光谱学与光谱分析 |
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Research on Raman Spectra of Glycerinat at the Pressure of 0-1.0 GPa and the Temperature of 29 ℃ |
LIU Jun-jie, ZHENG Hai-fei* |
School of Earth and Space Sciences, Peking University, Beijing 100871, China |
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Abstract The present paper investigates Raman spectral characters of liquid glycerin by the experiment at the pressure of 0-1.0 GPa and the temperature of 29 ℃, and defines the relation between the pressure and the Raman peak of glycerin at ambient temperature. The result shows that there are two characteristic Raman peaks of glycerin defined as ν(CH) and ν(CH2), and both of them move to higher positions as system pressure increases. The relation between the system pressure and peak positions of glycerin is given as the following: ν(CH)=0.009 2P+2 886.67 and ν(CH2)=0.009 4P+2 948.53. On the other hand, glycerin is reliable as a liquid pressure gauge for high pressure experiment. The equation applied to demarcate system pressure is also showed: P=106.4 ν(CH2)-3.14×105.
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Received: 2004-06-30
Accepted: 2004-10-15
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Corresponding Authors:
ZHENG Hai-fei
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Cite this article: |
LIU Jun-jie,ZHENG Hai-fei. Research on Raman Spectra of Glycerinat at the Pressure of 0-1.0 GPa and the Temperature of 29 ℃ [J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2005, 25(11): 1817-1820.
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URL: |
https://www.gpxygpfx.com/EN/Y2005/V25/I11/1817 |
[1] ZENG Guo-tao, XU Meng-hong(曾国涛, 徐梦红). Petrolic Geochemistry(石油地球化学). Beijing: Petrolic Industry Press(北京: 石油工业出版社), 1990. [2] LI Wei-hua, DUAN Yu-ran(李维华,段玉然). Spectroscopy and Spectral Analysis(光谱学与光谱分析), 1998,18(4):429. [3] Marvin C T. Lascer Raman Spectroscopy. New York: Wiley-Interscience, 1970, 35: 87. [4] TANG Hui-tong(唐恢同). The Spectral Authentication for Organic Compound(有机化合物的光谱鉴定). Beijing: Peking University Press(北京:北京大学出版社), 1992. 105. [5] JIN Hai-ru, ZHU Ge-jian(金海如,诸葛健). China Surfactant Detergent and Cosmetics(日用化学工业), 2000, 30(5): 37. [6] WANG Wen-ke(王文科). Journal of Beijing University of Chemcal Technology(北京化工大学学报, 自然科学版), 1995, 22(4): 81. [7] Cheol-Joong Kim, et al. Fluid Phase Equilibria, 2002, 51-65: 198. [8] Schmidt C, Ziemann M A. American Mineralogist, 2000, 85: 1725. [9] PAN Ja-lai(潘家来). The Application of Raman Spectra to Organic Chemistry(激光拉曼光谱在有机化学上的应用). Beijing: Chemical Industry Press(北京: 化学工业出版社), 1996. [10] XU Pei-cang , LI Ru-bi , WANG Yong-qiang(徐培苍, 李如璧, 王永强). Raman Spectroscopy in Geosciences(地学中的拉曼光谱). Xi'an: Shanxi Science and Technology Press(西安:陕西科学技术出版社), 1996.
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