| 光谱学与光谱分析 |
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| Enlargement Test of Synthesis of MCM-22 Zeolite by Means of XRD |
| SHI Jian-gong1,3,LU Guan-zhong1,CAO Gang2,YU Xiao-dong2 |
1. Research Institute of Industrial Catalysis, East China University of Science and Technology, Shanghai 200237, China
2. Chemicals Division, Beijing Yanshan Petrochemical Corp., SINOPEC, Beijing 102500, China
3. Xingye Tech. Devel. Corp., Beijing Yanshan Petrochemical Corp., SINOPEC, Beijing 102500, China |
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Abstract On the basis of MCM-22 zeolite synthesis at the static condition in 100 mL lined PTFE autoclave, 250 and 1 000 mL stainless steel autoclave respectively, the synthesis of MCM-22 zeolite was studied at the rotating condition in 2, 5 and 200 L autoclave respectively. The samples as-synthesized and calcined were characterized by means of XRD and so on. The results show that all the synthesized samples are the pure MCM-22 zeolites, and their crystallinities were high, and MCM-22 zeolite can be synthesized successfully at the rotating condition in 200 L stainless steel autoclave.
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Received: 2006-02-14
Accepted: 2006-06-29
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Corresponding Authors:
SHI Jian-gong
E-mail: shijiangong@126.com
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| Cite this article: |
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SHI Jian-gong,LU Guan-zhong,CAO Gang, et al. Enlargement Test of Synthesis of MCM-22 Zeolite by Means of XRD[J]. SPECTROSCOPY AND SPECTRAL ANALYSIS, 2007, 27(05): 1032-1035.
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https://www.gpxygpfx.com/EN/Y2007/V27/I05/1032 |
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