong-yun*. Stability and Structural Characterization of Chelated Fertilizers[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2019, 39(09): 2966-2973. |
| [11] |
XIAO Xue-feng1, SUN Yong-jun1, 2*, SHEN Hao1, SUN Wen-qaun1, ZHENG Huai-li3, XU Yan-hua2, ZHU Cheng-yu1. Spectral Characterizations of CSC-P(AM-AA) with Function of Trapping Heavy Metals and Its Removal Efficiency of Cu2+[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(06): 1809-1813. |
| [12] |
JIANG Zhong-min1, KONG Ling-jun2, NIE Peng1, YU Hai-qi1. Study on the Spectral Characterization Model of Multi-Color Printer Based on LabPQR Dimension Reduction[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2018, 38(06): 1975-1981. |
| [13] |
ZHANG Zheng-an1, 2, ZHENG Huai-li1, 3*, HUANG Fei2, FU Mao-mei4, LI Xiang1, 3, ZHOU Yu-hao1, 3. Ultraviolet-Initiated Template Polymerization of Cationic Polyacrylamide and Its Sludge Dewatering Performance[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(08): 2480-2485. |
| [14] |
SUN Yong-jun1, 2, ZHENG Huai-li3, ZHAO Chun3, XIAO Xue-feng1, XU Yan-hua2, WU Hui-fang1, SUN Wen-quan1, REN Meng-jiao1, ZHU Cheng-yu1. The Spectral Characterizations of Chitosan Based Flocculants Synthesized by Photopolymerization[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(08): 2527-2532. |
| [15] |
DAI Ze-lin, XU Xiang-dong*, GU Yu, ZOU Rui-jiao, HAN Shou-sheng, PENG Yong, LIAN Yu-xiang, WANG Fu, LI Xin-rong, CHEN Zhe-geng, SUN Ming-hui, JIANG Ya-dong. Experimental and Theoretical Study on Terahertz Spectra for Regenerated Cellulose [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2017, 37(03): 697-703. |
|
|
|
|
