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| Preparation, Characterization and Catalytic Properties of
ZnO/ZnSe Composites |
| ZHANG Xiao-kai1, JIANG Rui-feng2, FU Xiao-xue2, LIU Zhong-min3* |
1. School of Physics and Electronics, Shandong Normal University, Jinan 250014, China
2. School of Chemistry, Chemical Engineering and Materials Science, Shandong Normal University, Jinan 250014, China
3. Management Office of Asset and Laboratory, Shandong Normal University, Jinan 250014, China
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Abstract An improved two-step heat of hydration method was used to prepare a core-shell structured ZnO/ZnSe composite material. Zinc oxide nanoparticles were prepared with zinc acetate and diethanolamine, and a selenium-containing anion solution was prepared with selenium powder and sodium borohydride. The optimal condition of Zn∶Se=1.6∶1 was obtained by adjusting the ratio of raw materials, and a spherical core-shell structure was prepared. ZnO/ZnSe, combined with transmission electron microscope, X-ray powder diffractometer, ultraviolet-visible spectrophotometer, photoluminescence spectroscopy, X-ray photoelectron spectroscopy to characterize the material composition and morphological structure, and its photocatalytic activity is analyzed and studied.
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Received: 2021-09-20
Accepted: 2023-12-22
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Corresponding Authors:
LIU Zhong-min
E-mail: liuzhongmin@sdnu.edu.cn
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